ES2107885T3 - Procedimiento para la obtencion de aminas. - Google Patents

Procedimiento para la obtencion de aminas.

Info

Publication number
ES2107885T3
ES2107885T3 ES95111954T ES95111954T ES2107885T3 ES 2107885 T3 ES2107885 T3 ES 2107885T3 ES 95111954 T ES95111954 T ES 95111954T ES 95111954 T ES95111954 T ES 95111954T ES 2107885 T3 ES2107885 T3 ES 2107885T3
Authority
ES
Spain
Prior art keywords
cpds
contg
calculated
procedure
amines
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95111954T
Other languages
English (en)
Inventor
Wolfgang Dr Reif
Lothar Dr Franz
Peter Stops
Volkmar Dr Menger
Siegfried Dr Winderl
Rainer Dr Becker
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2107885T3 publication Critical patent/ES2107885T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/03—Monoamines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/18—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
    • C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
    • C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/885—Molybdenum and copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Steroid Compounds (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCESO PARA LA ELABORACION DE AMINAS A PARTIR DE ALCOHOLES PRIMARIOS O SECUNDARIOS Y COMPUESTOS DE NITROGENO, ELEGIDOS A PARTIR DEL GRUPO DE AMONIACO, AMINA PRIMARIA Y SECUNDARIA, EN TEMPERATURAS DESDE 80 HASTA 250 IA DE UN CATALIZADOR DE CIRCONIO, COBRE, NIQUEL, QUE SE CARACTERIZA DE TAL MODO, QUE LA MASA ACTIVA CATALITICA ALCANZA DESDE 20 HASTA 85 % EN PESO DE LOS COMPUESTOS DE ZIRCONIO CONTENIENDO OXIGENO, CALCULADO COMO ZRO{SUB,2}, 1 HASTA 30 % EN PESO DE COMPUESTOS QUE CONTIENEN OXIGENO DE COBRE, CALCULADO COMO CUO, 30 HASTA 70 % EN PESO DE COMPUESTOS QUE CONTIENEN OXIGENO DE NIQUEL, CALCULADO COMO NIO, 0,1 HASTA 5 % EN PESO DE COMPUESTO QUE CONTIENE OXIGENO DEL MOLIBDENO, CALCULADO COMO MOO{SUB,3} Y 0 HASTA 10 % EN PESO DE COMPUESTOS QUE CONTIENEN OXIGENO DE ALUMINIO Y/O MANGANESO, CALCULADOS COMO AL{SUB,2}O{SUB,3} O MNO{SUB,2}. CON PREFERENCIA SE REFIERE A LA ELABORACION DE AMINAS DE LA FORMULA GENERAL I DONDE R{SUP,1} Y R{SUP,2} SIGNIFICAN HIDROGENO, C{SUB,1} - HASTA C{SUB,20} - ALQUILO, C{SUB,3} - HASTA C{SUB,12} - CICLOALQUILO, ARILO, C{SUB,7} - HASTA C{SUB,20} - ARALQUILO Y C{SUB,7} - HASTA C{SUB,20} - ALQUILOARILO O CONJUNTAMENTE (CH{SUB,2}){SUB,L} - X (CH{SUB,2}){SUB,M}, R{SUP,3} Y R{SUB,4} SON HIDROGENO, C{SUB,1} - HASTA C{SUB,20} - ALQUILO, C{SUB,3} HASTA C{SUB,12} - CICLOALQUILO, C{SUB,1} - HASTA C{SUB,20} - HIDROXIALQUILO, C{SUB,1} HASTA C{SUB,20} - ALQUILO SUSTITUIDO POR AMINO Y/O HIDROXI, C{SUB,2} - HASTA C{SUB,30} - ALCOXIALQUILO, R{SUP,5} - (OCR{SUP,6}R{SUP,7}C R{SUB,8}R{SUP,9}){SUB,N} (OCR{SUP,6}R{SUP,7}), ARILO, C{SUB,7} - HASTA C{SUB,20} - ARALQUILO, C{SUB,7} - HASTA C{SUB,20} - ALQUILOARILO, (R{SUP,5}){SUB,2}N - (CH{SUB,2}){SUB,Q} Y Y (CH{SUB,2}{SUB,M} - NR{SUP,5} - (CH{SUB,2}){SUB,Q} O CONJUNTAMENTE (CH{SUB,2}){SUB,L} - X - (CH{SUB,2})M O R{SUP,2} Y R{SUP,4} CONJUNTAMENTE SON (CH{SUB,2}){SUB,L} - X - (CH{SUB,2}){SUB,M}, R{SUP,5} SIGNIFICA HIDROGENO, C{SUB,1} - HASTA C{SUB,4} - ALQUILO, C{SUB,12} - HASTA C{SUB,40} - ALQUILOFENILO, R{SUP,6},R{SUP,7},R{SUP,8},R{SUP,9} SON HIDROGENO, METILO Y ETILO, R{SUP,10} ES HIDROGENO, C{SUB,1} - C{SUB,4} - ALQUILO, X ES CH{SUB,2}, OXIGENO O N - R{SUP,6}, Y ES N(R{SUP,5}){SUB,2}, HIDROXI, C{SUB,2} - HASTA C{SUB,20} - ALQUILAMINO ALQUILO O C{SUB,3} - HASTA C{SUB,20} - DIALQUILAMINO ALQUILO, N ES UNA CIFRA COMPLETA DE 1 HASTA 30, L ES UNA CIFRA COMPLETA DE 2 HASTA 4, M, Q SON UNA CIFRA COMPLETA DESDE 1 HASTA 4 A PARTIR DE ALCOHOLES PRIMARIOS O SECUNDARIOS DE LA FORMULA GENERAL II Y COMPUESTOS DE NITROGENO DE LA FORMULA GENERAL III EN DONDE R{SUP,1}, R{SUP,2} ASI COMO R{SUP,3} Y R{SUP,4} TIENEN EL SIGNIFICADO ANTES CONOCIDO.
ES95111954T 1994-08-08 1995-07-29 Procedimiento para la obtencion de aminas. Expired - Lifetime ES2107885T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4428004A DE4428004A1 (de) 1994-08-08 1994-08-08 Verfahren zur Herstellung von Aminen

