ES2045159T3 - Diacetales de alditoles, de elevada pureza y exentos de trazas de disolventes organicos, y procedimientos para su preparacion. - Google Patents

Diacetales de alditoles, de elevada pureza y exentos de trazas de disolventes organicos, y procedimientos para su preparacion.

Info

Publication number
ES2045159T3
ES2045159T3 ES88400794T ES88400794T ES2045159T3 ES 2045159 T3 ES2045159 T3 ES 2045159T3 ES 88400794 T ES88400794 T ES 88400794T ES 88400794 T ES88400794 T ES 88400794T ES 2045159 T3 ES2045159 T3 ES 2045159T3
Authority
ES
Spain
Prior art keywords
diacetals
traces
organic solvents
benzoic
alditols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES88400794T
Other languages
English (en)
Inventor
Jean-Paul Salome
Guy Fleche
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Roquette Freres SA
Original Assignee
Roquette Freres SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Roquette Freres SA filed Critical Roquette Freres SA
Application granted granted Critical
Publication of ES2045159T3 publication Critical patent/ES2045159T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D325/00—Heterocyclic compounds containing rings having oxygen as the only ring hetero atom according to more than one of groups C07D303/00 - C07D323/00

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

LA INVENCION TIENE POR OBJETO LOS DIACETALES QUE RESULTAN DE LA DESHIDROCONDENSACION DE UN ALDITOL DE 5 O 6 ATOMOS DE C Y DE UN ALDEHIDO BENZOICO COMO PARTICULAMENTE EL DBS, BEBS, BMBS O DBX, CON UNA PUREZA DE AL MENOS 95% Y EXENTOS DE TRAZAS DE DISOLVENTES ORGANICOS, Y UN PROCEDIMIENTO PARA PREPARARLAS EN MEDIO ACUOSO SEGUN EL CUAL LA ACETILACION SE REALIZA POR MEZCLA DE REACTIVOS BAJO AGITACION, LA MEZCLA REACCIONAL ES NEUTRALIZADA ENSEGUIDA POR UNA BASE, DESPUES LA FASE SOLIDA SE SEPARA DE LA FASE LIQUIDA Y SE LAVA CON AGUA CALIENTE, SEGUN EL CUAL LA CANTIDAD MOLAR INICIAL DE ALDEHIDO BENZOICO DE ALDITOL ES INFERIOR A 2/L, EL CATALIZADOR ACIDO ES UN ARILSULFONICO, LA CANTIDAD MOLAR INICIAL DE ACIDO ARILSULFONICO DE ALDEHIDO BENZOICO ES SUPERIOR A 0,6, Y LA TEMPERATURA DE REACCION ES INFERIOR A ALREDEDOR DE 45 GRADOS C. APLICACION PARTICULARMENTE A LA CLARIFICACION Y LA ESTABILIZACION DE POLIIOLEFINAS.
ES88400794T 1987-04-07 1988-04-01 Diacetales de alditoles, de elevada pureza y exentos de trazas de disolventes organicos, y procedimientos para su preparacion. Expired - Lifetime ES2045159T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8704884A FR2613713B1 (fr) 1987-04-07 1987-04-07 Procede de preparation de diacetals d'alditols, notamment du dibenzylidene-sorbitol, en milieu aqueux

Publications (1)

Publication Number Publication Date
ES2045159T3 true ES2045159T3 (es) 1994-01-16

Family

ID=9349879

Family Applications (1)

Application Number Title Priority Date Filing Date
ES88400794T Expired - Lifetime ES2045159T3 (es) 1987-04-07 1988-04-01 Diacetales de alditoles, de elevada pureza y exentos de trazas de disolventes organicos, y procedimientos para su preparacion.

