CN106592223A - Water-proofing, oil-proofing and antifouling type easy-care finishing liquid of shirt and finishing method of water-proofing, oil-proofing and antifouling type easy-care finishing liquid - Google Patents
Water-proofing, oil-proofing and antifouling type easy-care finishing liquid of shirt and finishing method of water-proofing, oil-proofing and antifouling type easy-care finishing liquid Download PDFInfo
- Publication number
- CN106592223A CN106592223A CN201611190549.7A CN201611190549A CN106592223A CN 106592223 A CN106592223 A CN 106592223A CN 201611190549 A CN201611190549 A CN 201611190549A CN 106592223 A CN106592223 A CN 106592223A
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- Prior art keywords
- shirt
- proofing
- water
- drying
- pressing
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- 239000007788 liquid Substances 0.000 title claims abstract description 50
- 238000000034 method Methods 0.000 title claims abstract description 27
- 230000003373 anti-fouling effect Effects 0.000 title claims abstract description 18
- 239000002939 oilproofing Substances 0.000 title abstract 6
- 238000004078 waterproofing Methods 0.000 title abstract 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 12
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 10
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 8
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 7
- 235000019830 sodium polyphosphate Nutrition 0.000 claims abstract description 5
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 4
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 claims abstract description 4
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 4
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000001273 butane Substances 0.000 claims abstract description 4
- 239000000839 emulsion Substances 0.000 claims abstract description 4
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 4
- 239000001630 malic acid Substances 0.000 claims abstract description 4
- 235000011090 malic acid Nutrition 0.000 claims abstract description 4
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims abstract description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229920001451 polypropylene glycol Polymers 0.000 claims abstract description 4
- 229910001379 sodium hypophosphite Inorganic materials 0.000 claims abstract description 4
- VACCAVUAMIDAGB-UHFFFAOYSA-N sulfamethizole Chemical compound S1C(C)=NN=C1NS(=O)(=O)C1=CC=C(N)C=C1 VACCAVUAMIDAGB-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims description 55
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- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 12
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- 238000000643 oven drying Methods 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
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- 229910021529 ammonia Inorganic materials 0.000 claims description 6
- 238000000889 atomisation Methods 0.000 claims description 6
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 6
- 238000009992 mercerising Methods 0.000 claims description 6
- 238000000465 moulding Methods 0.000 claims description 6
- 238000005096 rolling process Methods 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 239000011265 semifinished product Substances 0.000 claims description 6
- 238000004513 sizing Methods 0.000 claims description 6
- 238000009987 spinning Methods 0.000 claims description 6
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- 150000001408 amides Chemical class 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 239000010977 jade Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 230000007935 neutral effect Effects 0.000 claims description 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 239000008279 sol Substances 0.000 claims description 3
- 239000012224 working solution Substances 0.000 claims description 3
- 239000004831 Hot glue Substances 0.000 claims description 2
- 241000165940 Houjia Species 0.000 claims description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 2
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 claims description 2
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- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 2
- 229910000077 silane Inorganic materials 0.000 claims description 2
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 claims description 2
- 235000021286 stilbenes Nutrition 0.000 claims description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 1
- 150000003376 silicon Chemical class 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract description 14
- 238000005406 washing Methods 0.000 abstract description 13
- 230000007613 environmental effect Effects 0.000 abstract description 4
- -1 polyethylene Polymers 0.000 abstract description 4
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 abstract description 3
- 239000004327 boric acid Substances 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 2
- 229920001296 polysiloxane Polymers 0.000 abstract description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 abstract description 2
