DK0840757T3 - Fremgangsmåde til fremstilling af polyoxytetramethylenglycol - Google Patents
Fremgangsmåde til fremstilling af polyoxytetramethylenglycolInfo
- Publication number
- DK0840757T3 DK0840757T3 DK96927609T DK96927609T DK0840757T3 DK 0840757 T3 DK0840757 T3 DK 0840757T3 DK 96927609 T DK96927609 T DK 96927609T DK 96927609 T DK96927609 T DK 96927609T DK 0840757 T3 DK0840757 T3 DK 0840757T3
- Authority
- DK
- Denmark
- Prior art keywords
- pct
- polyoxytetramethylene glycol
- preparing
- catalyst
- yne
- Prior art date
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 4
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title abstract 2
- -1 polyoxytetramethylene Polymers 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 4
- 239000003054 catalyst Substances 0.000 abstract 3
- DLDJFQGPPSQZKI-UHFFFAOYSA-N but-2-yne-1,4-diol Chemical compound OCC#CCO DLDJFQGPPSQZKI-UHFFFAOYSA-N 0.000 abstract 2
- 229920001577 copolymer Polymers 0.000 abstract 2
- 238000006116 polymerization reaction Methods 0.000 abstract 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/16—Cyclic ethers having four or more ring atoms
- C08G65/20—Tetrahydrofuran
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4854—Polyethers containing oxyalkylene groups having four carbon atoms in the alkylene group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/6795—Unsaturated polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/08—Saturated oxiranes
- C08G65/10—Saturated oxiranes characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2654—Aluminium or boron; Compounds thereof
- C08G65/2657—Aluminosilicates; Clays; Zeolites
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2666—Hetero polyacids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/269—Mixed catalyst systems, i.e. containing more than one reactive component or catalysts formed in-situ
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/40—Polyamides containing oxygen in the form of ether groups
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyethers (AREA)
- Catalysts (AREA)
- Polyesters Or Polycarbonates (AREA)
- Cephalosporin Compounds (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Polyamides (AREA)
- Polyurethanes Or Polyureas (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19527532A DE19527532A1 (de) | 1995-07-27 | 1995-07-27 | Verfahren zur Herstellung von Polyoxytetramethylenglycol |
| PCT/EP1996/003297 WO1997005188A1 (de) | 1995-07-27 | 1996-07-26 | Verfahren zur herstellung von polyoxytetramethylenglycol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0840757T3 true DK0840757T3 (da) | 2000-03-27 |
Family
ID=7767969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK96927609T DK0840757T3 (da) | 1995-07-27 | 1996-07-26 | Fremgangsmåde til fremstilling af polyoxytetramethylenglycol |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US6043338A (cs) |
| EP (1) | EP0840757B1 (cs) |
| JP (1) | JPH11510529A (cs) |
| KR (1) | KR19990035978A (cs) |
| CN (1) | CN1087314C (cs) |
| AT (1) | ATE187184T1 (cs) |
| CA (1) | CA2224294A1 (cs) |
| CZ (3) | CZ288130B6 (cs) |
| DE (2) | DE19527532A1 (cs) |
| DK (1) | DK0840757T3 (cs) |
| ES (1) | ES2141525T3 (cs) |
| GR (1) | GR3032679T3 (cs) |
| MX (1) | MX9800716A (cs) |
| PT (1) | PT840757E (cs) |
| SK (1) | SK282367B6 (cs) |
| TW (1) | TW341581B (cs) |
| WO (1) | WO1997005188A1 (cs) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19641481A1 (de) * | 1996-10-09 | 1998-04-16 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
| DE19719875A1 (de) * | 1997-05-12 | 1998-11-19 | Basf Ag | Verfahren zur Polymerisation cyclischer Ether |
| KR20020040208A (ko) * | 2000-11-24 | 2002-05-30 | 조 정 래 | 폴리옥시테트라메틸렌글리콜의 제조방법 |
| DE10245198A1 (de) | 2002-09-27 | 2004-04-01 | Basf Ag | Katalysator, Verfahren zu dessen Herstellung und Verfahren zur Polymerisation cyclischer Ether an diesem Katalysator |
| DE10261484A1 (de) * | 2002-12-23 | 2004-07-01 | Basf Ag | Verfahren zur Polymerisation cyclischer Ether |
| KR101111129B1 (ko) * | 2007-03-27 | 2012-03-13 | 디아이씨 가부시끼가이샤 | 폴리에스테르 제조용 고체산 촉매, 그 제조 방법 및 그것을 사용하는 폴리에스테르의 제조 방법 |