Country Status (10)

Country Link
US (1) US5023354A (es)
EP (1) EP0286522B1 (es)
JP (1) JP2694961B2 (es)
KR (1) KR960002595B1 (es)
AT (1) ATE82290T1 (es)
CA (1) CA1298306C (es)
DE (1) DE3875774T2 (es)
ES (1) ES2045159T3 (es)
FI (1) FI95706C (es)
FR (1) FR2613713B1 (es)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
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US5049605A (en) * 1989-09-20 1991-09-17 Milliken Research Corporation Bis(3,4-dialkylbenzylidene) sorbitol acetals and compositions containing same
US5609855A (en) * 1990-04-06 1997-03-11 The Procter & Gamble Company Gel stick antiperspirant compositions
US5106999A (en) * 1990-06-26 1992-04-21 The Procter & Gamble Company Process for preparing dibenzylidene-d-sorbitol compounds
US5216051A (en) * 1991-10-28 1993-06-01 Allied-Signal Inc. Polyolefins containing polyol nucleating agents and articles formed therefrom
DK0639968T3 (da) * 1992-05-12 1996-07-22 Procter & Gamble Antitranspirantgelstiftsammensætning
US5846520A (en) * 1996-12-20 1998-12-08 Procter & Gamble Company Antiperspirant gel-solid stick compositions containing select fatty acid gellants
US6190673B1 (en) 1996-12-20 2001-02-20 The Procter & Gamble Company Gel compositions containing gellants in the form of alkyl amides of tri-carboxylic acids
US5840287A (en) * 1996-12-20 1998-11-24 Procter & Gamble Company Antiperspirant compositions containing gellants in the form of alkyl amides of di- and tri-carboxylic acids
US5744130A (en) * 1996-12-20 1998-04-28 The Procter & Gamble Company Antiperspirant gel-solid stick compositions substantially free of select polar solvents
US5840286A (en) * 1996-12-20 1998-11-24 Procter & Gamble Company Methods of making low residue antiperspirant gel-solid stick compositions
US5776494A (en) * 1996-12-20 1998-07-07 The Procter & Gamble Company Pharmaceuticals compositions containing gellants in the form of alkyl amides of di-and tri-carboxylic acids
US6171601B1 (en) 1996-12-20 2001-01-09 The Procter & Gamble Company Low residue antiperspirant gel-solid stick compositions
US5849276A (en) * 1996-12-20 1998-12-15 Procter & Gamble Antiperspirant gel-solid stick compositions containing select nucleating agents
US5840288A (en) * 1996-12-20 1998-11-24 Procter & Gamble Company Antiperspirant gel-solid stick composition containing a modified silicone carrier
US5750096A (en) * 1996-12-20 1998-05-12 The Procter & Gamble Company Low residue antiperspirant gel-solid stick compositions containing select gellants
US5973043A (en) * 1997-11-26 1999-10-26 Milliken & Company Carbamoyl substituted acetals and compositions containing the same
FR2772767B1 (fr) * 1997-12-23 2000-02-25 Roquette Freres Composition amelioree d'acetal d'alditol et son utilisation dans les matieres plastiques et gelifiees
US6500964B2 (en) 2001-03-23 2002-12-31 Milliken & Company Method of producing high yield alditol acetals with mineral acids and surfactants
US7262236B2 (en) * 2004-04-26 2007-08-28 Milliken & Company Acetal-based compositions
PL1765843T3 (pl) * 2004-07-09 2017-01-31 Basf Se Sposób wytwarzania sproszkowanej kompozycji acetalu alditolu
US20060079720A1 (en) * 2004-10-13 2006-04-13 Milliken & Company Method for preparing acetal-containing compositions
US20090318593A1 (en) * 2005-09-28 2009-12-24 Klaus Stoll Process for Improving the Flow Properties of Polymer Melts
CN101873809B (zh) 2007-07-23 2014-11-12 R.J.雷诺兹烟草公司 无烟烟草组合物
JP5426120B2 (ja) * 2008-08-06 2014-02-26 南海化学株式会社 ジベンジリデンアルジトール類の製造方法
US20100037903A1 (en) * 2008-08-14 2010-02-18 R. J. Reynolds Tobacco Company Method for Preparing Flavorful and Aromatic Compounds
CN101434607B (zh) * 2008-12-12 2010-12-29 深圳大学 聚烯烃成核剂醇醛化合物的合成方法
US8434496B2 (en) 2009-06-02 2013-05-07 R. J. Reynolds Tobacco Company Thermal treatment process for tobacco materials
US8944072B2 (en) 2009-06-02 2015-02-03 R.J. Reynolds Tobacco Company Thermal treatment process for tobacco materials
US20110220130A1 (en) 2009-12-15 2011-09-15 John-Paul Mua Tobacco Product And Method For Manufacture
SG191886A1 (en) 2011-01-10 2013-08-30 Reliance Ind Ltd Process for preparation of acetals
US8969595B2 (en) 2011-01-10 2015-03-03 Reliance Industries Limited Method of making diacetal compound in aqueous medium
JP5827694B2 (ja) 2011-01-10 2015-12-02 リライアンス、インダストリーズ、リミテッドＲｅｌｉａｎｃｅ Ｉｎｄｕｓｔｒｉｅｓ Ｌｉｍｉｔｅｄ アルジトールアセタールの製造方法
KR20140027093A (ko) 2011-01-10 2014-03-06 릴라이언스 인더스트리즈 리미티드 알디톨 아세탈의 제조방법
TWI522405B (zh) * 2014-04-30 2016-02-21 國慶化學股份有限公司 Preparation of diacetal clear agent
KR102298667B1 (ko) * 2014-10-16 2021-09-06 에스케이이노베이션 주식회사 무증발 촉매를 이용한 무수당 알코올의 제조방법
US10081690B2 (en) 2016-06-23 2018-09-25 Sunko Ink Co., Ltd. Powdery diacetal clarifying agent and method of preparing the same
EP3478690B1 (en) 2016-06-30 2022-05-04 Hindustan Petroleum Corporation Limited C5 sugar based gelators for oil spills
WO2018040093A1 (zh) * 2016-09-05 2018-03-08 呈和科技股份有限公司 一种包含山梨醇三缩醛和单缩醛的透明成核剂组合物