- ZTGKHKPZSMMHNM-UHFFFAOYSA-N 3-(2-phenylethenyl)benzene-1,2-disulfonic acid Chemical class OS(=O)(=O)C1=CC=CC(C=CC=2C=CC=CC=2)=C1S(O)(=O)=O ZTGKHKPZSMMHNM-UHFFFAOYSA-N 0.000 abstract 1
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 239000004698 Polyethylene Substances 0.000 abstract 1
- BWKOZPVPARTQIV-UHFFFAOYSA-N azanium;hydron;2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [NH4+].OC(=O)CC(O)(C(O)=O)CC([O-])=O BWKOZPVPARTQIV-UHFFFAOYSA-N 0.000 abstract 1
- 229920000573 polyethylene Polymers 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- NBXZNTLFQLUFES-UHFFFAOYSA-N triethoxy(propyl)silane Chemical compound CCC[Si](OCC)(OCC)OCC NBXZNTLFQLUFES-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 13
- 238000012360 testing method Methods 0.000 description 11
- 238000010409 ironing Methods 0.000 description 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 9
- 230000008901 benefit Effects 0.000 description 6
- 239000004753 textile Substances 0.000 description 5
- 229920000742 Cotton Polymers 0.000 description 4
- 241000219146 Gossypium Species 0.000 description 4
- 208000031481 Pathologic Constriction Diseases 0.000 description 4
- 210000001215 vagina Anatomy 0.000 description 4
- 230000037303 wrinkles Effects 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical class OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 2
- 125000003368 amide group Chemical group 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- NNTWKXKLHMTGBU-UHFFFAOYSA-N 4,5-dihydroxyimidazolidin-2-one Chemical compound OC1NC(=O)NC1O NNTWKXKLHMTGBU-UHFFFAOYSA-N 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- 208000024780 Urticaria Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 238000005815 base catalysis Methods 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 229920001222 biopolymer Polymers 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
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- 230000007812 deficiency Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002964 excitative effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
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- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 229920000137 polyphosphoric acid Polymers 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/11—Oleophobic properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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Abstract
The invention discloses a water-proofing, oil-proofing and antifouling type easy-care finishing liquid of a shirt and a finishing method of the water-proofing, oil-proofing and antifouling type easy-care finishing liquid. The water-proofing, oil-proofing and antifouling type easy-care finishing liquid of the shirt is prepared from the following raw materials including butane tetracid, amine citrate, triethanolamine, malic acid, sodium hypophosphite, boric acid, a stilbene disulfonic acid derivative, polyethylene wax, magnesium chloride, a bisamino silicone emulsion, chitosan, N, N-dimethylformamide, titanium dioxide, polypropylene glycol 200, propyl triethoxy silane, tetraethoxysilane, sodium polyphosphate, silicasol, concentrated hydrochloric acid, alkyl alcohol amide polyoxyethylene ether, a proper amount of maleic anhydride, a proper amount of anhydrous alcohol and a proper amount of deionized water. According to the finishing liquid and the finished shirt finishing method, a functional shirt with functions of antiwrinkling, oil-proofing, water-proofing and antifouling is produced, is super in protection, durable in performance, not liable to discolor and yellow after repeated washing, soft and comfortable in hand feeling and fresh and natural to wear and is breathable, comfortable, green, environmental friendly and health without stimulation.
Description
Technical field
The present invention relates to ready-made clothes functional treatment technical field, more particularly to a kind of waterproof and oilproof anti-fouling type of shirt is non-ironing
Dressing liquid and its method for sorting.
Background technology
Cotton ready-made clothes is so that its is comfortable and easy to wear, natural environmental-protective the features such as it is very popular, but due in dress and washing
During exist and easily wrinkle, be difficult the performance deficiency arranged, the life for giving people brings inconvenience.Therefore wear and relax
Suitable, flat crease-resistant ready-made clothes application prospect that is very tangible, non-ironing, conveniently arranging is very wide.And current most popular N-
The crease-shedding finishing agent of methylol class, it may appear that formaldehyde, pH value be exceeded and residuals cause the problem of skin urtication, causes wide
Big consumer is panic to the psychology of crease-resistant ready-made clothes security performance, simultaneously because the crease-resistant process of tradition changes to original fabric performance
Become, cause to lose the original water suction of cotton ready-made clothes, lead wet comfort property, therefore produce meet market public demand into
Clothing is of great significance.
