ES2171793T3 - Procedimiento para la separacion de un producto de una reaccion de oxidacion y de un catalizador de oxidacion. - Google Patents

Procedimiento para la separacion de un producto de una reaccion de oxidacion y de un catalizador de oxidacion.

Info

Publication number
ES2171793T3
ES2171793T3 ES97113920T ES97113920T ES2171793T3 ES 2171793 T3 ES2171793 T3 ES 2171793T3 ES 97113920 T ES97113920 T ES 97113920T ES 97113920 T ES97113920 T ES 97113920T ES 2171793 T3 ES2171793 T3 ES 2171793T3
Authority
ES
Spain
Prior art keywords
sup
solvent
oxidation
oxidation catalyst
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97113920T
Other languages
English (en)
Inventor
Naruhisa Hirai
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daicel Corp
Original Assignee
Daicel Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd
Application granted granted Critical
Publication of ES2171793T3 publication Critical patent/ES2171793T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B33/00—Oxidation in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/58—Ring systems containing bridged rings containing three rings
    • C07C2603/70—Ring systems containing bridged rings containing three rings containing only six-membered rings
    • C07C2603/74—Adamantanes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

SE SEPARAN EFICIENTEMENTE UNA MEZCLA DE REACCION DE OXIDACION (P.EJ. ACIDO ADIPICO, ACIDO BENZOICO, BUTANODIOL) Y UN CATALIZADOR DE OXIDACION, A PARTIR DE UNA MEZCLA DE REACCION, MEDIANTE LA UTILIZACION DE UN DISOLVENTE ACUOSO (P.EJ. BENZOATO DE METILO, BENZONITRILO) QUE CONTIENE AL MENOS AGUA Y UN DISOLVENTE NO HIDROSOLUBLE, SEPARABLE DEL DISOLVENTE ACUOSO. LA MEZCLA DE REACCION SE OBTIENE OXIDANDO UN SUSTRATO (P.EJ. HIDROCARBURO), EN PRESENCIA DE UN COMPUESTO IMIDA, P.EJ. UNA N HIDROXIFTALIMIDA, REPRESENTADA POR LA SIGUIENTE FORMULA (1), COMO CATALIZADOR DE OXIDACION, DONDE R SUP,1} Y R SUP,2} REPRESENTAN UN SUSTITUYENTE, COMO UN ATOMO DE HIDROGENO Y UN ATOMO DE HALOGENO; R SUP,1} Y R SUP,2} PUEDEN FORMAR, CONJUNTAMENTE, UN ENLACE DOBLE O UN CICLO AROMATICO O NO AROMATICO DE 5-12 MIEMBROS; X REPRESENTA O O OH; Y N ES UN NUMERO COMPRENDIDO ENTRE 1 Y 3. NO SE OBSERVA DESCOMPOSICION DEL CATALIZADOR EN EL CITADO PROCEDIMIENTO DE SEPARACION.
ES97113920T 1996-08-20 1997-08-12 Procedimiento para la separacion de un producto de una reaccion de oxidacion y de un catalizador de oxidacion. Expired - Lifetime ES2171793T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP21869396 1996-08-20

Publications (1)

Publication Number Publication Date
ES2171793T3 true ES2171793T3 (es) 2002-09-16

Family

ID=16723941

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97113920T Expired - Lifetime ES2171793T3 (es) 1996-08-20 1997-08-12 Procedimiento para la separacion de un producto de una reaccion de oxidacion y de un catalizador de oxidacion.

Country Status (9)

Country Link
US (1) US6515171B1 (es)
EP (1) EP0825165B1 (es)
KR (1) KR100553280B1 (es)
CN (1) CN1093525C (es)
DE (1) DE69709587T2 (es)
ES (1) ES2171793T3 (es)
ID (1) ID18044A (es)
MY (1) MY125690A (es)
SG (1) SG60101A1 (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0003180D0 (en) * 2000-02-12 2000-04-05 Albright & Wilson Uk Ltd Catalyst recovery
DE60143516D1 (de) 2000-04-04 2011-01-05 Daicel Chem Verfahren zur trennung einer imidverbindung
JP4524020B2 (ja) * 2000-04-04 2010-08-11 ダイセル化学工業株式会社 イミド系触媒の再生方法及びイミド系触媒を用いた製造プロセス
US6555004B2 (en) 2000-05-02 2003-04-29 Sumitomo Chemical Company, Limited Method for separating catalyst, product and solvent
JP4651181B2 (ja) * 2000-11-01 2011-03-16 ダイセル化学工業株式会社 反応生成物と触媒との分離方法
US6814867B2 (en) * 2002-09-12 2004-11-09 Inuista North America S.à.r.l. Process for reducing chromium in nonvolatile residue resulting from air oxidation of cyclohexane
CN102701959B (zh) * 2012-06-05 2014-07-02 山东大学 一种从ta残渣中提取苯甲酸的新方法
CN103924007B (zh) * 2014-04-18 2015-10-14 厦门大学 一类弱极性酸双液相催化纤维素水解制备葡萄糖的方法
CN105418375B (zh) * 2014-08-27 2018-01-05 湖南中创化工股份有限公司 一种异丁烷氧化制备叔丁醇的方法
CN109678723B (zh) * 2018-12-03 2021-12-10 浙江工业大学 一种取代苯甲酸类化合物的制备方法
DE202019104992U1 (de) * 2019-09-10 2020-12-15 Mr Chemie Gmbh Cycloaliphatische Diole und/oder Diketone enthaltende Mattierungskomponente zur reversiblen Oberflächenbeschichtung und Zusammensetzungen enthaltend die Mattierungskomponente
CN111992133B (zh) * 2020-09-22 2021-11-12 陕西科技大学 一种三羧基两性表面活性剂及制备方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DK173704B1 (da) * 1985-04-17 2001-07-09 Hoffmann La Roche Fremgangsmåde til katalytisk oxidation af allyliske grupper
JP3434034B2 (ja) * 1994-08-02 2003-08-04 ダイセル化学工業株式会社 酸化触媒およびそれを用いた酸化方法

Also Published As

Publication number Publication date
EP0825165A2 (en) 1998-02-25
EP0825165B1 (en) 2002-01-16
ID18044A (id) 1998-02-19
CN1093525C (zh) 2002-10-30
US6515171B1 (en) 2003-02-04
KR100553280B1 (ko) 2007-01-18
MY125690A (en) 2006-08-30
SG60101A1 (en) 1999-02-22
DE69709587T2 (de) 2002-06-13
EP0825165A3 (en) 1998-04-15
CN1174828A (zh) 1998-03-04
KR19980018752A (ko) 1998-06-05
DE69709587D1 (de) 2002-02-21

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