| CN103755944B (zh) * | 2014-01-10 | 2015-12-02 | 大连工业大学 | 复合金属氧化物修饰二氧化钛型固体酸的制备方法及其催化聚四氢呋喃醚的合成方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2499725A (en) * | 1948-02-06 | 1950-03-07 | Du Pont | Process for making esters of monocarboxylic acids |
| US3358042A (en) * | 1963-09-20 | 1967-12-12 | Quaker Oats Co | Process for recovering polytetramethylene ether glycol |
| US4163115A (en) * | 1976-03-31 | 1979-07-31 | E. I. Du Pont De Nemours And Company | Preparation of esters of poly-(tetramethylene ether) glycol |
| DE2760272C2 (de) * | 1976-03-31 | 1987-04-16 | E.I. Du Pont De Nemours And Co., Wilmington, Del. | Verfahren zur Herstellung von Poly-(tetramethylenether)-glykol durch Alkoholyse eines Ester-Endgruppen aufweisenden Poly-(tetramethylenether)-glykols |
| US4120903A (en) * | 1977-03-30 | 1978-10-17 | E. I. Du Pont De Nemours And Company | Method for preparing poly(tetramethylene ether) glycol |
| US4243799A (en) * | 1978-01-14 | 1981-01-06 | Basf Aktiengesellschaft | Polymerization of tetrahydrofuran |
| US4189566A (en) * | 1978-01-14 | 1980-02-19 | Basf Aktiengesellschaft | Polymerization of tetrahydrofuran |
| US4303782A (en) * | 1980-01-21 | 1981-12-01 | Mobil Oil Corporation | Polymerization of cyclic ethers |
| JPS5883028A (ja) * | 1981-11-10 | 1983-05-18 | Daicel Chem Ind Ltd | ポリテトラメチレングリコ−ルの製造方法 |
| CA1216597A (en) * | 1983-05-23 | 1987-01-13 | Atsushi Aoshima | Process for producing polyetherglycol |
| US4658065A (en) * | 1984-03-28 | 1987-04-14 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for producing polyether polyol and a product |
| US5149862A (en) * | 1991-02-26 | 1992-09-22 | E. I. Du Pont De Nemours And Company | Preparation of polytetramethylene ether glycol using an acidic zirconia catalyst |
| DE4316138A1 (de) * | 1993-05-14 | 1994-11-17 | Basf Ag | Verfahren zur Herstellung von Polytetrahydrofuran |
| DE19507399A1 (de) * | 1995-03-03 | 1996-09-05 | Basf Ag | C-C-Dreifachbindungen enthaltende Tetrahydrofuran/But-2-in-1,4-diol-Copolymere |
-
1995
- 1995-07-27 DE DE19527532A patent/DE19527532A1/de not_active Withdrawn
-
1996
- 1996-07-26 DE DE59603792T patent/DE59603792D1/de not_active Expired - Lifetime
- 1996-07-26 US US09/000,053 patent/US6043338A/en not_active Expired - Fee Related
- 1996-07-26 CN CN96196731A patent/CN1087314C/zh not_active Expired - Fee Related
- 1996-07-26 EP EP96927609A patent/EP0840757B1/de not_active Expired - Lifetime
- 1996-07-26 WO PCT/EP1996/003297 patent/WO1997005188A1/de not_active Ceased
- 1996-07-26 PT PT96927609T patent/PT840757E/pt unknown
- 1996-07-26 SK SK106-98A patent/SK282367B6/sk unknown
- 1996-07-26 TW TW085109159A patent/TW341581B/zh active
- 1996-07-26 CA CA002224294A patent/CA2224294A1/en not_active Abandoned
- 1996-07-26 KR KR1019980700639A patent/KR19990035978A/ko not_active Ceased
- 1996-07-26 MX MX9800716A patent/MX9800716A/es not_active IP Right Cessation
- 1996-07-26 JP JP9507230A patent/JPH11510529A/ja active Pending
- 1996-07-26 AT AT96927609T patent/ATE187184T1/de active
- 1996-07-26 ES ES96927609T patent/ES2141525T3/es not_active Expired - Lifetime
- 1996-07-26 CZ CZ1998244A patent/CZ288130B6/cs not_active IP Right Cessation
- 1996-07-26 DK DK96927609T patent/DK0840757T3/da active
-
2000
- 2000-02-16 GR GR20000400377T patent/GR3032679T3/el unknown
- 2000-08-03 CZ CZ20002851A patent/CZ288206B6/cs not_active IP Right Cessation
- 2000-08-03 CZ CZ20002850A patent/CZ288205B6/cs not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| US6043338A (en) | 2000-03-28 |
| EP0840757A1 (de) | 1998-05-13 |
| DE19527532A1 (de) | 1997-01-30 |
| ES2141525T3 (es) | 2000-03-16 |
| CZ288130B6 (cs) | 2001-04-11 |
| SK10698A3 (en) | 1998-11-04 |
| GR3032679T3 (en) | 2000-06-30 |
| EP0840757B1 (de) | 1999-12-01 |
| CA2224294A1 (en) | 1997-02-13 |
| ATE187184T1 (de) | 1999-12-15 |
| TW341581B (en) | 1998-10-01 |
| DE59603792D1 (de) | 2000-01-05 |
| PT840757E (pt) | 2000-05-31 |
| CN1195358A (zh) | 1998-10-07 |
| CN1087314C (zh) | 2002-07-10 |
| SK282367B6 (sk) | 2002-01-07 |
| WO1997005188A1 (de) | 1997-02-13 |
| CZ24498A3 (cs) | 1998-07-15 |
| KR19990035978A (ko) | 1999-05-25 |
| JPH11510529A (ja) | 1999-09-14 |
| CZ288205B6 (en) | 2001-05-16 |
| CZ288206B6 (en) | 2001-05-16 |
| MX9800716A (es) | 1998-04-30 |
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