ES2136661T3 - Procedimiento de produccion de acido tereftalico purificado. - Google Patents
Procedimiento de produccion de acido tereftalico purificado.Info
- Publication number
- ES2136661T3 ES2136661T3 ES93910240T ES93910240T ES2136661T3 ES 2136661 T3 ES2136661 T3 ES 2136661T3 ES 93910240 T ES93910240 T ES 93910240T ES 93910240 T ES93910240 T ES 93910240T ES 2136661 T3 ES2136661 T3 ES 2136661T3
- Authority
- ES
- Spain
- Prior art keywords
- cta
- mixture
- aqueous
- purified
- production procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title 1
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 5
- 239000012736 aqueous medium Substances 0.000 abstract 2
- 238000002425 crystallisation Methods 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000002347 injection Methods 0.000 abstract 1
- 239000007924 injection Substances 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
EL PROCESO PARA LA PRODUCCION DE ACIDO TEREFTALICO PURIFICADO (PTA) A PARTIR DEL ACIDO TEREFTALICO BRUTO (CTA) COMPRENDE MEZCLAR EL CTA CON UN MEDIO ACUOSO PARA FORMAR UNA MEZCLA CTA ACUOSA, CALENTAR LA MEZCLA QUE LLEVA TOTAL SUBSTANCIALMENTE DISUELTA LA CTA EN EL MEDIO ACUOSO POR INTRODUCCION EN LA MISMA DE VAPOR A UNA TEMPERATURA SUPERIOR A LA DE LA MEZCLA Y REDUCIR QUIMICAMENTE LAS IMPUREZAS EN LA SOLUCION ACUOSA DE CTA, SEGUIDO DE LA RECUPERACION DE PTA EN UN PROCESO DE CRISTALIZACION. EL VAPOR SE DERIVA DE LA CORRIENTE TIPICA DEL PROCESO DE CRISTALIZACION Y A PARTIR DE AHI SE INTRODUCE COMPLETAMENTE EN LA MEZCLA DE CTA ACUOSA POR MEDIO DE UN DISPOSITIVIO (30) DE INYECCION (FIG 2, FIG 3).
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB929211415A GB9211415D0 (en) | 1992-05-29 | 1992-05-29 | Process for the production of purified terephthalic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2136661T3 true ES2136661T3 (es) | 1999-12-01 |
Family
ID=10716228
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93910240T Expired - Lifetime ES2136661T3 (es) | 1992-05-29 | 1993-05-20 | Procedimiento de produccion de acido tereftalico purificado. |
Country Status (14)
| Country | Link |
|---|---|
| EP (1) | EP0642491B1 (es) |
| JP (1) | JPH07507292A (es) |
| CN (1) | CN1039315C (es) |
| AT (1) | ATE182877T1 (es) |
| AU (1) | AU668725B2 (es) |
| BR (1) | BR9306418A (es) |
| CA (1) | CA2134873A1 (es) |
| DE (1) | DE69325905T2 (es) |
| ES (1) | ES2136661T3 (es) |
| GB (2) | GB9211415D0 (es) |
| IN (1) | IN186258B (es) |
| RU (1) | RU94046087A (es) |
| WO (1) | WO1993024441A1 (es) |
| ZA (1) | ZA933572B (es) |
Families Citing this family (64)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5504121A (en) * | 1992-05-18 | 1996-04-02 | Swig Pty Ltd. | Polyethylene terephthalate decontamination |
| US5602187A (en) * | 1992-05-18 | 1997-02-11 | Swig Pty Ltd. | Polyethylene terephthalate decontamination |
| US5922775A (en) * | 1997-10-23 | 1999-07-13 | Octamer, Inc. | Method of treating malignant tumors with ketone thyroxine analogues having no significant hormonal activity |
| AU2003292831A1 (en) * | 2003-01-08 | 2004-08-10 | Mitsubishi Chemical Corporation | Method for producing high purity terephthalic acid |
| US7410632B2 (en) | 2003-06-05 | 2008-08-12 | Eastman Chemical Company | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
| US7381386B2 (en) | 2003-06-05 | 2008-06-03 | Eastman Chemical Company | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
| US7452522B2 (en) | 2003-06-05 | 2008-11-18 | Eastman Chemical Company | Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid |
| US7351396B2 (en) | 2003-06-05 | 2008-04-01 | Eastman Chemical Company | Extraction process for removal of impurities from an aqueous mixture |
| US7282151B2 (en) | 2003-06-05 | 2007-10-16 | Eastman Chemical Company | Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration |
| US7494641B2 (en) | 2003-06-05 | 2009-02-24 | Eastman Chemical Company | Extraction process for removal of impurities from an oxidizer purge stream in the synthesis of carboxylic acid |
| WO2006001449A1 (ja) * | 2004-06-28 | 2006-01-05 | Mitsubishi Chemical Corporation | 高純度テレフタル酸の製造方法 |
