NO20081962L - Fremgangsmate for a separere syrer fra kjemiske reaksjonsblandinger ved hjelp av apolare aminer - Google Patents
Fremgangsmate for a separere syrer fra kjemiske reaksjonsblandinger ved hjelp av apolare aminerInfo
- Publication number
- NO20081962L NO20081962L NO20081962A NO20081962A NO20081962L NO 20081962 L NO20081962 L NO 20081962L NO 20081962 A NO20081962 A NO 20081962A NO 20081962 A NO20081962 A NO 20081962A NO 20081962 L NO20081962 L NO 20081962L
- Authority
- NO
- Norway
- Prior art keywords
- end product
- auxiliary base
- acid
- polar
- base
- Prior art date
Links
- 239000002253 acid Substances 0.000 title abstract 7
- 150000007513 acids Chemical class 0.000 title abstract 3
- 239000011541 reaction mixture Substances 0.000 title abstract 3
- 150000001412 amines Chemical class 0.000 title 1
- 238000006243 chemical reaction Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 239000007795 chemical reaction product Substances 0.000 abstract 9
- 239000002798 polar solvent Substances 0.000 abstract 4
- 150000003839 salts Chemical class 0.000 abstract 4
- DBAKFASWICGISY-DASCVMRKSA-N Dexchlorpheniramine maleate Chemical compound OC(=O)\C=C/C(O)=O.C1([C@H](CCN(C)C)C=2N=CC=CC=2)=CC=C(Cl)C=C1 DBAKFASWICGISY-DASCVMRKSA-N 0.000 abstract 2
- RYYWUUFWQRZTIU-UHFFFAOYSA-N Thiophosphoric acid Chemical compound OP(O)(S)=O RYYWUUFWQRZTIU-UHFFFAOYSA-N 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000012736 aqueous medium Substances 0.000 abstract 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 abstract 1
- 125000000467 secondary amino group Chemical class [H]N([*:1])[*:2] 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
- C07F9/224—Phosphorus triamides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fertilizers (AREA)
Abstract
Oppfinnelsen omhandler en fremgangsmåte for fjerning av syrer fra reaksjonsblandinger, som omfatter minst ett verdifullt produkt som er lite løselig i vann, ved hjelp av minst ett upolart amin som hjelpebase, som omfatter de følgende trinn: a) reaksjon av hjelpebasen med syren med dannelse av et salt; b) reaksjon av saltet dannet i trinn a) med en ytterligere base, som overtar syren med frigivelse av hjelpebasen; c) ekstraksjon av blandingen oppnådd i trinn b) med vann eller et vandig medium, hvor saltet av den ytterligere base løses opp i den vandige fasen og det verdifulle produkt eller løsningen av det verdifulle produkt, i et egnet løsemiddel og hjelpebasen danner minst én separat ikke-vandig fase; og d) destillativ fjerning av hjelpebasen og/eller minst noe av løsemidlet som eventuelt er til stede fra den minst ene ikke-vandige fase oppnådd i trinn c), det er mulig at det dannes to ikke-blandbare flytende faser. Oppfinnelsen omhandler dessuten en fremgangsmåte for fremstilling av tiofosforsyretriamider, tiofosforsyretriamidene oppnådd i samsvar med denne fremgangsmåten og anvendelsen av disse tiofosforsyretriamidene som additiv til ureaholdige mineralske og/eller organisk-mineralske gjødningsmidler.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005053540A DE102005053540A1 (de) | 2005-11-08 | 2005-11-08 | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe unpolarer Amine |
