ES2068986T3 - Metodo para preparar bisfenol a. - Google Patents

Metodo para preparar bisfenol a.

Info

Publication number
ES2068986T3
ES2068986T3 ES90125099T ES90125099T ES2068986T3 ES 2068986 T3 ES2068986 T3 ES 2068986T3 ES 90125099 T ES90125099 T ES 90125099T ES 90125099 T ES90125099 T ES 90125099T ES 2068986 T3 ES2068986 T3 ES 2068986T3
Authority
ES
Spain
Prior art keywords
reaction
phenol
acetone
accordance
water generated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES90125099T
Other languages
English (en)
Inventor
Kenichi Okamoto
Hidetoshi Faculty Of Engi Kita
Yasuo Tanaka
Shigeru Iimuro
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Application granted granted Critical
Publication of ES2068986T3 publication Critical patent/ES2068986T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/12—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings
    • C07C39/15—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings with all hydroxy groups on non-condensed rings, e.g. phenylphenol
    • C07C39/16—Bis-(hydroxyphenyl) alkanes; Tris-(hydroxyphenyl)alkanes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1893—Membrane reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/009—Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00176—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles outside the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SE PRESENTA UN METODO PARA PREPARAR 2,2 NIL) PROPANO QUE COMPRENDE LA REACCION DE LA ACETONA Y EL FENOL EN PRESENCIA DE UNA RESINA ACIDICA INTERCAMBIADORA DE IONES COMO CATALIZADOR, EN DONDE LA REACCION DE LA ACETONA Y EL FENOL SE REALIZA MIENTRAS SE SEPARA UNA PARTE DEL AGUA GENERADA DURANTE LA REACCION DE UNA SOLUCION MEZCLADA QUE CONTENGA ACETONA Y FENOL MEDIANTE UN METODO DE EVAPORACION. DE ACUERDO CON EL METODO EL AGUA GENERADA A TRAVES DE LA REACCION PUEDE SEPARARSE RAPIDAMENTE SIMULTANEA O CON O ALTERNATIVIDAD A LA REACCION MEDIANTE UNA OPERACION DE EVAPORACION Y, ADEMAS, LA ACTIVIDAD CATALITICA DE LA RESINA INTERCAMBIADORA DE IONES PERMANECE INACEPTADA. MAS AUN, NO SE REQUIERE NINGUNA OPERACION COMPLICADA ASOCIADA CON LA DESHIDRATACION. DE ESTA MANERA, EL CATALIZADOR DE RESINA ACIDICA INTERCAMBIADORA DE IONES PUEDE USARSE DE FORMA CONTINUA A LO LARGO DE UN DILATADO PERIODO DE TIEMPO SIN NINGUN TRATAMIENTO PARA LA REGENERACION DEL MISMO. ADEMAS, DE ACUERDO CON ESTE METODO, EL BISFENOL A PUEDE PREPARARSE DE FORMA ECONOMICA A PARTIR DE ACETONA Y FENOL CON UN ALTO DE GRADO DE CONVERSION Y UN BUEN RENDIMIENTO.
ES90125099T 1989-12-25 1990-12-21 Metodo para preparar bisfenol a. Expired - Lifetime ES2068986T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP33280289 1989-12-25

Publications (1)

Publication Number Publication Date
ES2068986T3 true ES2068986T3 (es) 1995-05-01

Family

ID=18258968

Family Applications (1)

Application Number Title Priority Date Filing Date
ES90125099T Expired - Lifetime ES2068986T3 (es) 1989-12-25 1990-12-21 Metodo para preparar bisfenol a.

Country Status (5)