By patent retrieval, the contrast patent of Patent No. 201010300167.1, a kind of cotton shirt is it discloses
No-iron treatment method, step is successively Resin Absorbent → preliminary drying → pressing → bake → cool down；Resin Absorbent step is will be main
The working solution of component modification bishydroxymethyl dihydroxy ethylene urea or modified alkyl dihydroxy ethylene urea is applied on shirt, raw
Output has the cotton shirt of wash and wear, although resin is being given birth to through modification, but due to the reversibility of modifying process
Produce, accumulating and wear during use easily generation formaldehyde indirectly, can not completely by work by last cooling link
Residuals are removed clean in liquid, there is that formaldehyde, pH value content are unstable, wear excitatory safe and environmentally friendly hidden danger.
A kind of contrast patent 2 of Patent No. 201410639422.3, the formaldehydeless antibacterial that it discloses shirt is non-ironing whole
Reason liquid and method for sorting, its adopt ready-made clothes prewashing-drying-dressing liquid process-determine wet drying-pressing-bake-static equilibrium-into
The technological process of clothing after backwashing-drying is processed shirt, in this invention before and after dry production link twice, employing is
40-60 DEG C of oven drying at low temperature temperature, while be " 6-12h " the time required to static equilibrium production link, with duration, production efficiency
It is low, it is unfavorable for industrialization, streamlined, mass, large-scale production, economic and social benefit is low；It is multiple in ready-made clothes prewashing and ready-made clothes
Wash and wash in link twice, there is a problem of water resources consumption greatly and environment protection emission, be unfavorable for energy-saving and emission-reduction.Repeatedly wash simultaneously
Wash and easily occur clothes when shirt washing quantity is more and mutually wind, knot and cause the serious fold of clothes, outward appearance poor
Problem, affects crease-resistant rank and product quality, and utilization rate of equipment and installations is low during negligible amounts, and scale and benefit are poor.For prior art
The problem and defect of presence, the present invention provides a kind of environmentally friendly noniron finish liquid and its ready-made clothes method for sorting so that produce
Ready-made clothes reaches non-ironing, Water-proof and oil-proof, antifouling performance, and safe and healthy, ring on the basis of original wrinkle resistance is kept
Protect, easily realize industrialization, streamlined, mass and scale, reach huge economic benefit and social benefit.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of waterproof and oilproof anti-fouling type of shirt is non-ironing
Dressing liquid and its method for sorting.
The present invention is achieved by the following technical solutions：
A kind of waterproof and oilproof anti-fouling type noniron finish liquid of shirt, is made up of the raw material of following weight portion：Butane tetracid 24-
26th, Fructus Citri Limoniae acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8-1, boric acid 0.27-0.3, two
The semi-annular jade pendant acid derivative 2-2.5 of styrene two, Tissuemat E 1.3-1.6, magnesium chloride 0.4-0.5, double amido organosilicon emulsions 2-3, shell
Polysaccharide 4.5-5, DMF 68-80, titanium dioxide 1.2-1.4, the 0.25-0.4 of polypropylene glycol 200, the second of propyl group three
TMOS 0.6-0.8, tetraethoxysilane 0.3-0.5, sodium polyphosphate 0.3-0.4, Ludox 3.2-3.5, concentrated hydrochloric acid
1.2-1.4, alkylolamideses polyoxyethylene ether 0.35-0.5, appropriate maleic anhydride, appropriate dehydrated alcohol, appropriate deionized water.
A kind of waterproof and oilproof anti-fouling type noniron finish liquid of shirt, is made up of following concrete steps：
（1）Titanium dioxide granule is added in the 15-18 times of dehydrated alcohol measured, the ethoxy of propyl group three is added after magnetic agitation 30min
Base silane and tetraethoxysilane, in system with the speed Deca concentrated hydrochloric acid of 5 seconds one drops after 30min, stir 48h, Ran Houjia
Enter sodium polyphosphate high shear agitation 10-20min, stirring adds Ludox to continue stirring 1-1.5h and obtains modified silicon after terminating
Colloidal sol is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water
Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will
Standby solidss and deionized water mixing are placed in the container with agitating device, are stirred and are added step to after being completely dissolved
（1）The product and alkylolamideses polyoxyethylene ether of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred
Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
A kind of noniron finish method of shirt ready-made clothes, is made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved using compact spinning technique, and uses liquefied ammonia
+ mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high high quality fabric；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into into separate panels；
（3）Filler rod：With filler rod technology, hot melt adhesive tape or lining cloth are sewed at suture, then through pressing work
Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension
Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol,
Simultaneously the dressing liquid for descending slowly and lightly is collected by blood circulation and recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine
Dimension liquid carrying rate is controlled in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 80-