| PCT/EP2006/066397 WO2007054392A1 (de) | 2005-11-08 | 2006-09-15 | Verfahren zur abtrennung von säuren aus chemischen reaktionsgemischen mit hilfe unpolarer amine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO20081962L true NO20081962L (no) | 2008-08-06 |
Family
ID=37596190
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20081962A NO20081962L (no) | 2005-11-08 | 2008-04-25 | Fremgangsmate for a separere syrer fra kjemiske reaksjonsblandinger ved hjelp av apolare aminer |
Country Status (18)
| Country | Link |
|---|---|
| US (2) | US9359269B2 (no) |
| EP (2) | EP1948670B1 (no) |
| CN (1) | CN101305015A (no) |
| AT (2) | ATE489393T1 (no) |
| AU (1) | AU2006311130B2 (no) |
| BR (1) | BRPI0618331B1 (no) |
| CA (1) | CA2628503C (no) |
| DE (2) | DE102005053540A1 (no) |
| DK (2) | DK2204372T3 (no) |
| ES (2) | ES2378344T3 (no) |
| MX (2) | MX295383B (no) |
| NO (1) | NO20081962L (no) |
| NZ (1) | NZ567995A (no) |
| PL (2) | PL2204372T3 (no) |
| PT (2) | PT2204372E (no) |
| RU (1) | RU2417229C9 (no) |
| UA (1) | UA90188C2 (no) |
| WO (1) | WO2007054392A1 (no) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007062614C5 (de) * | 2007-12-22 | 2019-03-14 | Eurochem Agro Gmbh | Mischung zur Behandlung von harnstoffhaltigen Düngemitteln, Verwendungen der Mischung und harnstoffhaltiges Düngemittel enthaltend die Mischung |
| EP2107064A1 (de) | 2008-04-02 | 2009-10-07 | Basf Se | Verfahren zur Herstellung von Triamiden aus Ammoniak und Amido-Dichloriden |
| CZ302400B6 (cs) | 2008-10-20 | 2011-05-04 | Agra Group, A.S. | Zpusob prípravy N-(hydrokarbyl)triamidu kyseliny fosforecné nebo thiofosforecné |
| CN102746333B (zh) * | 2012-06-12 | 2015-04-01 | 上虞盛晖化工股份有限公司 | 一种n-正丁基硫代磷酰三胺的合成方法 |
| EP2687536B1 (de) | 2012-07-18 | 2015-12-09 | Saltigo GmbH | Verfahren zur Herstellung von asymmetrischen (Thio)phosphorsäuretriamiden |
| AR092148A1 (es) | 2012-08-15 | 2015-03-25 | Koch Agronomic Services Llc | Composicones liquidas mejoradas que contienen inhibidores de ureasa y glicol alquil eteres y metodos de elaboracion y uso de las mismas |
| BR112015003095A2 (pt) | 2012-08-15 | 2017-07-04 | Koch Agronomic Services Llc | composições líquidas contendo inibidores de urease e aril-alquila álcoois |
| US8888886B1 (en) | 2013-08-06 | 2014-11-18 | Garnett B Whitehurst | NBPT solutions for preparing urease inhibited urea fertilizers prepared from N-substituted morpholines |
| US10501383B2 (en) | 2014-10-31 | 2019-12-10 | Koch Agronomic Services, Llc | Nitrification inhibitor compositions and methods of making thereof |
| CN112374933A (zh) | 2014-12-23 | 2021-02-19 | 巴斯夫欧洲公司 | 包含(硫代)磷酸三酰胺和其它化合物如胺和着色剂的具有改进脲酶抑制效果的组合物 |
| CN108026120B (zh) * | 2015-10-01 | 2021-11-16 | 巴斯夫欧洲公司 | 回收含有(硫代)磷酸衍生物的混合物的方法 |
| US10961264B2 (en) | 2015-12-01 | 2021-03-30 | Basf Se | Process for isolating a (thio)phosphoric acid derivative |
| CN112402998B (zh) * | 2020-12-11 | 2022-06-14 | 安徽标王农牧股份有限公司 | 一种适用于氨基酸的分级提取装置 |
| US12098109B2 (en) | 2021-03-15 | 2024-09-24 | Soilgenic Technologies, Llc | Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions |
| AU2022238316B2 (en) | 2021-03-15 | 2025-05-08 | Gary David Mcknight | Reaction methods for producing nitrogenous phosphoryl compounds that are in situ fluid compositions |
