DK2971252T3 - Fremgangsmåde til fremstilling af lithiumhydroxid - Google Patents

Fremgangsmåde til fremstilling af lithiumhydroxid Download PDF

Info

Publication number
DK2971252T3
DK2971252T3 DK14764466.0T DK14764466T DK2971252T3 DK 2971252 T3 DK2971252 T3 DK 2971252T3 DK 14764466 T DK14764466 T DK 14764466T DK 2971252 T3 DK2971252 T3 DK 2971252T3
Authority
DK
Denmark
Prior art keywords
lithium hydroxide
preparing lithium
preparing
hydroxide
lithium
Prior art date
Application number
DK14764466.0T
Other languages
English (en)
Inventor
Guy Bourassa
Gary Pearse
Peter Symons
J David Genders
Daniel Bar
Marie-Eve Langevin
Jean-François Magnan
Original Assignee
Nemaska Lithium Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nemaska Lithium Inc filed Critical Nemaska Lithium Inc
Application granted granted Critical
Publication of DK2971252T3 publication Critical patent/DK2971252T3/da

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • C25B1/14Alkali metal compounds
    • C25B1/16Hydroxides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44Ion-selective electrodialysis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/42Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
    • B01D61/44Ion-selective electrodialysis
    • B01D61/445Ion-selective electrodialysis with bipolar membranes; Water splitting
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • C25B1/22Inorganic acids
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00Diaphragms; Spacing elements
    • C25B13/02Diaphragms; Spacing elements characterised by shape or form
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B13/00Diaphragms; Spacing elements
    • C25B13/04Diaphragms; Spacing elements characterised by the material
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • C25B15/023Measuring, analysing or testing during electrolytic production
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • C25B15/023Measuring, analysing or testing during electrolytic production
    • C25B15/025Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/027Temperature
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • C25B15/023Measuring, analysing or testing during electrolytic production
    • C25B15/025Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/029Concentration
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • C25B15/023Measuring, analysing or testing during electrolytic production
    • C25B15/025Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/029Concentration
    • C25B15/031Concentration pH
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C25B9/19Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms
    • C25B9/21Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof with diaphragms two or more diaphragms
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/02Process control or regulation
    • C25B15/023Measuring, analysing or testing during electrolytic production
    • C25B15/025Measuring, analysing or testing during electrolytic production of electrolyte parameters
    • C25B15/033Conductivity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/36Hydrogen production from non-carbon containing sources, e.g. by water electrolysis

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Water Supply & Treatment (AREA)
  • Inorganic Chemistry (AREA)
  • Automation & Control Theory (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Urology & Nephrology (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Manufacture And Refinement Of Metals (AREA)
DK14764466.0T 2013-03-15 2014-03-17 Fremgangsmåde til fremstilling af lithiumhydroxid DK2971252T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201361788292P 2013-03-15 2013-03-15
PCT/CA2014/000264 WO2014138933A1 (en) 2013-03-15 2014-03-17 Processes for preparing lithium hydroxide

Publications (1)

Publication Number Publication Date
DK2971252T3 true DK2971252T3 (da) 2021-03-29

Family

ID=51535686

Family Applications (1)

Application Number Title Priority Date Filing Date
DK14764466.0T DK2971252T3 (da) 2013-03-15 2014-03-17 Fremgangsmåde til fremstilling af lithiumhydroxid

Country Status (11)

