ES2032811T3 - Procedimiento para la produccion de tetrafluoruro de silicio. - Google Patents
Procedimiento para la produccion de tetrafluoruro de silicio.Info
- Publication number
- ES2032811T3 ES2032811T3 ES198787201303T ES87201303T ES2032811T3 ES 2032811 T3 ES2032811 T3 ES 2032811T3 ES 198787201303 T ES198787201303 T ES 198787201303T ES 87201303 T ES87201303 T ES 87201303T ES 2032811 T3 ES2032811 T3 ES 2032811T3
- Authority
- ES
- Spain
- Prior art keywords
- silicon tetrafluoride
- acid
- production
- aqueous solution
- gas flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- ABTOQLMXBSRXSM-UHFFFAOYSA-N silicon tetrafluoride Chemical compound F[Si](F)(F)F ABTOQLMXBSRXSM-UHFFFAOYSA-N 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- 239000003463 adsorbent Substances 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/107—Halogenated silanes
- C01B33/10705—Tetrafluoride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
SE PRESENTA UN PROCESO CONTINUO PARA LA PRODUCCION, CON GRAN RENDIMIENTO, DE TETRAFLUORURO DE SILICIO DE ALTA PUREZA, PARTIENDO DE UNA SOLUCION ACUOSA DE ACIDO FLUOSILICICO QUE COMPRENDE A) LA REACCION DE UNA SOLUCION ACUOSA DE ACIDO FLUOSILICICO CON ACIDO SULFURICO CONCENTRADO, REALIZADA CON UN CORTO TIEMPO DE RESIDENCIA Y PREFERIBLEMENTE BAJO CONDICIONES FLUIDODINAMICAS DE TURBULENCIA DENTRO DE UNA ZONA DE REACCION; B) LE SEPARACION DE UNA CORRIENTE GASEOSA CONTENIENDO TETRAFLUORURO DE SILICIO DE UNA CORRIENTE LIQUIDA DE ACIDO SULFURICO ACUOSO, REALIZADA DENTRO DE UNA ZONA DE SEPARACION, CONECTADA DIRECTAMENTE CON LA ZONA DE REACCION. C) EL LAVADO, CON ACIDO SULFURICO FRIO Y CONCENTRADO DE DICHA CORRIENTE GASEOSA, REALIZADA DENTRO DE UNA ZONA DE LAVADO, CON EL FIN DE SEPARAR UNA CORRIENTE GASEOSA DE TETRAFLUORURO DE SILICIO PURIFICADO; Y POSIBLEMENTE, D) LA POSTERIOR PURIFICACION DE DICHA CORRIENTE GASEOSA DE TETRAFLUORURO DE SILICIO PURIFICADO, POR MEDIO DE TECNICAS DE ADSORCION SOBRE UN MATERIAL SOLIDO ADSORBENTE.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT21226/86A IT1196983B (it) | 1986-07-23 | 1986-07-23 | Procedimento per la produzione di tetrafluoruro di silicio |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2032811T3 true ES2032811T3 (es) | 1993-03-01 |
Family
ID=11178673
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES198787201303T Expired - Lifetime ES2032811T3 (es) | 1986-07-23 | 1987-07-08 | Procedimiento para la produccion de tetrafluoruro de silicio. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4900530A (es) |
| EP (1) | EP0254349B1 (es) |
| JP (1) | JPS6340714A (es) |
| AT (1) | ATE76040T1 (es) |
| DE (1) | DE3778993D1 (es) |
| ES (1) | ES2032811T3 (es) |
| GR (1) | GR3004735T3 (es) |
| IT (1) | IT1196983B (es) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NO931606L (no) * | 1992-05-26 | 1993-11-29 | Saint Gobain Vitrage | Vindusplate med en funksjonell film |
| US5232602A (en) * | 1992-07-01 | 1993-08-03 | Hemlock Semiconductor Corporation | Phosphorous removal from tetrachlorosilane |
| US5242670A (en) * | 1992-07-02 | 1993-09-07 | Gehringer Ronald C | Method for hydrofluoric acid digestion of silica/alumina matrix material for the production of silicon tetrafluoride, aluminum fluoride and other residual metal fluorides and oxides |
| US5888468A (en) * | 1998-06-05 | 1999-03-30 | Starmet Corp. | Method for producing silicon tetrafluoride from uranium tetrafluoride |
| US6033642A (en) * | 1999-03-29 | 2000-03-07 | Starmet Corporation | Method for producing silicon tetrafluoride from uranium oxyfluoride |
| US7666379B2 (en) * | 2001-07-16 | 2010-02-23 | Voltaix, Inc. | Process and apparatus for removing Bronsted acid impurities in binary halides |