105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140-
160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 60-65%
Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55-
80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90-
105 DEG C, the Drying and cooling time is 15-30min.
It is an advantage of the invention that：Shitosan as the unique positively charged native biopolymer polysaccharide of nature, due to
Nantural non-toxic degradable, good biocompatibility, antibiotic property are used as excellent dyeing accelerant, shrink-resistant agent, antibacterial
Etc. being widely used in textile process industry, substantial amounts of hydroxyl and amino group are contained in the surface of shitosan, and biological activity is high, are conducive to
The Shrinkproof crease-resistant effect of finishing agent is improved, water insoluble due to shitosan, the present invention is using dimethylformamide as reaction
Medium, N- maleylations is carried out to shitosan and is modified, and water solublity is improved, using propyl-triethoxysilicane to titanium dioxide granule
It is modified, reduces surface energy, also makes to enter one with the silicone hydroxyl of Ludox by acid-base catalysises effect using tetraethoxysilane
Step condensation bonding, improves the performances such as mechanical performance, chemical stability and automatically cleaning, the grease-proof and waterproof of Ludox, recycles modified
Shitosan colloidal sol and modified Ludox be compounded to form hybrid collosol, and polybasic carboxylic acid compound etc. is in the work of composite catalyst
With under, made by dressing liquid cellulosic molecule can be coupled together with the hydroxyl reaction of cellulose, formed ester crosslinking three-dimensional
Network, gives wrinkle resistance in fabrics, easy-care properties, antifouling self-cleaning property, the feel that improve fabric, the strength for enhancing fabric, and
Washability.
In addition the shirt ready-made clothes method for sorting that the present invention is provided avoids in convection oven drying mode to go out between different garment pieces
Existing cold wave problem of non-uniform, the clothes that reduction tradition drying drying is brought winds, piles up the fold of generation and cause shirt
The poor problem of outward appearance, can in shirt obtain huge energy fiber molecule rapidly be cooled down so as to acquisition it is crease-resistant
Performance is solidified rapidly, reaches excellent non-ironing rank, in the wasting of resources and environmental protection row that avoid traditional water-washing method from producing
While putting problem, the shirt feel after process is very soft, nature comfortable and easy to wear, after testing through this patent production into
Clothing, before washing water absorption be less than or equal to 8s, washing 50 times after water absorption within 25s, while its content of formaldehyde reaches and does not examine
The basic security performance indications such as the level for going out, pH value, abnormal flavour and decomposable asymmetric choice net carcinogenic aromatic amine dyestuff are up to state standards requirement, do
To environmental protection, safety, noresidue, and flat appearance degree, rivel outward appearance, seam outward appearance are higher by the 0.5-1 levels of national standard.Simultaneously
The production of industrialization, streamlined, mass, scale is realized, preferably economic and social benefit is reached.
Dressing liquid and shirt ready-made clothes method for sorting that the present invention is provided, have produced with wrinkle resistant, grease proofing, waterproof, antifouling
Feature shirt, super protection, consistency of performance, repeated washing is difficult complexion changed and xanthochromia, and feel is softly comfortable, wears pure and fresh
It is natural, to breathe freely comfortable, environmental protection, health is non-stimulated.
Specific embodiment
The waterproof and oilproof anti-fouling type noniron finish liquid of a kind of shirt, by following weight portion（Kilogram）Raw material make：
Butane tetracid 24, Fructus Citri Limoniae acid amide 16, triethanolamine 2.5, malic acid 0.9, sodium hypophosphite 0.8, boric acid 0.27, the semi-annular jade pendant of stilbene two
Acid derivative 2, Tissuemat E 1.3, magnesium chloride 0.4, double amido organosilicon emulsions 2, shitosan 4.5, DMF
68th, titanium dioxide 1.2, polypropylene glycol 200 0.25, propyl-triethoxysilicane 0.6, tetraethoxysilane 0.3, polyphosphoric acids
Sodium 0.3, Ludox 3.2, concentrated hydrochloric acid 1.2, alkylolamideses polyoxyethylene ether 0.35, appropriate maleic anhydride, appropriate dehydrated alcohol,
Appropriate deionized water.