Country Link
US (5) US20160032471A1 (da)
EP (4) EP3805428B1 (da)
AU (3) AU2014231593B2 (da)
CA (3) CA3014124A1 (da)
DK (1) DK2971252T3 (da)
ES (1) ES2859556T3 (da)
HR (1) HRP20210506T1 (da)
PL (1) PL2971252T3 (da)
PT (1) PT2971252T (da)
RS (2) RS67436B1 (da)
WO (1) WO2014138933A1 (da)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2871092C (en) 2012-04-23 2017-05-09 Nemaska Lithium Inc. Processes for preparing lithium hydroxide
AU2013270412C1 (en) 2012-05-30 2017-04-06 Nemaska Lithium Inc. Processes for preparing lithium carbonate
DK2971252T3 (da) 2013-03-15 2021-03-29 Nemaska Lithium Inc Fremgangsmåde til fremstilling af lithiumhydroxid
CA2928227C (en) * 2013-10-23 2017-05-16 Nemaska Lithium Inc. Processes and systems for preparing lithium hydroxide
KR102445712B1 (ko) 2013-10-23 2022-09-20 네마스카 리튬 인코포레이션 리튬 카보네이트의 제조방법
RS59229B1 (sr) 2014-02-24 2019-10-31 Nemaska Lithium Inc Postupci za obradu materijalima koji sadrže litijum
DE102015203395A1 (de) 2015-02-25 2016-08-25 Technische Universität Bergakademie Freiberg Verfahren zur elektrodialytischen Herstellung von Lithiumhydroxid aus verunreinigten lithiumhaltigen wässrigen Diluaten
KR101711854B1 (ko) * 2015-05-13 2017-03-03 재단법인 포항산업과학연구원 수산화리튬 및 탄산리튬의 제조 방법
US10597305B2 (en) 2015-08-27 2020-03-24 Nemaska Lithium Inc. Methods for treating lithium-containing materials
GB201602259D0 (en) * 2016-02-08 2016-03-23 Bateman Advanced Technologies Ltd Integrated Lithium production process
US11289700B2 (en) 2016-06-28 2022-03-29 The Research Foundation For The State University Of New York KVOPO4 cathode for sodium ion batteries
CA2940509A1 (en) 2016-08-26 2018-02-26 Nemaska Lithium Inc. Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid
CN106495188B (zh) * 2016-10-28 2017-08-08 荆门市格林美新材料有限公司 氢氧化锂制备系统
AU2018354320B2 (en) * 2017-10-26 2024-06-13 International Battery Metals, Ltd. Modular extraction apparatus
CN113772750B (zh) * 2017-11-22 2024-05-10 内玛斯卡锂业有限公司 制备各种金属的氢氧化物和氧化物以及其衍生物的方法
CZ2018250A3 (cs) * 2018-05-29 2020-01-15 Membrain S.R.O. Způsob výroby chemických sloučenin lithia metodou elektrodialýzy a zařízení k provádění tohoto způsobu
CA3124281C (en) * 2018-12-21 2023-08-22 Mangrove Water Technologies Ltd. Li recovery processes and onsite chemical production for li recovery processes
EP3972937A4 (en) 2019-05-22 2023-07-26 Nemaska Lithium Inc. PROCESSES FOR THE PREPARATION OF HYDROXIDES AND OXIDES OF VARIOUS METALS AND THEIR DERIVATIVES
CN111252749B (zh) * 2020-01-21 2022-11-22 曲靖市德方纳米科技有限公司 由锂磷铝石制备磷酸铁和氢氧化铝的方法
JP7156322B2 (ja) * 2020-02-17 2022-10-19 住友金属鉱山株式会社 水酸化リチウムの製造方法
CN111765500B (zh) * 2020-06-30 2021-06-01 湖南第一师范学院 稳定高效油烟生物净化系统及其净化处理效率控制方法
US20230406717A1 (en) 2020-11-20 2023-12-21 Basf Se Process for the removal of fluoride from alkaline hydroxide solutions
WO2022173852A1 (en) * 2021-02-09 2022-08-18 Energy Exploration Technologies, Inc. Systems and methods for direct lithium hydroxide production
US20250003099A1 (en) * 2021-07-09 2025-01-02 Basf Se ELECTROLYSIS OF Li2SO4 AT LOW PH RANGES
EP4186997A1 (en) 2021-11-26 2023-05-31 K-UTEC AG Salt Technologies Preparation of lithium hydroxide
FR3139563A1 (fr) * 2022-09-08 2024-03-15 Eurodia Industrie Procédé de préparation d’hydroxyde de lithium, et installation pour la mise en œuvre du procédé
EP4335827A1 (de) 2022-09-12 2024-03-13 Evonik Operations GmbH Herstellen von wasserstoff und festem lithiumhydroxid
EP4335828B1 (de) 2022-09-12 2025-02-12 Evonik Operations GmbH Herstellen von wasserstoff und lithiumhydroxid im basischen milieu
PL4335829T3 (pl) 2022-09-12 2025-12-08 Evonik Operations Gmbh Elektrochemiczne wytwarzanie wodoru i tlenku litu w określonych warunkach przepływu

