DK2204372T3 - Fremgangsmåde til fremstilling af thiophosphorsyretriamider ved hjælp af upolære aminer - Google Patents

Fremgangsmåde til fremstilling af thiophosphorsyretriamider ved hjælp af upolære aminer

Info

Publication number: DK2204372T3
Authority: DK; Denmark
Prior art keywords: end product; auxiliary base; acid; polar; base
Prior art date: 2005-11-08

Application number

DK10156176.9T

Other languages

English (en)

Inventor

Wolfgang Koernig

Oliver Huttenloch

Patrick Deck

Holger Ganz

Michael Bock

Michael Maua

Original Assignee

Basf Se

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2005-11-08

Filing date

2006-09-15

Publication date

2012-05-07

2006-09-15 Application filed by Basf Se filed Critical Basf Se

2012-05-07 Application granted granted Critical

2012-05-07 Publication of DK2204372T3 publication Critical patent/DK2204372T3/da

Links

150000001412 amines Chemical class 0.000 title 1
239000007795 chemical reaction product Substances 0.000 abstract 9
239000002253 acid Substances 0.000 abstract 6
239000002798 polar solvent Substances 0.000 abstract 4
150000003839 salts Chemical class 0.000 abstract 4
DBAKFASWICGISY-DASCVMRKSA-N Dexchlorpheniramine maleate Chemical compound OC(=O)\C=C/C(O)=O.C1([C@H](CCN(C)C)C=2N=CC=CC=2)=CC=C(Cl)C=C1 DBAKFASWICGISY-DASCVMRKSA-N 0.000 abstract 2
RYYWUUFWQRZTIU-UHFFFAOYSA-N Thiophosphoric acid Chemical compound OP(O)(S)=O RYYWUUFWQRZTIU-UHFFFAOYSA-N 0.000 abstract 2
150000007513 acids Chemical class 0.000 abstract 2
239000007791 liquid phase Substances 0.000 abstract 2
239000011541 reaction mixture Substances 0.000 abstract 2
238000000926 separation method Methods 0.000 abstract 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
239000012736 aqueous medium Substances 0.000 abstract 1
125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
- C07F9/224—Phosphorus triamides
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
Molecular Biology (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Fertilizers (AREA)

DK10156176.9T 2005-11-08 2006-09-15 Fremgangsmåde til fremstilling af thiophosphorsyretriamider ved hjælp af upolære aminer DK2204372T3 (da)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE102005053540A DE102005053540A1 (de)	2005-11-08	2005-11-08	Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe unpolarer Amine
EP06793548A EP1948670B1 (de)	2005-11-08	2006-09-15	Verfahren zur abtrennung von säuren aus chemischen reaktionsgemischen mit hilfe unpolarer tertiärer amine

Publications (1)

Publication Number	Publication Date
DK2204372T3 true DK2204372T3 (da)	2012-05-07

Family

ID=37596190

Family Applications (2)

Application Number	Title	Priority Date	Filing Date
DK06793548.6T DK1948670T3 (da)	2005-11-08	2006-09-15	Fremgangsmåde til adskillelse af syrer fra kemiske reaktionsblandinger ved hjælp af upolære tertiære aminer
DK10156176.9T DK2204372T3 (da)	2005-11-08	2006-09-15	Fremgangsmåde til fremstilling af thiophosphorsyretriamider ved hjælp af upolære aminer

Family Applications Before (1)

Application Number	Title	Priority Date	Filing Date
DK06793548.6T DK1948670T3 (da)	2005-11-08	2006-09-15	Fremgangsmåde til adskillelse af syrer fra kemiske reaktionsblandinger ved hjælp af upolære tertiære aminer

Country Status (18)