Publications (1)

Publication Number Publication Date
ES2107885T3 true ES2107885T3 (es) 1997-12-01

Family

ID=6525167

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95111954T Expired - Lifetime ES2107885T3 (es) 1994-08-08 1995-07-29 Procedimiento para la obtencion de aminas.

Country Status (11)

Country Link
US (1) US5530127A (es)
EP (1) EP0696572B1 (es)
JP (1) JP3809963B2 (es)
KR (1) KR100376641B1 (es)
CN (1) CN1078200C (es)
AT (1) ATE158788T1 (es)
CA (1) CA2155171C (es)
DE (2) DE4428004A1 (es)
DK (1) DK0696572T3 (es)
ES (1) ES2107885T3 (es)
ZA (1) ZA956574B (es)

Families Citing this family (176)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4429547A1 (de) * 1994-08-19 1996-02-22 Basf Ag Verfahren zur Herstellung von Aminen
DE19516940A1 (de) * 1995-05-09 1996-11-14 Rwe Dea Ag Herstellung von primären Guerbetaminen
JP3361414B2 (ja) * 1995-09-22 2003-01-07 花王株式会社 Ｎ，ｎ−ジメチル−ｎ−アルキルもしくはアルケニルアミンの製造方法
US5679862A (en) * 1996-03-25 1997-10-21 Chemical Research & Licensing Company Amination process
DE19645430A1 (de) * 1996-11-04 1998-05-07 Basf Ag Polyolefine und deren funktionalisierte Derivate
DE19742911A1 (de) * 1997-09-29 1999-04-01 Basf Ag Verfahren zur Herstellung von Aminen
DE19905837A1 (de) * 1999-02-12 2000-08-17 Basf Ag Verfahren zur Racemisierung von optisch aktiven Aminen
DE19910960A1 (de) * 1999-03-12 2000-09-14 Basf Ag Verfahren zur Herstellung von Aminen
DE19916512A1 (de) * 1999-04-13 2000-10-19 Basf Ag Polyalkenalkohol-Polyetheramine und deren Verwendung in Kraft- und Schmierstoffen
EP1106601B1 (de) * 1999-12-06 2004-02-25 Basf Aktiengesellschaft Verfahren zur Herstellung von Monoisopropylamin
ATE272605T1 (de) 1999-12-06 2004-08-15 Basf Ag Verfahren zur herstellung von aminen
DE10145119A1 (de) 2001-09-13 2003-04-03 Basf Ag Verfahren zur Herstellung von Aminen
US7196033B2 (en) 2001-12-14 2007-03-27 Huntsman Petrochemical Corporation Advances in amination catalysis
DE10211101A1 (de) 2002-03-14 2003-09-25 Basf Ag Katalysatoren und Verfahren zur Herstellung von Aminen
DE10261193A1 (de) 2002-12-20 2004-07-01 Basf Ag Verfahren zur Herstellung eines Armins
DE10261195A1 (de) * 2002-12-20 2004-07-01 Basf Ag Verfahren zur Herstellung eines symmetrischen sekundären Amins
US7339080B2 (en) 2003-09-10 2008-03-04 Basf Aktiengesellschaft Method for the production of diaminoxylene by continuous hydrogenation of liquid phthalonitrile
DE10361503A1 (de) 2003-12-23 2005-07-28 Basf Ag Verfahren zur Herstellung eines Ethylamins
DE102004062253A1 (de) * 2004-12-23 2006-07-06 Basf Ag Direktaminierung von Kohlenwasserstoffen
DE102005029932A1 (de) 2005-06-28 2007-01-11 Clariant Produkte (Deutschland) Gmbh Verfahren zur Herstellung von Polyetheraminen
US7728174B2 (en) 2005-08-02 2010-06-01 Basf Se Continuous hydrogenation processes for the preparation of xylylenediamines
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JP4989889B2 (ja) 2005-12-28 2012-08-01 花王株式会社 含窒素化合物の製造方法