Family Cites Families (138)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA659894A (en) 1963-03-19 N. Glew David Aqueous solution treatment
CA504477A (en) 1954-07-20 B. Ellestad Reuben Method of extracting lithium values from spodumene ores
GB530028A (en) 1938-06-22 1940-12-03 Bolidens Gruv Ab Method of recovering lithium from minerals
US2331838A (en) 1938-06-22 1943-10-12 Bolidens Gruv Ab Method of recovering lithium from minerals
US2516109A (en) 1948-09-16 1950-07-25 Metalloy Corp Method of extracting lithium values from spodumene ores
US2793941A (en) 1949-03-21 1957-05-28 Nelson N Estes Apparatus for growing crystals
US2882243A (en) 1953-12-24 1959-04-14 Union Carbide Corp Molecular sieve adsorbents
US2872393A (en) 1954-12-03 1959-02-03 Olin Mathieson Production of lithium hydroxide
GB841989A (en) * 1955-06-03 1960-07-20 Ronald Herbert Henry Morley Improvements in and relating to methods of extracting lithium from petalite, products of those methods and applications of those products
GB845511A (en) 1956-01-03 1960-08-24 Permutit Co Ltd Improvements relating to the production of metal hydroxides
US3007771A (en) 1956-11-30 1961-11-07 American Potash & Chem Corp Manufacture of lithium carbonate
US3214362A (en) 1961-01-09 1965-10-26 Ionics Electrolysis of aqueous electrolyte solutions and apparatus therefor
US3597340A (en) 1968-11-05 1971-08-03 Lithium Corp Recovery of lithium as lioh.h20 from aqueous chloride brines containing lithium chloride and sodium chloride
SU310538A1 (da) 1969-08-04 1974-08-05 Институт неорганической химии , электрохимии Грузинской ССР
US3857920A (en) 1971-07-29 1974-12-31 Department Of Health Education Recovery of lithium carbonate
US3899403A (en) 1973-11-01 1975-08-12 Hooker Chemicals Plastics Corp Electrolytic method of making concentrated hydroxide solutions by sequential use of 3-compartment and 2-compartment electrolytic cells having separating compartment walls of particular cation-active permselective membranes
JPS5174253A (ja) * 1974-12-24 1976-06-28 Sharp Kk Teidenatsusochi
US3959095A (en) 1975-01-31 1976-05-25 Hooker Chemicals & Plastics Corporation Method of operating a three compartment electrolytic cell for the production of alkali metal hydroxides
US3994741A (en) * 1975-03-26 1976-11-30 Lithium Corporation Of America Production of bricks
JPS51113108A (en) 1975-03-28 1976-10-06 Sawafuji Electric Co Ltd Automatic voltage control system in brushless generator
US4036713A (en) 1976-03-04 1977-07-19 Foote Mineral Company Process for the production of high purity lithium hydroxide
JPS5948870B2 (ja) * 1977-09-13 1984-11-29 旭硝子株式会社 水酸化リチウムの製造方法
US4207297A (en) 1978-03-27 1980-06-10 Foote Mineral Company Process for producing high purity lithium carbonate
US4273628A (en) 1979-05-29 1981-06-16 Diamond Shamrock Corp. Production of chromic acid using two-compartment and three-compartment cells
US4287163A (en) 1979-05-29 1981-09-01 Saline Processors, Inc. Process for recovering lithium from brine by salting out lithium sulfate monohydrate
JPS5795826A (en) 1980-12-04 1982-06-14 Rasa Kogyo Kk Manufacture of high purity lithium salt of mineral acid
US4391680A (en) 1981-12-03 1983-07-05 Allied Corporation Preparing alkali metal hydroxide by water splitting and hydrolysis