| US7399882B2 (en) | 2004-09-02 | 2008-07-15 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7608732B2 (en) | 2005-03-08 | 2009-10-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7495125B2 (en) | 2004-09-02 | 2009-02-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7582793B2 (en) | 2004-09-02 | 2009-09-01 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7608733B2 (en) | 2004-09-02 | 2009-10-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| MX359077B (es) * | 2004-09-02 | 2018-09-13 | Grupo Petrotemex Sa De Cv | Produccion optimizada de acidos dicarboxilicos aromaticos. |
| US7692036B2 (en) | 2004-11-29 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7563926B2 (en) | 2004-09-02 | 2009-07-21 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7692037B2 (en) | 2004-09-02 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7683210B2 (en) | 2004-09-02 | 2010-03-23 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7381836B2 (en) | 2004-09-02 | 2008-06-03 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7897810B2 (en) | 2004-09-02 | 2011-03-01 | Eastman Chemical Company | Optimized production of aromatic dicarboxylic acids |
| US7888530B2 (en) | 2004-09-02 | 2011-02-15 | Eastman Chemical Company | Optimized production of aromatic dicarboxylic acids |
| US7568361B2 (en) | 2004-09-02 | 2009-08-04 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7504535B2 (en) | 2004-09-02 | 2009-03-17 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7589231B2 (en) | 2004-09-02 | 2009-09-15 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| BRPI0514756A (pt) * | 2004-09-02 | 2008-06-24 | Eastman Chem Co | processo para produzir ácidos dicarboxìlicos aromáticos, e, aparelhagem |
| US20070238899A9 (en) | 2004-09-02 | 2007-10-11 | Robert Lin | Optimized production of aromatic dicarboxylic acids |
| US7572936B2 (en) | 2004-09-02 | 2009-08-11 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7572932B2 (en) | 2004-09-02 | 2009-08-11 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7371894B2 (en) | 2004-09-02 | 2008-05-13 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7741515B2 (en) | 2004-09-02 | 2010-06-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7482482B2 (en) | 2004-09-02 | 2009-01-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7390921B2 (en) | 2004-09-02 | 2008-06-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7507857B2 (en) | 2004-09-02 | 2009-03-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7586000B2 (en) | 2004-09-02 | 2009-09-08 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7291270B2 (en) | 2004-10-28 | 2007-11-06 | Eastman Chemical Company | Process for removal of impurities from an oxidizer purge stream |
| US7273559B2 (en) | 2004-10-28 | 2007-09-25 | Eastman Chemical Company | Process for removal of impurities from an oxidizer purge stream |
| US7557243B2 (en) | 2005-05-19 | 2009-07-07 | Eastman Chemical Company | Enriched terephthalic acid composition |
| US7432395B2 (en) | 2005-05-19 | 2008-10-07 | Eastman Chemical Company | Enriched carboxylic acid composition |
| US7304178B2 (en) | 2005-05-19 | 2007-12-04 | Eastman Chemical Company | Enriched isophthalic acid composition |
| US7741516B2 (en) | 2005-05-19 | 2010-06-22 | Eastman Chemical Company | Process to enrich a carboxylic acid composition |
| US7884231B2 (en) | 2005-05-19 | 2011-02-08 | Eastman Chemical Company | Process to produce an enriched composition |
| US7834208B2 (en) | 2005-05-19 | 2010-11-16 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
| US7880031B2 (en) | 2005-05-19 | 2011-02-01 | Eastman Chemical Company | Process to produce an enrichment feed |
| US7919652B2 (en) | 2005-05-19 | 2011-04-05 | Eastman Chemical Company | Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone |
| US7897809B2 (en) | 2005-05-19 | 2011-03-01 | Eastman Chemical Company | Process to produce an enrichment feed |
| US7884232B2 (en) | 2005-06-16 | 2011-02-08 | Eastman Chemical Company | Optimized liquid-phase oxidation |
| US7569722B2 (en) | 2005-08-11 | 2009-08-04 | Eastman Chemical Company | Process for removal of benzoic acid from an oxidizer purge stream |