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US8063239B2 (en) 2006-05-09 2011-11-22 Basf Se Process for preparing aminoalkylnitriles and diamines from such nitriles
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US7754922B2 (en) 2006-07-14 2010-07-13 Basf Se Process for preparing amines and zirconium dioxide- and nickel-containing catalysts for use therein
CN101484105B (zh) * 2006-07-20 2012-04-18 Sca卫生产品股份公司 用于形成气流成网吸收芯体的设备和方法
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EP2079718B1 (de) * 2006-09-28 2010-04-07 Basf Se Verfahren zur kontinuierlichen destillativen auftrennung von gemischen enthaltend morpholin (mo), monoaminodiglykol (adg), ammoniak und wasser
JP5290181B2 (ja) 2006-09-28 2013-09-18 ビーエーエスエフ ソシエタス・ヨーロピア モルホリン（ｍｏ）、モノアミノジグリコール（ａｄｇ）、アンモニア及び水を含有する混合物を連続的に蒸留により分離するための方法
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CN101622224B (zh) 2007-03-01 2015-10-07 巴斯夫欧洲公司 借助eddn生产teta的新方法
KR20100014695A (ko) 2007-03-01 2010-02-10 바스프 에스이 테트라에틸렌펜타민의 제조 방법
RU2473537C2 (ru) 2007-03-01 2013-01-27 Басф Се Способ получения смеси этиленаминов
RU2478092C2 (ru) 2007-03-01 2013-03-27 Басф Се Способ получения смесей этиленаминов
WO2008104592A1 (de) 2007-03-01 2008-09-04 Basf Se Verfahren zur herstellung von ethylendiamin
EP2114861B1 (de) 2007-03-01 2012-09-05 Basf Se Verfahren zur herstellung von triethylentetraamin
JP2010520167A (ja) 2007-03-01 2010-06-10 ビーエーエスエフ ソシエタス・ヨーロピア 原料ａａｎからのエチレンアミンの製造方法
WO2009013192A1 (de) 2007-07-23 2009-01-29 Basf Se Verfahren zur herstellung von menthol durch hydrierung von isopulegol
EP2185499A1 (de) * 2007-08-29 2010-05-19 Basf Se Verfahren zur herstellung von aminen aus glycerin
CN101842346B (zh) 2007-08-29 2013-05-15 巴斯夫欧洲公司 由糖醇生产胺的方法
EP2225192B1 (de) 2007-11-30 2017-05-03 Basf Se Verfahren zur herstellung von optisch aktivem und racemischem menthol
WO2009080507A1 (de) 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
CN101903329B (zh) 2007-12-21 2014-11-05 巴斯夫欧洲公司 非对映选择性转化手性亚胺的方法
WO2009080514A1 (de) * 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
SG187393A1 (en) 2007-12-21 2013-02-28 Basf Se Process for preparing an amine
EP2225030B1 (de) 2007-12-21 2012-04-18 Basf Se Verfahren zur herstellung eines amins
CA2708315A1 (en) 2007-12-21 2009-07-02 Basf Se One-stage reductive amination
US8293945B2 (en) 2007-12-21 2012-10-23 Basf Se Method for producing an amine
WO2010009995A2 (de) 2008-07-25 2010-01-28 Basf Se 5-isopropyl-3-aminomethyl-2-methyl-1-amino-cyclohexan (carvondiamin) und ein verfahren zu dessen herstellung
US20110124919A1 (en) * 2008-07-25 2011-05-26 Basf Se 3-aminomethyl-1-cyclohexylamine, and method for the production thereof
RU2522761C2 (ru) 2008-11-05 2014-07-20 Басф Се Способ получения n, n-замещенных 3-аминопропан-1-олов
EP2393593A2 (de) 2009-02-09 2011-12-14 Basf Se Hydrierkatalysatoren, deren herstellung und verwendung