US4504373A (en) * 1982-06-01 1985-03-12 Allied Corporation Electrodialytic water splitting process and apparatus for conversion of alkali metal sulfate values derived from spent rayon spin baths
US4561945A (en) 1984-07-30 1985-12-31 United Technologies Corporation Electrolysis of alkali metal salts with hydrogen depolarized anodes
US4723962A (en) 1985-02-04 1988-02-09 Lithium Corporation Of America Process for recovering lithium from salt brines
US4999095A (en) 1985-05-03 1991-03-12 Allied-Signal Inc. Recovery of mixed acids from mixed salts
US4707234A (en) 1985-10-25 1987-11-17 Toyo Soda Manufacturing Co., Ltd. Method for separating an acid and an alkali from an aqueous solution of a salt
CA1272982A (en) 1985-11-14 1990-08-21 Donald Lorne Ball Method for the recovery of lithium from solutions by electrodialysis
US5120576A (en) 1988-05-24 1992-06-09 Ceramem Separations Limited Partnership Impregnating porous inorganic membrane with reactive inorganic binder
US4806215A (en) 1988-07-27 1989-02-21 Tenneco Canada Inc. Combined process for production of chlorine dioxide and sodium hydroxide
US4961909A (en) 1989-11-09 1990-10-09 Comino Ltd. Process for the manufacture of copper arsenate
DE4009410A1 (de) * 1990-03-23 1991-09-26 Basf Ag Verfahren zur elektrochemischen spaltung von alkali sulfaten
US5198080A (en) 1990-06-08 1993-03-30 Tenneco Canada Inc. Electrochemical processing of aqueous solutions
US5129936A (en) 1990-07-30 1992-07-14 Wilson Harold W Processes for the preparation of acid fortified paramagnetic iron sulfate salt compounds for use in the treatment of agricultural soils
US5258103A (en) 1991-01-17 1993-11-02 Mitsubishi Kasei Corporation Process for producing terbium alloy or terbium metal
JP2535748B2 (ja) 1991-03-04 1996-09-18 工業技術院長 リチウム回収方法
US5098532A (en) * 1991-05-24 1992-03-24 Ormiston Mining And Smelting Co. Ltd. Process for producing sodium hydroxide and ammonium sulfate from sodium sulfate
SE500107C2 (sv) 1991-06-26 1994-04-18 Eka Nobel Ab Förfarande för framställning av klordioxid
IT1248564B (it) 1991-06-27 1995-01-19 Permelec Spa Nora Processo di decomposizione elettrochimica di sali neutri senza co-produzione di alogeni o di acido e cella di elettrolisi adatta per la sua realizzazione.
GB9119613D0 (en) 1991-09-13 1991-10-23 Ici Plc Electrochemical process
US5246551A (en) 1992-02-11 1993-09-21 Chemetics International Company Ltd. Electrochemical methods for production of alkali metal hydroxides without the co-production of chlorine
SE511003C2 (sv) 1992-03-16 1999-07-19 Eka Chemicals Ab Förfarande och apparat för framställning av svavelsyra och alkalimetallhydroxid
EP0600470A3 (en) 1992-12-04 1995-01-04 Asahi Glass Co Ltd Bipolar membrane.
FI94063C (fi) * 1993-08-17 1995-07-10 Kemira Oy Menetelmä alkalimetalli- tai ammoniumperoksodisulfaattisuolojen ja alkalimetallihydroksidin samanaikaiseksi valmistamiseksi
US5830422A (en) 1995-06-23 1998-11-03 Ormiston Mining And Smelting Co. Ltd. Method for production of sodium bicarbonate, sodium carbonate and ammonium sulfate from sodium sulfate
US6514640B1 (en) 1996-04-23 2003-02-04 Board Of Regents, The University Of Texas System Cathode materials for secondary (rechargeable) lithium batteries