A kind of waterproof and oilproof anti-fouling type noniron finish liquid of shirt, is made up of following concrete steps：
（1）Titanium dioxide granule is added in the dehydrated alcohol of 15 times of amounts, propyl-triethoxysilicane is added after magnetic agitation 30min
Alkane and tetraethoxysilane, in system with the speed Deca concentrated hydrochloric acid of 5 seconds one drops after 30min, stir 48h, are subsequently adding many
Polyphosphate sodium high shear agitation 10min, stirring adds Ludox continuation stirring 1h to obtain modified silicasol after terminating standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water
Stirring reaction 7h at 100 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will be standby
Solidss and deionized water mixing are placed in the container with agitating device, are stirred and are added step to after being completely dissolved（1）Prepare
Product and alkylolamideses polyoxyethylene ether, regulation system pH value is standby to 7 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred
Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
Case study on implementation 1：By taking 80 diclinic stricture of vagina shirt production as an example:
（1）Fabric is preferred：Select the 80 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Adopt needle gage garment piece is sewed for the filler rod overseam technology of three centimeter of 16 pin, obtain semi-finished product lining
Shirt；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, make ready-made clothes face liber band liquid
Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 105
DEG C, preliminary drying time 90s makes shirt be 45% containing damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 160 DEG C, and pressing pressure is 13kg/cm2, during pressing
Between 30s；
（7）Bake sizing：Baking temperature is 185 DEG C, bakes the time for 50s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 65% constant temperature
In constant humidity sealing cooling room, 30min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 105
DEG C, the Drying and cooling time is 30min.
The Testing index and standard GB/T/T 18863- of shirt its ironing-free performance that the production of case study on implementation 1 is completed
2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 2：By taking 80 double flat stricture of vagina shirt production as an example：
（1）Fabric is preferred：Select the 80 double flat pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Adopt needle gage garment piece is sewed for the filler rod overseam technology of three centimeter of 17 pin, obtain semi-finished product lining
Shirt；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, make ready-made clothes face liber band liquid
Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 100
DEG C, preliminary drying time 80s makes shirt be 42% containing damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 155 DEG C, and pressing pressure is 10kg/cm2, during pressing
Between 26s；
（7）Bake sizing：Baking temperature is 180 DEG C, bakes the time for 30s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 65% constant temperature
In constant humidity sealing cooling room, 25min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 75%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 100
DEG C, the Drying and cooling time is 25min.
The Testing index and standard GB/T/T 18863- of shirt its ironing-free performance that the production of case study on implementation 2 is completed
2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 3：By taking 100 diclinic stricture of vagina shirt production as an example：
（1）Fabric is preferred：Select the 100 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Adopt needle gage garment piece is sewed for the filler rod overseam technology of three centimeter of 19 pin, obtain semi-finished product lining
Shirt；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, make ready-made clothes face liber band liquid
Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 95
DEG C, preliminary drying time 95s makes shirt be 35% containing damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 150 DEG C, and pressing pressure is 5kg/cm2, the pressing time
22s；
（7）Bake sizing：Baking temperature is 170 DEG C, bakes the time for 90s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 65% constant temperature
In constant humidity sealing cooling room, 15min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 65%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 95 DEG C,
The Drying and cooling time is 20min.