Country	Link
US (2)	US9359269B2 (da)
EP (2)	EP1948670B1 (da)
CN (1)	CN101305015A (da)
AT (2)	ATE489393T1 (da)
AU (1)	AU2006311130B2 (da)
BR (1)	BRPI0618331B1 (da)
CA (1)	CA2628503C (da)
DE (2)	DE102005053540A1 (da)
DK (2)	DK1948670T3 (da)
ES (2)	ES2355941T3 (da)
MX (2)	MX295383B (da)
NO (1)	NO20081962L (da)
NZ (1)	NZ567995A (da)
PL (2)	PL1948670T3 (da)
PT (2)	PT2204372E (da)
RU (1)	RU2417229C9 (da)
UA (1)	UA90188C2 (da)
WO (1)	WO2007054392A1 (da)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE102007062614C5 (de) *	2007-12-22	2019-03-14	Eurochem Agro Gmbh	Mischung zur Behandlung von harnstoffhaltigen Düngemitteln, Verwendungen der Mischung und harnstoffhaltiges Düngemittel enthaltend die Mischung
EP2107064A1 (de) *	2008-04-02	2009-10-07	Basf Se	Verfahren zur Herstellung von Triamiden aus Ammoniak und Amido-Dichloriden
CZ302400B6 (cs)	2008-10-20	2011-05-04	Agra Group, A.S.	Zpusob prípravy N-(hydrokarbyl)triamidu kyseliny fosforecné nebo thiofosforecné
CN102746333B (zh) *	2012-06-12	2015-04-01	上虞盛晖化工股份有限公司	一种n-正丁基硫代磷酰三胺的合成方法
HUE028532T2 (en)	2012-07-18	2016-12-28	Saltigo Gmbh	Process for the preparation of asymmetric (thio) phosphoric triamides
CN104640826A (zh)	2012-08-15	2015-05-20	科氏农艺服务有限责任公司	含有脲酶抑制剂和二醇烷基醚的改善的液体组合物及其制造和使用方法
CA2881711A1 (en)	2012-08-15	2014-02-20	Koch Agronomic Services, Llc	Liquid compositions containing urease inhibitors and aryl alkyl alcohols
US8888886B1 (en)	2013-08-06	2014-11-18	Garnett B Whitehurst	NBPT solutions for preparing urease inhibited urea fertilizers prepared from N-substituted morpholines
EP3212592A1 (en)	2014-10-31	2017-09-06	Koch Agronomic Services, LLC	Nitrification inhibitor compositions and methods of making thereof
EP3763692B1 (en)	2014-12-23	2024-10-02	Basf Se	Compositions with improved urease-inhibiting effect comprising (thio) phosphoric acid triamide and further compounds such as amines and colorants
HUE061477T2 (hu)	2015-10-01	2023-07-28	Basf Se	Eljárás (tio)foszforsav-származékot tartalmazó elegy kinyerésére
BR112018009985B8 (pt)	2015-12-01	2021-04-06	Basf Se	processo para o isolamento de um derivado de ácido
CN112402998B (zh) *	2020-12-11	2022-06-14	安徽标王农牧股份有限公司	一种适用于氨基酸的分级提取装置
AU2022238316B2 (en)	2021-03-15	2025-05-08	Gary David Mcknight	Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions
US12098109B2 (en)	2021-03-15	2024-09-24	Soilgenic Technologies, Llc	Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions
CN113860943B (zh) *	2021-09-24	2022-11-25	中船(邯郸)派瑞特种气体股份有限公司	一种对三氟甲磺酸制备中釜残的综合处理方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
BE791311A (fr)	1971-11-16	1973-05-14	Wacker Chemie Gmbh	Procede pour isoler le chlorure du bis-(dimethylamide) de l'acide phosphorique ou le tris-(dimethylamide) de l'acide phosphorique de leurs solutions impures
DD100475A1 (da) *	1972-01-31	1973-09-20
US4530714A (en) *	1983-03-16	1985-07-23	Allied Corporation	N-aliphatic and N,N-aliphatic phosphoric triamide urease inhibitors and urease inhibited urea based fertilizer compositions
CH678054A5 (de)	1989-07-17	1991-07-31	Enco Eng Ag	Verfahren zur herstellung von tertiaeren amin-schwefel-trioxid-komplexen.
US5770771A (en) *	1997-01-21	1998-06-23	Albemarle Corporation	Preparation of N-hydrocarbylthiophosphoric triamides
AR038161A1 (es)	2002-01-24	2004-12-29	Basf Ag	Procedimiento para separar acidos de mezclas de reaccion quimicas con la ayuda de liquidos ionicos
DE10360397A1 (de)	2003-12-19	2005-07-14	Basf Ag	Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von 1-Alkylimidazolen