US5788943A (en) 1996-09-05 1998-08-04 The Hall Chemical Company Battery-grade nickel hydroxide and method for its preparation
US6004439A (en) * 1997-03-19 1999-12-21 Bakhir; Vitold M. Apparatus for obtaining products by anode oxidation of dissolved chlorides of alkaline or alkaline-earth metals
EP1016152A1 (en) 1997-06-23 2000-07-05 Pacific Lithium Limited Lithium recovery and purification
WO1999000178A1 (en) * 1997-06-30 1999-01-07 Electrosynthesis Company, Inc. Electrochemical methods for recovery of ascorbic acid
US6120576A (en) 1997-09-11 2000-09-19 Mitsui Mining And Smelting Co., Ltd. Method for preparing nickel fine powder
US6048507A (en) 1997-12-09 2000-04-11 Limtech Process for the purification of lithium carbonate
DE19809420A1 (de) 1998-03-05 1999-09-09 Basf Ag Verfahren zur Herstellung von hochreinen Lithiumsalzen
US6306787B1 (en) 1998-06-10 2001-10-23 Sakai Chemical Industry Co., Ltd. Nickel hydroxide particles and production and use thereof
US6331236B1 (en) 1998-07-21 2001-12-18 Archer Daniels Midland Company Electrodialysis of salts for producing acids and bases
JP2000129364A (ja) 1998-10-27 2000-05-09 Toshiba Corp 金属の回収方法
US6547836B1 (en) 1998-11-10 2003-04-15 Sqm Salar S.A. Process for obtaining monohydrated lithium sulfate from natural brines
US6627061B2 (en) 1999-05-05 2003-09-30 Archer-Daniels-Midland Company Apparatus and process for electrodialysis of salts
US7390466B2 (en) 1999-07-14 2008-06-24 Chemetall Foote Corporation Production of lithium compounds directly from lithium containing brines
DE19940069A1 (de) 1999-08-24 2001-03-08 Basf Ag Verfahren zur elektrochemischen Herstellung eines Alkalimetalls aus wäßriger Lösung
US6747065B1 (en) 2000-09-01 2004-06-08 Chemical Products Corporation System and method for producing high purity colloidal silica and potassium hydroxide
CA2319285A1 (en) 2000-09-13 2002-03-13 Hydro-Quebec A method for neutralizing and recycling spent lithium metal polymer rechargeable batteries
US6375824B1 (en) * 2001-01-16 2002-04-23 Airborne Industrial Minerals Inc. Process for producing potassium hydroxide and potassium sulfate from sodium sulfate
RU2196735C1 (ru) 2001-07-20 2003-01-20 Закрытое акционерное общество "Экостар-Наутех" Способ получения моногидрата гидроксида лития высокой степени чистоты из материалов, содержащих карбонат лития
TW511306B (en) 2001-08-20 2002-11-21 Ind Tech Res Inst Clean process of recovering metals from waste lithium ion batteries
NZ520452A (en) 2002-10-31 2005-03-24 Lg Chemical Ltd Anion containing mixed hydroxide and lithium transition metal oxide with gradient of metal composition
US7438817B2 (en) 2003-07-24 2008-10-21 Otu Sa System and method for treatment of acidic wastewater
AP2318A (en) 2005-10-03 2011-11-04 Outotec Oyj Method for processing nickel bearing raw material in chloride-based leaching.
JP4211865B2 (ja) 2006-12-06 2009-01-21 戸田工業株式会社 非水電解質二次電池用Li−Ni複合酸化物粒子粉末及びその製造方法、並びに非水電解質二次電池
CN104878405A (zh) 2008-04-22 2015-09-02 罗克伍德锂公司 制备高纯度氢氧化锂和盐酸的方法
JP5087790B2 (ja) 2008-06-17 2012-12-05 住友金属鉱山株式会社 アルミニウム含有水酸化ニッケル粒子の製造方法
JP5251401B2 (ja) 2008-09-29 2013-07-31 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質及びその製造方法、並びに非水系電解質二次電池
MX2011005159A (es) * 2008-11-17 2011-07-28 Chemetall Foote Corp Recuperacion de litio de soluciones acuosas.
