DK0970092T3 - Fremgangsmåde til at rense tetraethoxysilan - Google Patents
Fremgangsmåde til at rense tetraethoxysilanInfo
- Publication number
- DK0970092T3 DK0970092T3 DK96940369T DK96940369T DK0970092T3 DK 0970092 T3 DK0970092 T3 DK 0970092T3 DK 96940369 T DK96940369 T DK 96940369T DK 96940369 T DK96940369 T DK 96940369T DK 0970092 T3 DK0970092 T3 DK 0970092T3
- Authority
- DK
- Denmark
- Prior art keywords
- tetraethoxysilane
- pure
- purifying
- purified
- column
- Prior art date
Links
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 title abstract 4
- 239000000463 material Substances 0.000 abstract 3
- 238000009835 boiling Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/04—Esters of silicic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Separation Of Gases By Adsorption (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/558,682 US5840953A (en) | 1995-11-16 | 1995-11-16 | Purified tetraethoxysilane and method of purifying |
| PCT/US1996/018067 WO1997018219A1 (en) | 1995-11-16 | 1996-11-14 | Purified tetraethoxysilane and method of purifying |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK0970092T3 true DK0970092T3 (da) | 2002-09-02 |
Family
ID=24230519
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK96940369T DK0970092T3 (da) | 1995-11-16 | 1996-11-14 | Fremgangsmåde til at rense tetraethoxysilan |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US5840953A (da) |
| EP (1) | EP0970092B1 (da) |
| JP (1) | JP2000500457A (da) |
| AT (1) | ATE221891T1 (da) |
| AU (1) | AU7726696A (da) |
| DE (1) | DE69622893T2 (da) |
| DK (1) | DK0970092T3 (da) |
| ES (1) | ES2176517T3 (da) |
| WO (1) | WO1997018219A1 (da) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6660875B1 (en) | 1998-06-09 | 2003-12-09 | Ppt Technologies, Llc | Ion exchange purification of dielectric condensate precursor fluids and silicate esters such as tetraethylorthosilicate (TEOS) |
| JP4288130B2 (ja) * | 2003-09-30 | 2009-07-01 | 東京エレクトロン株式会社 | 電気的接合部材及びプラズマ処理装置 |
| DE102004025766A1 (de) * | 2004-05-26 | 2005-12-22 | Degussa Ag | Herstellung von Organosilanestern |
| JP4212106B2 (ja) * | 2005-04-19 | 2009-01-21 | オルガノ株式会社 | ガス分離装置及びガス分離方法 |
| WO2012021596A1 (en) | 2010-08-10 | 2012-02-16 | Idex Health & Science Llc | Biocompatible tubing for liquid chromatography systems |
| CN103772424B (zh) * | 2013-12-31 | 2016-01-27 | 贵州威顿晶磷电子材料股份有限公司 | 一种电子级正硅酸四乙酯的制备方法 |
| US20170023235A1 (en) * | 2015-07-21 | 2017-01-26 | Apple Inc. | Sublimator/vaporizer |
| EP3894044B1 (en) * | 2018-11-29 | 2025-09-24 | Fluitec N.V. | Filter housings, purification skids and methods of use thereof |
| CN109459539B (zh) * | 2018-12-29 | 2024-03-22 | 金宏气体股份有限公司 | 一种高纯正硅酸乙酯中微量水分的检测方法及检测系统 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB802339A (en) * | 1955-05-17 | 1958-10-01 | Union Carbide Corp | Preparation of orthosilicates |
| US3041141A (en) * | 1955-09-06 | 1962-06-26 | Baker Chem Co J T | Process of purifying silane |
| US3002583A (en) * | 1957-06-10 | 1961-10-03 | Phillips Petroleum Co | Fluid separation by gas chromatography |
| US2972626A (en) * | 1958-01-15 | 1961-02-21 | Monsanto Chemicals | Purification of organo-silicate condensation products |
| US3019087A (en) * | 1958-09-29 | 1962-01-30 | Merck & Co Inc | Purification of silane |
| US3118947A (en) * | 1960-06-22 | 1964-01-21 | Exxon Research Engineering Co | Epoxide conversion process |
| US3267646A (en) * | 1963-03-04 | 1966-08-23 | Hewlett Packard Co | Automatic preparative gas chromatograph |
| JPS5315477B2 (da) * | 1972-09-30 | 1978-05-25 | ||
| US4003257A (en) * | 1974-03-12 | 1977-01-18 | Nasa | Analysis of volatile organic compounds |
| US4070444A (en) * | 1976-07-21 | 1978-01-24 | Motorola Inc. | Low cost, high volume silicon purification process |
| US4159966A (en) * | 1977-12-27 | 1979-07-03 | The Dow Chemical Company | Chromatographic column packing |
| US4537759A (en) * | 1981-08-24 | 1985-08-27 | Eagle-Picher Industries, Inc. | Production of elemental silicon from impure silane feed |
| JPS5930711A (ja) * | 1982-08-12 | 1984-02-18 | Showa Denko Kk | モノシランの精製法 |
| US4447632A (en) * | 1983-04-18 | 1984-05-08 | Union Carbide Corporation | Process for production of alkyl silicates from silicon metal |
| US4532120A (en) * | 1983-12-28 | 1985-07-30 | Ethyl Corporation | Silane purification process |
| US4772296A (en) * | 1987-05-12 | 1988-09-20 | Eagle-Picher Industries, Inc. | Method of purifying and depositing group IIIa and group Va compounds to produce epitaxial films |
| US5069690A (en) * | 1991-02-21 | 1991-12-03 | Air Products And Chemicals, Inc. | Process for kinetic gas-solid chromatographic separations |
| DE4130643A1 (de) * | 1991-09-14 | 1993-03-18 | Degussa | Verfahren zur reinigung von alkoxysilanen |
| JPH0586069A (ja) * | 1991-09-26 | 1993-04-06 | Asahi Denka Kogyo Kk | 有機珪素化合物の精製法 |
-
1995
- 1995-11-16 US US08/558,682 patent/US5840953A/en not_active Expired - Lifetime
-
1996
- 1996-11-14 DE DE69622893T patent/DE69622893T2/de not_active Expired - Fee Related
- 1996-11-14 EP EP96940369A patent/EP0970092B1/en not_active Expired - Lifetime
- 1996-11-14 AT AT96940369T patent/ATE221891T1/de not_active IP Right Cessation
- 1996-11-14 AU AU77266/96A patent/AU7726696A/en not_active Abandoned
- 1996-11-14 DK DK96940369T patent/DK0970092T3/da active
- 1996-11-14 JP JP9518981A patent/JP2000500457A/ja not_active Ceased
- 1996-11-14 ES ES96940369T patent/ES2176517T3/es not_active Expired - Lifetime
- 1996-11-14 WO PCT/US1996/018067 patent/WO1997018219A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JP2000500457A (ja) | 2000-01-18 |
| WO1997018219A1 (en) | 1997-05-22 |
| DE69622893T2 (de) | 2002-12-12 |
| EP0970092B1 (en) | 2002-08-07 |
| AU7726696A (en) | 1997-06-05 |
| DE69622893D1 (de) | 2002-09-12 |
| US5840953A (en) | 1998-11-24 |
| ES2176517T3 (es) | 2002-12-01 |
| ATE221891T1 (de) | 2002-08-15 |
| EP0970092A1 (en) | 2000-01-12 |
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