| US7402694B2 (en) | 2005-08-11 | 2008-07-22 | Eastman Chemical Company | Process for removal of benzoic acid from an oxidizer purge stream |
| US7358389B2 (en) | 2006-01-04 | 2008-04-15 | Eastman Chemical Company | Oxidation system employing internal structure for enhanced hydrodynamics |
| US7355068B2 (en) | 2006-01-04 | 2008-04-08 | Eastman Chemical Company | Oxidation system with internal secondary reactor |
| US7888529B2 (en) | 2006-03-01 | 2011-02-15 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
| US7897808B2 (en) | 2006-03-01 | 2011-03-01 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
| US20070203359A1 (en) | 2006-03-01 | 2007-08-30 | Philip Edward Gibson | Versatile oxidation byproduct purge process |
| US7863481B2 (en) | 2006-03-01 | 2011-01-04 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
| US7880032B2 (en) | 2006-03-01 | 2011-02-01 | Eastman Chemical Company | Versatile oxidation byproduct purge process |
| RU2525914C2 (ru) * | 2008-10-31 | 2014-08-20 | Инвиста Текнолоджиз С.А.Р.Л. | Улучшенный способ фильтрования очищенной карбоновой кислоты |
| GB201016049D0 (en) * | 2010-09-24 | 2010-11-10 | Davy Process Techn Ltd | Process and system |
| CN103121940B (zh) * | 2011-11-18 | 2015-11-18 | 中国石油化工股份有限公司 | 加氢处理粗间苯二甲酸方法 |
| DE102012007675A1 (de) * | 2012-04-17 | 2013-10-17 | BOKELA Ingenieurgesellschaft für mechanische Verfahrenstechnik mbH | Verfahren und Anlage zum Herstellen von TA(Terephtalsäure) |
| BR112016015320A2 (pt) | 2013-12-30 | 2017-10-10 | Bp Corp North America Inc | misturas de alimentação de ácido carboxílico aromático bruto pressurizado |
| KR102172131B1 (ko) * | 2013-12-31 | 2020-10-30 | 비피 코포레이션 노쓰 아메리카 인코포레이티드 | 정제된 방향족 카르복실산들의 제조시 고압 응축물 생성 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3522298A (en) * | 1966-03-30 | 1970-07-28 | Mobil Oil Corp | Terephthalic acid purification process |
| DE2601431A1 (de) * | 1976-01-16 | 1977-07-21 | Wiegand Karlsruhe Gmbh | Direkt-dampf-injektionsgeraet |
| US4405809A (en) * | 1981-12-04 | 1983-09-20 | Standard Oil Company (Indiana) | Process for the manufacture of aromatic polycarboxylic acids having delta Y values below ten |
| US4500732A (en) * | 1983-09-15 | 1985-02-19 | Standard Oil Company (Indiana) | Process for removal and recycle of p-toluic acid from terephthalic acid crystallizer solvent |
-
1992
- 1992-05-29 GB GB929211415A patent/GB9211415D0/en active Pending
-
1993
- 1993-05-17 GB GB939310094A patent/GB9310094D0/en active Pending
- 1993-05-20 WO PCT/GB1993/001033 patent/WO1993024441A1/en not_active Ceased
- 1993-05-20 DE DE69325905T patent/DE69325905T2/de not_active Expired - Lifetime
- 1993-05-20 CA CA002134873A patent/CA2134873A1/en not_active Abandoned
- 1993-05-20 JP JP6500293A patent/JPH07507292A/ja active Pending
- 1993-05-20 AT AT93910240T patent/ATE182877T1/de active
- 1993-05-20 EP EP93910240A patent/EP0642491B1/en not_active Expired - Lifetime
- 1993-05-20 IN IN521DE1993 patent/IN186258B/en unknown
- 1993-05-20 BR BR9306418A patent/BR9306418A/pt not_active Application Discontinuation
- 1993-05-20 ES ES93910240T patent/ES2136661T3/es not_active Expired - Lifetime
- 1993-05-20 AU AU40825/93A patent/AU668725B2/en not_active Ceased
- 1993-05-20 RU RU94046087/04A patent/RU94046087A/ru unknown
- 1993-05-21 ZA ZA933572A patent/ZA933572B/xx unknown
- 1993-05-29 CN CN93108224A patent/CN1039315C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ATE182877T1 (de) | 1999-08-15 |
| AU668725B2 (en) | 1996-05-16 |
| EP0642491B1 (en) | 1999-08-04 |
| CN1039315C (zh) | 1998-07-29 |
| ZA933572B (en) | 1994-02-14 |
| AU4082593A (en) | 1993-12-30 |
| DE69325905D1 (de) | 1999-09-09 |
| JPH07507292A (ja) | 1995-08-10 |
| CA2134873A1 (en) | 1993-12-09 |
| DE69325905T2 (de) | 2000-03-30 |
| CN1085891A (zh) | 1994-04-27 |
| RU94046087A (ru) | 1996-09-27 |
| GB9310094D0 (en) | 1993-06-30 |
| EP0642491A1 (en) | 1995-03-15 |
| IN186258B (es) | 2001-07-21 |
| WO1993024441A1 (en) | 1993-12-09 |
| GB9211415D0 (en) | 1992-07-15 |
| BR9306418A (pt) | 1998-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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