AU2012261548B2 (en) 2008-11-17 2013-02-21 Rockwood Lithium Inc. Recovery of lithium from aqueous solutions
DE102009010264B4 (de) 2009-02-24 2015-04-23 Süd-Chemie Ip Gmbh & Co. Kg Verfahren zur Aufreinigung lithiumhaltiger Abwässer bei der kontinuierlichen Herstellung von Lithiumübergangsmetallphosphaten
FI121785B (fi) 2009-03-11 2011-04-15 Outotec Oyj Menetelmä litiumbikarbonaatin puhdistamiseksi
JP2011031232A (ja) * 2009-08-04 2011-02-17 Kee:Kk 水酸化リチウムの製造方法
CA2786317C (en) * 2010-01-07 2020-07-07 Galaxy Resources Limited Process for the production of lithium carbonate
US8936770B2 (en) 2010-01-22 2015-01-20 Molycorp Minerals, Llc Hydrometallurgical process and method for recovering metals
CA2985579C (en) * 2010-02-17 2022-11-29 Alger Alternative Energy, Llc Method of producing lithium carbonate from lithium chloride with gas-liquid-solid separator
FI122188B (fi) 2010-03-18 2011-09-30 Outotec Oyj Hydrometallurginen menetelmä metallisen nikkelin valmistamiseksi
EP2560920B1 (en) 2010-04-23 2020-09-16 TerraLithium LLC A process for making lithium carbonate from lithium chloride
FI122831B (fi) 2010-05-25 2012-07-31 Outotec Oyj Menetelmä spodumeenin käsittelemiseksi
WO2011156861A1 (en) 2010-06-15 2011-12-22 The University Of Queensland Method of recovering a metal
US8431005B1 (en) 2010-06-24 2013-04-30 Western Lithium Corporation Production of lithium and potassium compounds
JP2013531738A (ja) 2010-06-30 2013-08-08 シー アメンドラ スティーヴン リチウム金属の電解生成
WO2012021033A2 (en) 2010-08-12 2012-02-16 Research Institute Of Industrial Science & Technology Method of extracting lithium with high purity from lithium bearing solution by electrolysis
WO2012048280A2 (en) * 2010-10-08 2012-04-12 Ceramatec, Inc. Electrochemical systems and methods for operating electrochemical cell with an acidic anolyte
US8641874B2 (en) * 2010-12-09 2014-02-04 Rayne Guest Compact closed-loop electrolyzing process and apparatus
CN102020295B (zh) 2010-12-22 2012-07-25 四川天齐锂业股份有限公司 高纯碳酸锂的制备方法
PL2668303T3 (pl) 2011-01-25 2019-10-31 Univ Queensland Ulepszony sposób przetwarzania rudy
US8937037B2 (en) * 2011-03-02 2015-01-20 Ecolab Usa Inc. Electrochemical enhancement of detergent alkalinity
CA2868373A1 (en) 2011-03-24 2012-09-27 New Sky Energy, Llc Sulfate-based electrolysis processing with flexible feed control, and use to capture carbon dioxide
ITMI20110500A1 (it) * 2011-03-29 2012-09-30 Industrie De Nora Spa Cella per l elettrodialisi depolarizzata di soluzioni saline
AU2012248126B2 (en) 2011-04-29 2015-09-24 Commonwealth Scientific And Industrial Research Organisation Recovery of soda from bauxite residue
JP5316726B2 (ja) 2011-06-07 2013-10-16 住友金属鉱山株式会社 ニッケル複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および、非水系電解質二次電池
JP6007601B2 (ja) 2011-06-23 2016-10-12 東ソー株式会社 マンガン酸化物の製造方法
CN102408411B (zh) 2011-09-19 2014-10-22 北京康辰药业股份有限公司 一种含喹啉基的羟肟酸类化合物及其制备方法、以及含有该化合物的药物组合物及其应用
JP5138822B1 (ja) 2012-02-23 2013-02-06 株式会社アストム 高純度水酸化リチウムの製造方法
WO2013140039A1 (en) 2012-03-19 2013-09-26 Outotec Oyj Method for recovering lithium carbonate
JP5406955B2 (ja) 2012-03-22 2014-02-05 日鉄鉱業株式会社 炭酸リチウムを製造する方法
WO2013153692A1 (ja) 2012-04-13 2013-10-17 旭化成株式会社 リチウム回収方法