The Testing index and standard GB/T/T 18863- of shirt its ironing-free performance that the production of case study on implementation 3 is completed
2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
Case study on implementation 4：By taking 120 diclinic stricture of vagina shirt production as an example：
（1）Fabric is preferred：Select the 120 diclinic pattern fabrics of long-staple cotton compact spinning through liquefied ammonia+mercerising technical finesse；
（2）Three-dimensional cutting：Fabric is cut into by separate panels using three-dimensional cutting technology；
（3）Filler rod：Adopt needle gage garment piece is sewed for the filler rod overseam technology of three centimeter of 21 pin, obtain semi-finished product lining
Shirt；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, make ready-made clothes face liber band liquid
Rate is controlled 50%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 80
DEG C, preliminary drying time 110s makes shirt be 20% containing damp rate；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, pressing temperature is 140 DEG C, and pressing pressure is 3kg/cm2, the pressing time
12s；
（7）Bake sizing：Baking temperature is 165 DEG C, bakes the time for 120s；
（8）Dynamic cooling：It it is 17 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 65% constant temperature
In constant humidity sealing cooling room, 10min is cooled down；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled 55%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90 DEG C,
The Drying and cooling time is 15min.
The Testing index and standard GB/T/T 18863- of shirt its ironing-free performance that the production of case study on implementation 4 is completed
2002《Non-ironing textile》Comparing result and according to AATCC 79 test washing before and after water absorbing properties it is as shown in table 1.
The case study on implementation properties of product test index of table 1 and national standard contrast table
| Test event | National standard | Case study on implementation 1 | Case study on implementation 2 | Case study on implementation 3 | Case study on implementation 4 |
| Flat appearance degree | 3.5 | 4 | 4 | 4 | 4 |
| Seam outward appearance | 3 | 4 | 4 | 4 | 4 |
| Rivel outward appearance | 3 | 4 | 4 | 4 | 4 |
| Content of formaldehyde | ≤75 | Do not detect | Do not detect | Do not detect | Do not detect |
| Water absorption before washing | - | 8 | 7 | 6 | 6 |
| Water absorption after 50 washings | - | 24 | 22 | 18 | 15 |
Claims (3)
1. the waterproof and oilproof anti-fouling type noniron finish liquid of a kind of shirt, it is characterised in that system is prepared by the raw material of following weight portion
Into：Butane tetracid 24-26, Fructus Citri Limoniae acid amide 16-18, triethanolamine 2.5-2.7, malic acid 0.9-1.2, sodium hypophosphite 0.8-1, boron
Sour 0.27-0.3, the semi-annular jade pendant acid derivative 2-2.5 of stilbene two, Tissuemat E 1.3-1.6, magnesium chloride 0.4-0.5, double amino are organic
Silicon emulsion 2-3, shitosan 4.5-5, DMF 68-80, titanium dioxide 1.2-1.4, the 0.25- of polypropylene glycol 200
0.4th, propyl-triethoxysilicane 0.6-0.8, tetraethoxysilane 0.3-0.5, sodium polyphosphate 0.3-0.4, Ludox 3.2-
3.5th, concentrated hydrochloric acid 1.2-1.4, alkylolamideses polyoxyethylene ether 0.35-0.5, appropriate maleic anhydride, appropriate dehydrated alcohol, go from
Sub- appropriate amount of water.
2. the waterproof and oilproof anti-fouling type noniron finish liquid of a kind of shirt according to claim 1, it is characterised in that by following tool
Body step is made：
（1）Titanium dioxide granule is added in the 15-18 times of dehydrated alcohol measured, the ethoxy of propyl group three is added after magnetic agitation 30min
Base silane and tetraethoxysilane, in system with the speed Deca concentrated hydrochloric acid of 5 seconds one drops after 30min, stir 48h, Ran Houjia
Enter sodium polyphosphate high shear agitation 10-20min, stirring adds Ludox to continue stirring 1-1.5h and obtains modified silicon after terminating
Colloidal sol is standby；
（2）By shitosan and maleic anhydride according to mass ratio 1：1.8 ratio mixing is added in DMF, in water
Stirring reaction 7-9h at 100-120 DEG C of bath temperature, reaction is washed with deionized standby in neutral post-drying after terminating；Then will
Standby solidss and deionized water mixing are placed in the container with agitating device, are stirred and are added step to after being completely dissolved
（1）The product and alkylolamideses polyoxyethylene ether of preparation, regulation system pH value is standby to 7-8 after stirring；
（3）Remaining remaining raw material is added in deionized water, is 1 according to total raw material and deionized water quality ratio：1.5 mixing are stirred
Mix uniform, add step（2）The product mixing and stirring of preparation obtains final product dressing liquid.