| CN113860943B (zh) * | 2021-09-24 | 2022-11-25 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种对三氟甲磺酸制备中釜残的综合处理方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE791311A (fr) * | 1971-11-16 | 1973-05-14 | Wacker Chemie Gmbh | Procede pour isoler le chlorure du bis-(dimethylamide) de l'acide phosphorique ou le tris-(dimethylamide) de l'acide phosphorique de leurs solutions impures |
| DD100475A1 (no) * | 1972-01-31 | 1973-09-20 | ||
| US4530714A (en) | 1983-03-16 | 1985-07-23 | Allied Corporation | N-aliphatic and N,N-aliphatic phosphoric triamide urease inhibitors and urease inhibited urea based fertilizer compositions |
| CH678054A5 (de) | 1989-07-17 | 1991-07-31 | Enco Eng Ag | Verfahren zur herstellung von tertiaeren amin-schwefel-trioxid-komplexen. |
| US5770771A (en) * | 1997-01-21 | 1998-06-23 | Albemarle Corporation | Preparation of N-hydrocarbylthiophosphoric triamides |
| AR038161A1 (es) * | 2002-01-24 | 2004-12-29 | Basf Ag | Procedimiento para separar acidos de mezclas de reaccion quimicas con la ayuda de liquidos ionicos |
| DE10360397A1 (de) | 2003-12-19 | 2005-07-14 | Basf Ag | Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von 1-Alkylimidazolen |
-
2005
- 2005-11-08 DE DE102005053540A patent/DE102005053540A1/de not_active Withdrawn
-
2006
- 2006-09-15 ES ES10156176T patent/ES2378344T3/es active Active
- 2006-09-15 DK DK10156176.9T patent/DK2204372T3/da active
- 2006-09-15 DE DE502006008403T patent/DE502006008403D1/de active Active
- 2006-09-15 AT AT06793548T patent/ATE489393T1/de active
- 2006-09-15 CN CNA2006800417865A patent/CN101305015A/zh active Pending
- 2006-09-15 EP EP06793548A patent/EP1948670B1/de active Active
- 2006-09-15 PT PT10156176T patent/PT2204372E/pt unknown
- 2006-09-15 ES ES06793548T patent/ES2355941T3/es active Active
- 2006-09-15 DK DK06793548.6T patent/DK1948670T3/da active
- 2006-09-15 UA UAA200807757A patent/UA90188C2/ru unknown
- 2006-09-15 PL PL10156176T patent/PL2204372T3/pl unknown
- 2006-09-15 WO PCT/EP2006/066397 patent/WO2007054392A1/de not_active Ceased
- 2006-09-15 CA CA2628503A patent/CA2628503C/en active Active
- 2006-09-15 US US12/092,392 patent/US9359269B2/en active Active
- 2006-09-15 EP EP10156176A patent/EP2204372B1/de active Active
- 2006-09-15 BR BRPI0618331A patent/BRPI0618331B1/pt not_active IP Right Cessation
- 2006-09-15 AT AT10156176T patent/ATE540045T1/de active
- 2006-09-15 RU RU2008122537/04A patent/RU2417229C9/ru active
- 2006-09-15 AU AU2006311130A patent/AU2006311130B2/en not_active Ceased
- 2006-09-15 PT PT06793548T patent/PT1948670E/pt unknown
- 2006-09-15 NZ NZ567995A patent/NZ567995A/en not_active IP Right Cessation
- 2006-09-15 PL PL06793548T patent/PL1948670T3/pl unknown
-
2008
- 2008-04-25 NO NO20081962A patent/NO20081962L/no not_active Application Discontinuation
- 2008-05-02 MX MX2011000779A patent/MX295383B/es unknown
- 2008-05-02 MX MX2008005701A patent/MX285596B/es active IP Right Grant
-
2016
- 2016-05-06 US US15/148,430 patent/US9493491B2/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FC2A | Withdrawal, rejection or dismissal of laid open patent application |