| TW200512159A (en) * | 2003-09-25 | 2005-04-01 | Showa Denko Kk | Method for producing tetrafluorosilane |
| JP4588396B2 (ja) * | 2003-09-25 | 2010-12-01 | 昭和電工株式会社 | テトラフルオロシランの製造方法 |
| JP4576312B2 (ja) * | 2005-10-03 | 2010-11-04 | 東北電力株式会社 | 四フッ化ケイ素の製造方法、及びそれに用いる製造装置 |
| US7541015B2 (en) | 2005-11-25 | 2009-06-02 | Vesta Research, Ltd. | Process for producing a silicon nitride compound |
| MY156877A (en) * | 2007-09-21 | 2016-04-15 | Memc Electronic Materials | Processes for purification of silicon tetrafluoride |
| US8528026B2 (en) * | 2008-12-05 | 2013-09-03 | At&T Intellectual Property I, L.P. | System and method for processing audio signals received by a communication device |
| US8124039B2 (en) | 2009-01-26 | 2012-02-28 | Vithal Revankar | Process of silicon tetrafluoride gas synthesis |
| CN112158849B (zh) * | 2020-09-27 | 2023-06-30 | 湖北祥云(集团)化工股份有限公司 | 一种磷矿伴生氟制备四氟化硅的方法 |
| WO2025165728A1 (en) * | 2024-01-30 | 2025-08-07 | Arkema Inc. | An improved method to produce silicon tetrafluoride from fluorosilicic acid |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2456509A (en) * | 1944-10-06 | 1948-12-14 | Allied Chem & Dye Corp | Manufacture of hydrogen fluoride |
| GB745800A (en) * | 1953-08-06 | 1956-02-29 | Kali Chemie Ag | Process for the production of pure silicon tetrafluoride |
| DE1022569B (de) * | 1954-06-09 | 1958-01-16 | Grace W R & Co | Verfahren zur Herstellung von Siliciumtetrafluorid |
| GB1015604A (en) * | 1961-10-11 | 1966-01-05 | Texas Instruments Ltd | A treatment process for silicon compounds |
| US3758674A (en) * | 1971-09-16 | 1973-09-11 | Wellman Power Gas Inc | Process for producing anhydrous hf from fluosilicic acid |
| US3969485A (en) * | 1971-10-28 | 1976-07-13 | Flemmert Goesta Lennart | Process for converting silicon-and-fluorine-containing waste gases into silicon dioxide and hydrogen fluoride |
| US4138509A (en) * | 1977-12-23 | 1979-02-06 | Motorola, Inc. | Silicon purification process |
| JPS604126B2 (ja) * | 1981-03-18 | 1985-02-01 | セントラル硝子株式会社 | 四弗化珪素の精製法 |
| JPS604127B2 (ja) * | 1981-08-06 | 1985-02-01 | セントラル硝子株式会社 | 四弗化珪素ガスの精製法 |
| US4470959A (en) * | 1983-06-20 | 1984-09-11 | Allied Corporation | Continuous production of silicon tetrafluoride gas in a vertical column |
| JPS6090810A (ja) * | 1983-10-20 | 1985-05-22 | Mitsui Toatsu Chem Inc | フルオロシランガスの製造方法 |
| US4557921A (en) * | 1984-06-27 | 1985-12-10 | Ethyl Corporation | Purification of halide |
| JPS6197129A (ja) * | 1984-10-18 | 1986-05-15 | Mitsui Toatsu Chem Inc | フルオロシラン類の精製法 |
| JPS61118117A (ja) * | 1984-11-14 | 1986-06-05 | Taiyo Sanso Kk | 有毒ガス成分を含むガスの処理方法 |
-
1986
- 1986-07-23 IT IT21226/86A patent/IT1196983B/it active
-
1987
- 1987-07-08 DE DE8787201303T patent/DE3778993D1/de not_active Expired - Fee Related
- 1987-07-08 ES ES198787201303T patent/ES2032811T3/es not_active Expired - Lifetime
- 1987-07-08 EP EP87201303A patent/EP0254349B1/en not_active Expired - Lifetime
- 1987-07-08 AT AT87201303T patent/ATE76040T1/de not_active IP Right Cessation
- 1987-07-23 US US07/076,736 patent/US4900530A/en not_active Expired - Fee Related
- 1987-07-23 JP JP62182427A patent/JPS6340714A/ja active Pending
-
1992
- 1992-05-27 GR GR920401084T patent/GR3004735T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GR3004735T3 (es) | 1993-04-28 |
| JPS6340714A (ja) | 1988-02-22 |
| EP0254349B1 (en) | 1992-05-13 |
| EP0254349A2 (en) | 1988-01-27 |
| US4900530A (en) | 1990-02-13 |
| IT8621226A1 (it) | 1988-01-23 |
| IT8621226A0 (it) | 1986-07-23 |
| EP0254349A3 (en) | 1988-08-31 |
| IT1196983B (it) | 1988-11-25 |
| DE3778993D1 (de) | 1992-06-17 |
| ATE76040T1 (de) | 1992-05-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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