3. a kind of noniron finish method of shirt ready-made clothes, it is characterised in that be made up of step in detail below：
（1）Fabric is preferred：Preferred stripe is dry uniform, and the consistent long-staple cotton of length is weaved using compact spinning technique, and uses liquefied ammonia
+ mercerising technology carries out Final finishing to the fabric knitted, and obtains bright color, comfortable feel, is strongly worth high high quality fabric；
（2）Three-dimensional cutting：Using the three-dimensional cutting technology for meeting ergonomic, fabric is cut into into separate panels；
（3）Filler rod：With filler rod technology, hot melt adhesive tape or lining cloth are sewed at suture, then through pressing work
Skill carries out high temperature pressing to it, and acquisition suture puts down semi-finished product very；
（4）Dressing liquid process：Dressing liquid is completed by the way of piecewise operation in reative cell to absorb, leading portion is placed using suspension
Mode takes shirt hanger in self-propagating circulation, working solution is attached on ready-made clothes by way of aerosol,
Simultaneously the dressing liquid for descending slowly and lightly is collected by blood circulation and recycled；Back segment is depth absorption chamber, makes ready-made clothes fabric fine
Dimension liquid carrying rate is controlled in 50-90%；
（5）Preliminary drying damping：Using infrared three-dimensional drying technology, the shirt for hanging placement is carried out into preliminary drying damping, preliminary drying temperature 80-
105 DEG C, preliminary drying time 80-110s, overall humidity is controlled in 20-45%；
（6）Pressing is moulding：Using three-dimensional high temperature pressing machine, independent pressing is carried out to shirt difference body piece, pressing temperature is 140-
160 DEG C, pressing pressure is 3-13kg/cm2, pressing time 12-30s；
（7）Bake sizing：Baking temperature is 165-185 DEG C, bakes the time for 30-120s；
（8）Dynamic cooling：It it is 17-20 DEG C in temperature using three-dimensional suspension, self-propagating dynamical fashion, humidity is 60-65%
Constant temperature and humidity sealing cooling room in, cool down 10-30min；
（9）Feel is adjusted：The technology sprayed using atomization carries out feel regulation to the shirt after cooling, and liquid carrying rate is controlled in 55-
80%；
（10）Drying is cooled down：The shirt after feel regulation will be carried out carries out rolling type baking oven drying, and drying temperature is set in 90-
105 DEG C, the Drying and cooling time is 15-30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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| CN106758155A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758202A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The shrinkproof hydroscopic fast-drying type noniron finish liquid and its method for sorting of a kind of shirt |
| CN106758200A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt |
| CN107724073A (en) * | 2017-09-28 | 2018-02-23 | 江苏新瑞贝科技股份有限公司 | A kind of fabric finishing agent and preparation method thereof |
| CN107780200A (en) * | 2017-09-28 | 2018-03-09 | 江苏新瑞贝科技股份有限公司 | A kind of wash and wear finisher and preparation method thereof |
| CN107794751A (en) * | 2017-09-27 | 2018-03-13 | 江苏新瑞贝科技股份有限公司 | A kind of anti-crease and Iron-free agent and preparation method thereof |
| CN108893980A (en) * | 2018-07-13 | 2018-11-27 | 温州东廷服饰有限公司 | A kind of shirt environmental protection ironing-free technology |
| CN111877017A (en) * | 2020-07-10 | 2020-11-03 | 温州厚德服饰有限公司 | Waterproof cotton-padded clothes |
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| CN106758155A (en) * | 2016-12-21 | 2017-05-31 | 阜阳市豹子头服饰科技有限公司 | The fire-retardant vapor-permeable type noniron finish liquid and its method for sorting of a kind of shirt |
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| CN111877017A (en) * | 2020-07-10 | 2020-11-03 | 温州厚德服饰有限公司 | Waterproof cotton-padded clothes |
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