Country Link
US (1) US5087767A (es)
EP (1) EP0442122B1 (es)
KR (1) KR920010570B1 (es)
DE (1) DE69017653T2 (es)
ES (1) ES2068986T3 (es)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL164289B1 (pl) * 1990-11-24 1994-07-29 Inst Ciezkiej Syntezy Orga Sposób otrzymywani blsfenolu A PL PL
CN1080914A (zh) * 1993-02-17 1994-01-19 中国石油化工总公司 一种2,2-二(4-羟基苯基)丙烷的制造方法
JP3437575B2 (ja) * 1993-02-17 2003-08-18 チャイナ ペトロ−ケミカル コーポレーション 多段懸垂反応ストリッピング方法および装置
US6254978B1 (en) * 1994-11-14 2001-07-03 W. L. Gore & Associates, Inc. Ultra-thin integral composite membrane
EP0770590B1 (en) * 1995-09-29 2001-10-24 General Electric Company Process for the preparation of bisphenol compounds with simultaneous dehydration
US6635384B2 (en) * 1998-03-06 2003-10-21 Gore Enterprise Holdings, Inc. Solid electrolyte composite for electrochemical reaction apparatus
DE19756771A1 (de) * 1997-12-19 1999-06-24 Bayer Ag Verfahren zur Herstellung von Bis(4-hydroxyaryl)alkanen
DE19947505A1 (de) * 1999-10-01 2001-04-05 Degussa Verfahren zur Herstellung organischer Verbindungen im Membranreaktor
JP4042325B2 (ja) * 2000-12-07 2008-02-06 三菱化学株式会社 アミノチオール変性スルホン酸型陽イオン交換樹脂の保存方法
JP2002205966A (ja) * 2001-01-11 2002-07-23 Idemitsu Petrochem Co Ltd ビスフェノールａの製造方法
JP4723105B2 (ja) * 2001-03-01 2011-07-13 出光興産株式会社 ビスフェノールａの製造方法
US6703530B2 (en) 2002-02-28 2004-03-09 General Electric Company Chemical reactor system and process
US20040099605A1 (en) 2002-07-29 2004-05-27 Chen-Chou Chiang High performance continuous reaction/separation process using a continuous liquid-solid contactor
US7112702B2 (en) * 2002-12-12 2006-09-26 General Electric Company Process for the synthesis of bisphenol
US7132575B2 (en) * 2003-07-01 2006-11-07 General Electric Company Process for the synthesis of bisphenol
CN100494140C (zh) * 2003-09-28 2009-06-03 中国石油化工股份有限公司 一种制备双酚a的方法
US6939994B1 (en) * 2004-09-23 2005-09-06 Catalytic Distillation Technologies Process for the production of bisphenol-A
US8247619B2 (en) * 2008-12-11 2012-08-21 Sabic Innovative Plastics Ip B.V. BPA and polycarbonate made from renewable materials
US8735634B2 (en) 2011-05-02 2014-05-27 Sabic Innovative Plastics Ip B.V. Promoter catalyst system with solvent purification
US9290618B2 (en) 2011-08-05 2016-03-22 Sabic Global Technologies B.V. Polycarbonate compositions having enhanced optical properties, methods of making and articles comprising the polycarbonate compositions
US9490405B2 (en) 2012-02-03 2016-11-08 Sabic Innovative Plastics Ip B.V. Light emitting diode device and method for production thereof containing conversion material chemistry
CN104145001A (zh) 2012-02-29 2014-11-12 沙特基础创新塑料Ip私人有限责任公司 含转换材料化学物质并具有增强的光学特性的聚碳酸酯组合物、其制造方法及包含其的制品
EP2819981B1 (en) 2012-02-29 2016-12-21 SABIC Global Technologies B.V. Process for producing low sulfur bisphenol a, processes for producing polycarbonate, articles made from polycarbonate
US9346949B2 (en) 2013-02-12 2016-05-24 Sabic Global Technologies B.V. High reflectance polycarbonate
US9821523B2 (en) 2012-10-25 2017-11-21 Sabic Global Technologies B.V. Light emitting diode devices, method of manufacture, uses thereof
WO2014186548A1 (en) 2013-05-16 2014-11-20 Sabic Innovative Plastics Ip B.V. Branched polycarbonate compositions having conversion material chemistry and articles thereof
WO2014191943A1 (en) 2013-05-29 2014-12-04 Sabic Innovative Plastics Ip B.V. Illuminating devices with color stable thermoplastic light-transmitting articles
KR20170031137A (ko) 2014-07-15 2017-03-20 사빅 글로벌 테크놀러지스 비.브이. 비스페놀의 합성
CN119822925A (zh) * 2025-01-15 2025-04-15 天津大学 一种连续强化丙酮与苯酚缩合反应制双酚a的工艺

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2572141A (en) * 1946-02-11 1951-10-23 California Spray Chemical Corp Condensation of aldehydes
US2884462A (en) * 1956-02-28 1959-04-28 Union Carbide Corp Production of 2, 2-bis(oxyaryl)propane compounds
US3049569A (en) * 1958-10-20 1962-08-14 Union Carbide Corp Production of 2, 2-bis(4-hydroxyphenyl) propane
AU489747B2 (en) * 1973-12-17 1976-06-17 Monsanto Australia Limited Production of bis (hydroxyphenyl) alkanes
DE2418975A1 (de) * 1974-04-19 1975-10-30 Bayer Ag Verfahren zur herstellung von dihydroxydiphenylalkanen
GB1578225A (en) * 1977-07-11 1980-11-05 Shell Int Research Preparation of bisphenols
JPS6178741A (ja) * 1984-09-25 1986-04-22 Mitsui Toatsu Chem Inc ビスフエノ−ルａの製造方法
US4777301A (en) * 1986-06-25 1988-10-11 Union Carbide Corporation Process for the condensation of carbonyl and aromatic compounds
CA1312550C (en) * 1986-10-14 1993-01-12 Karl W. Boddeker Pervaporation of phenols
US4952319A (en) * 1986-12-15 1990-08-28 Mitsubishi Kasei Corporation Process for separating liquid mixture

Also Published As

Publication number Publication date
EP0442122A1 (en) 1991-08-21
KR910011726A (ko) 1991-08-07
DE69017653T2 (de) 1995-11-30
EP0442122B1 (en) 1995-03-08
US5087767A (en) 1992-02-11
KR920010570B1 (ko) 1992-12-07
DE69017653D1 (de) 1995-04-13

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