JP2012517333A (ja) 2009-02-09 2012-08-02 ビーエーエスエフ ソシエタス・ヨーロピア モノリス触媒の触媒活性を改善する方法
JP2012517331A (ja) 2009-02-09 2012-08-02 ビーエーエスエフ ソシエタス・ヨーロピア 水素化触媒、その製造方法およびその使用
WO2010103062A1 (de) * 2009-03-12 2010-09-16 Basf Se Verfahren zur herstellung von 1-adamantyltrimethylammoniumhydroxid
CN102803213B (zh) 2009-06-18 2015-05-13 巴斯夫欧洲公司 甲基取代的teta化合物
CN102029166B (zh) * 2009-09-27 2012-07-18 上海焦化有限公司 一种合成气制取低碳混合醇的催化剂及其制备方法
WO2011067199A1 (de) 2009-12-03 2011-06-09 Basf Se Katalysator und verfahren zur herstellung eines amins
JP5755237B2 (ja) 2009-12-03 2015-07-29 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 触媒及びアミンの製造方法
US8742174B2 (en) 2009-12-17 2014-06-03 Basf Se Method for preparing higher ethanolamines
PH12012501449B1 (en) * 2010-01-18 2017-12-13 Basf Se Compound comprising a pesticide and an alkoxylate of 2-propylheptyl amine
US8618179B2 (en) 2010-01-18 2013-12-31 Basf Se Composition comprising a pesticide and an alkoxylate of 2-propylheptylamine
WO2011101303A2 (de) 2010-02-16 2011-08-25 Basf Se Zusammensetzung umfassend ein pestizid und ein alkoxylat von iso-heptadecylamin
US20110201497A1 (en) * 2010-02-16 2011-08-18 Basf Se Composition Comprising A Pesticide and an Alkoxylate of Iso-Heptadecylamine
US8673275B2 (en) 2010-03-02 2014-03-18 Basf Se Block copolymers and their use
US20110218295A1 (en) * 2010-03-02 2011-09-08 Basf Se Anionic associative rheology modifiers
EP2542206B1 (de) 2010-03-02 2015-05-13 Basf Se Blockcopolymere und deren verwendung
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KR20130051927A (ko) 2010-03-17 2013-05-21 바스프 에스이 살충제 및 분지형 노닐 아민의 알콕실레이트를 포함하는 조성물
CN102906082A (zh) 2010-05-27 2013-01-30 巴斯夫欧洲公司 制备在2位上被取代的四氢吡喃醇的方法
US8779169B2 (en) 2010-05-27 2014-07-15 Basf Se Process for the preparation of 2 substituted tetrahydropyranols
US8791276B2 (en) 2010-06-10 2014-07-29 Basf Se Process for the preparation and isolation of 2-substituted tetrahydropyranols
US8637668B2 (en) 2010-06-15 2014-01-28 Basf Se Process for preparing a cyclic tertiary methylamine
WO2012000952A1 (de) 2010-06-30 2012-01-05 Basf Se Verfahren zur herstellung von tri-n-propylamin (tpa)
US8466322B2 (en) 2010-06-30 2013-06-18 Basf Se Process for preparing tri-n-propylamine (TPA)
DE102010040427A1 (de) 2010-09-08 2012-03-08 Basf Se Verfahren zur Herstellung von Mono-n-Octylamin (MOA)
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US8933223B2 (en) 2010-10-14 2015-01-13 Basf Se Process for preparing a cyclic tertiary amine
EP2635544B1 (de) 2010-11-02 2014-12-17 Basf Se Verfahren zur herstellung eines phenylcyclohexans
US8653313B2 (en) 2010-11-02 2014-02-18 Basf Se Process for preparing a phenylcyclohexane
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ATE158788T1 (de) 1997-10-15
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US5530127A (en) 1996-06-25
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CN1123789A (zh) 1996-06-05

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