2005
- 2005-11-08 DE DE102005053540A patent/DE102005053540A1/de not_active Withdrawn
2006
- 2006-09-15 NZ NZ567995A patent/NZ567995A/en not_active IP Right Cessation
- 2006-09-15 PL PL06793548T patent/PL1948670T3/pl unknown
- 2006-09-15 PT PT10156176T patent/PT2204372E/pt unknown
- 2006-09-15 RU RU2008122537/04A patent/RU2417229C9/ru active
- 2006-09-15 US US12/092,392 patent/US9359269B2/en active Active
- 2006-09-15 BR BRPI0618331A patent/BRPI0618331B1/pt not_active IP Right Cessation
- 2006-09-15 ES ES06793548T patent/ES2355941T3/es active Active
- 2006-09-15 DE DE502006008403T patent/DE502006008403D1/de active Active
- 2006-09-15 AT AT06793548T patent/ATE489393T1/de active
- 2006-09-15 CN CNA2006800417865A patent/CN101305015A/zh active Pending
- 2006-09-15 CA CA2628503A patent/CA2628503C/en active Active
- 2006-09-15 DK DK06793548.6T patent/DK1948670T3/da active
- 2006-09-15 AU AU2006311130A patent/AU2006311130B2/en not_active Ceased
- 2006-09-15 EP EP06793548A patent/EP1948670B1/de active Active
- 2006-09-15 PL PL10156176T patent/PL2204372T3/pl unknown
- 2006-09-15 PT PT06793548T patent/PT1948670E/pt unknown
- 2006-09-15 AT AT10156176T patent/ATE540045T1/de active
- 2006-09-15 UA UAA200807757A patent/UA90188C2/ru unknown
- 2006-09-15 DK DK10156176.9T patent/DK2204372T3/da active
- 2006-09-15 WO PCT/EP2006/066397 patent/WO2007054392A1/de not_active Ceased
- 2006-09-15 ES ES10156176T patent/ES2378344T3/es active Active
- 2006-09-15 EP EP10156176A patent/EP2204372B1/de active Active
2008
- 2008-04-25 NO NO20081962A patent/NO20081962L/no not_active Application Discontinuation
- 2008-05-02 MX MX2011000779A patent/MX295383B/es unknown
- 2008-05-02 MX MX2008005701A patent/MX285596B/es active IP Right Grant
2016
- 2016-05-06 US US15/148,430 patent/US9493491B2/en active Active

Also Published As

Publication number	Publication date
NZ567995A (en)	2010-04-30
US9359269B2 (en)	2016-06-07
NO20081962L (no)	2008-08-06
CA2628503A1 (en)	2007-05-18
EP2204372A1 (de)	2010-07-07
PT1948670E (pt)	2010-12-23
US9493491B2 (en)	2016-11-15
ES2378344T3 (es)	2012-04-11
EP1948670A1 (de)	2008-07-30
MX295383B (en)	2012-01-31
BRPI0618331B1 (pt)	2016-09-13
DE502006008403D1 (de)	2011-01-05
UA90188C2 (ru)	2010-04-12
EP2204372B1 (de)	2012-01-04
PL2204372T3 (pl)	2012-05-31
RU2417229C9 (ru)	2012-05-10
ATE489393T1 (de)	2010-12-15
ES2355941T3 (es)	2011-04-01
MX285596B (en)	2011-04-12
WO2007054392A1 (de)	2007-05-18
CA2628503C (en)	2013-08-06
AU2006311130B2 (en)	2012-04-05
BRPI0618331A2 (pt)	2012-05-08
PL1948670T3 (pl)	2011-05-31
RU2008122537A (ru)	2009-12-20
DE102005053540A1 (de)	2007-05-10
US20080287709A1 (en)	2008-11-20
RU2417229C2 (ru)	2011-04-27
DK1948670T3 (da)	2011-02-28
PT2204372E (pt)	2012-02-09
EP1948670B1 (de)	2010-11-24
AU2006311130A1 (en)	2007-05-18
CN101305015A (zh)	2008-11-12
ATE540045T1 (de)	2012-01-15
US20160251384A1 (en)	2016-09-01

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