CA2871092C (en) 2012-04-23 2017-05-09 Nemaska Lithium Inc. Processes for preparing lithium hydroxide
JP5770675B2 (ja) 2012-04-26 2015-08-26 古河機械金属株式会社 硫化リチウムの製造方法
AU2013270412C1 (en) 2012-05-30 2017-04-06 Nemaska Lithium Inc. Processes for preparing lithium carbonate
FI124088B (fi) 2012-06-05 2014-03-14 Outotec Oyj Menetelmä ja laitteisto puhtaan litiumpitoisen liuoksen valmistamiseksi
WO2014040138A1 (en) 2012-09-14 2014-03-20 The University Of Queensland Resin scavenging of nickel and cobalt
JP6359018B2 (ja) 2012-10-10 2018-07-18 ロックウッド リチウム ゲゼルシャフト ミット ベシュレンクテル ハフツングRockwood Lithium GmbH 使用済みガルバニ電池のリチウム遷移金属酸化物含有部分からの、湿式冶金法によるリチウム、ニッケル、コバルトの回収方法
CN103086405B (zh) 2013-01-05 2013-12-25 阿坝中晟锂业有限公司 一种电池级碳酸锂的清洁化生产方法
DK2971252T3 (da) 2013-03-15 2021-03-29 Nemaska Lithium Inc Fremgangsmåde til fremstilling af lithiumhydroxid
CA2928227C (en) 2013-10-23 2017-05-16 Nemaska Lithium Inc. Processes and systems for preparing lithium hydroxide
KR102445712B1 (ko) 2013-10-23 2022-09-20 네마스카 리튬 인코포레이션 리튬 카보네이트의 제조방법
CN105874089A (zh) 2013-12-03 2016-08-17 昆士兰大学 加工铜的方法
RS59229B1 (sr) 2014-02-24 2019-10-31 Nemaska Lithium Inc Postupci za obradu materijalima koji sadrže litijum
AU2015330958B2 (en) 2014-10-10 2019-11-28 Cornish Lithium plc Recovery process
JP2016162601A (ja) 2015-03-02 2016-09-05 Jx金属株式会社 リチウムイオン電池用正極活物質の製造方法、リチウムイオン電池用正極活物質、リチウムイオン電池用正極及びリチウムイオン電池
KR101711854B1 (ko) 2015-05-13 2017-03-03 재단법인 포항산업과학연구원 수산화리튬 및 탄산리튬의 제조 방법
US10597305B2 (en) 2015-08-27 2020-03-24 Nemaska Lithium Inc. Methods for treating lithium-containing materials
GB201602259D0 (en) 2016-02-08 2016-03-23 Bateman Advanced Technologies Ltd Integrated Lithium production process
DE102016103100A1 (de) 2016-02-23 2017-08-24 Outotec (Finland) Oy Verfahren und Vorrichtung zur thermischen Behandlung von körnigen Feststoffen
DE102016104738A1 (de) 2016-03-15 2017-09-21 Outotec (Finland) Oy Verfahren und Vorrichtung zur thermischen Behandlung von körnigen Feststoffen
CN106365181B (zh) 2016-08-26 2018-03-09 成都开飞高能化学工业有限公司 一种利用含较高杂质富锂溶液制备电池级碳酸锂的方法
CA2940509A1 (en) 2016-08-26 2018-02-26 Nemaska Lithium Inc. Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid
CN106315625B (zh) 2016-08-26 2018-07-10 成都开飞高能化学工业有限公司 复合生产高纯单水氢氧化锂、高纯碳酸锂和电池级碳酸锂的方法
WO2018087697A1 (en) 2016-11-09 2018-05-17 Avalon Advanced Materials Inc. Methods and systems for preparing lithium hydroxide
US10508049B2 (en) 2017-05-11 2019-12-17 Tesla, Inc. System for regenerating sodium hydroxide and sulfuric acid from waste water stream containing sodium and sulfate ions
AU2018280351A1 (en) 2017-06-08 2020-01-02 Nmr 360 Inc Process for the recovery of cobalt, lithium, and other metals from spent lithium-based batteries and other feeds
US20210079496A1 (en) 2017-06-08 2021-03-18 Nmr 360 Inc Method for the recovery of lithium
WO2018227237A1 (en) 2017-06-14 2018-12-20 Urban Mining Pty Ltd Method for the production of cobalt and associated oxides from various feed materials
US12180082B2 (en) 2017-06-22 2024-12-31 Outotec (Finland) Oy Method of extracting lithium compound(s)
WO2019059654A1 (ko) 2017-09-19 2019-03-28 주식회사 엘지화학 이차전지용 양극 활물질 전구체, 양극 활물질 및 이를 포함하는 리튬 이차전지
CN113772750B (zh) 2017-11-22 2024-05-10 内玛斯卡锂业有限公司 制备各种金属的氢氧化物和氧化物以及其衍生物的方法
CN109694957B (zh) 2019-02-26 2020-12-18 中国科学院城市环境研究所 一种利用离子液体萃取锂离子电池浸出液金属离子的方法