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4843748B1 (es) * 1969-10-06 1973-12-20 New Japan Chem Co Ltd
JPS5147709B2 (es) * 1973-02-05 1976-12-16
JPS535165A (en) * 1976-07-01 1978-01-18 Ec Chem Ind Co Purification of dibenzylidenesorbitol
US4267110A (en) * 1978-11-29 1981-05-12 E.C. Chemical Ind. Co., Ltd. Process for preparing dibenzylidenesorbitol and composition containing the same
US4562265A (en) * 1979-10-11 1985-12-31 Milliken Research Corporation Method for producing a di-acetal of sorbitol and an aromatic aldehyde
DE3064734D1 (en) * 1979-05-02 1983-10-13 Ici Plc Acetals and their preparation
JPS5822157B2 (ja) * 1980-05-16 1983-05-06 新日本理化株式会社 １，３：２，４−ジベンジリデンソルビト−ル類及び１，３：２，４−ジベンジリデンキシルト−ル類の製造法
FR2486080A1 (fr) * 1980-07-02 1982-01-08 Milliken Res Corp Procede pour preparer un diacetal de sorbitol et d'un aldehyde aromatique
JPS5718682A (en) * 1980-07-08 1982-01-30 Mitsui Toatsu Chem Inc Preparation of bis p-ethylbenzylidene sorbitol
JPS5732278A (en) * 1980-07-16 1982-02-20 Milliken Res Corp Manufacture of diacetal
US4429140A (en) * 1981-12-29 1984-01-31 New Japan Chemical Co., Ltd. Process for preparing dibenzylidene sorbitols and dibenzylidene xylitols
JPS60199891A (ja) * 1984-03-22 1985-10-09 Seitetsu Kagaku Co Ltd ジベンジリデンソルビト−ル類の精製法

Also Published As

Publication number Publication date
FR2613713B1 (fr) 1989-08-04
KR960002595B1 (ko) 1996-02-23
FR2613713A1 (fr) 1988-10-14
US5023354A (en) 1991-06-11
ATE82290T1 (de) 1992-11-15
CA1298306C (en) 1992-03-31
FI95706C (fi) 1996-03-11
KR880012513A (ko) 1988-11-28
DE3875774D1 (de) 1992-12-17
JP2694961B2 (ja) 1997-12-24
EP0286522B1 (fr) 1992-11-11
EP0286522A1 (fr) 1988-10-12
DE3875774T2 (de) 1993-04-29
FI881507L (fi) 1988-10-08
FI881507A0 (fi) 1988-03-30
JPS63267777A (ja) 1988-11-04
FI95706B (fi) 1995-11-30

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