Also Published As

Publication number Publication date
US20160032471A1 (en) 2016-02-04
US20200087804A1 (en) 2020-03-19
PT2971252T (pt) 2021-04-06
EP3805428B1 (en) 2025-09-03
HRP20210506T1 (hr) 2021-06-11
CA2905197A1 (en) 2014-09-18
AU2014231593B2 (en) 2017-08-17
AU2017258936B2 (en) 2019-05-02
US20240229266A1 (en) 2024-07-11
EP4424408A9 (en) 2025-03-26
PL2971252T3 (pl) 2021-07-12
EP4424408A2 (en) 2024-09-04
RS67436B1 (sr) 2025-12-31
EP4631606A2 (en) 2025-10-15
AU2019210218A1 (en) 2019-08-15
WO2014138933A1 (en) 2014-09-18
US12410531B2 (en) 2025-09-09
CA3014124A1 (en) 2014-09-18
AU2019210218B2 (en) 2021-09-02
US20210348285A1 (en) 2021-11-11
EP2971252B1 (en) 2020-12-30
EP2971252A1 (en) 2016-01-20
CA2905197C (en) 2016-11-22
AU2017258936C1 (en) 2019-11-14
EP2971252A4 (en) 2016-11-23
AU2017258936A1 (en) 2017-11-30
EP3805428C0 (en) 2025-09-03
ES2859556T3 (es) 2021-10-04
US20260055526A1 (en) 2026-02-26
AU2014231593A1 (en) 2015-10-08
EP3805428A1 (en) 2021-04-14
EP4424408A3 (en) 2025-04-09
CA2944759C (en) 2025-11-18
US11078583B2 (en) 2021-08-03
CA2944759A1 (en) 2014-09-18
RS61656B1 (sr) 2021-04-29

Similar Documents

Publication Publication Date Title
DK2841623T3 (da) Fremgangsmåder til fremstilling af lithiumhydroxid
DK3083540T3 (da) Fremgangsmåde til fremstilling af substituerede phenoxyphenylketoner
DK3006568T3 (da) Fremgangsmåde til fremstilling af tagatose
DK3079836T3 (da) Fremgangsmåder til fremstilling af effektlag
DK3060522T3 (da) Processer til forberedelse af lithiumkarbonat
IL246002A0 (en) Novel methods
PL2971252T3 (pl) Procesy dla sporządzania wodorotlenku litu
DK3611262T3 (da) Fremgangsmåder til sekvensering af immunrepertoire
DK3015467T3 (da) Morpholino-oligonukleotidfremstillingsfremgangsmåde
DK2845905T3 (da) Fremstilling af oligosaccharider
DK3010352T3 (da) Fremgangsmåde til fremstilling af fodertilsætning
DK2953904T3 (da) Fremgangsmåde til kontrolleret fremstilling af et biocid
DK2992104T3 (da) Fremgangsmåde til ekspression
DK2965026T3 (da) Generering af slushice
DK3054782T3 (da) Fremgangsmåde til tørring af biomasse
DK3010895T3 (da) Fremgangsmåde til fremstilling af 4-propargyleret aminobenzoxazinoner
IL243471B (en) Electrolyte regeneration
DK3065790T3 (da) Fremgangsmåder til fjernelse af alpha-galactose
DK3166927T3 (da) Fremgangsmåde til fremstilling af 4-alkoxy-3-hydroxy-picolinsyre
DK3369724T3 (da) Fremgangsmåde til fremstilling af iopamidol
BR112015021083A2 (pt) método
DK2996488T3 (da) Talloliefedtsyre
DK3137449T3 (da) Fremgangsmåder til fremstilling af substituerede cycloseriner
DK3175571T3 (da) Fremgangsmåder til tilpasning af over-the-air-synkronisering til radioforhold
BR112015029076A2 (pt) método