ES2174497T3 - Procedimiento continuo para la fabricacion de aminas aromaticas. - Google Patents
Procedimiento continuo para la fabricacion de aminas aromaticas.Info
- Publication number
- ES2174497T3 ES2174497T3 ES98951488T ES98951488T ES2174497T3 ES 2174497 T3 ES2174497 T3 ES 2174497T3 ES 98951488 T ES98951488 T ES 98951488T ES 98951488 T ES98951488 T ES 98951488T ES 2174497 T3 ES2174497 T3 ES 2174497T3
- Authority
- ES
- Spain
- Prior art keywords
- manufacture
- compounds
- aromatic amines
- hydrogen
- aromatic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000004982 aromatic amines Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- ZXVONLUNISGICL-UHFFFAOYSA-N 4,6-dinitro-o-cresol Chemical group CC1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1O ZXVONLUNISGICL-UHFFFAOYSA-N 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 2
- 150000004984 aromatic diamines Chemical class 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 229920000768 polyamine Polymers 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimiento continuo para la fabricación de diaminas y/o poliaminas aromáticas mediante la hidrogenación catalítica de los dinitrocompuestos y/o polinitrocompuestos aromáticos correspondientes con hidrógeno, caracterizado porque en un reactor con lecho catalítico fijo o con lecho de rociado, a una presión en el intervalo entre 5 y 100 bar y a una temperatura de reacción en el intervalo de 100 hasta 220 C, a) se incorporan en una corriente de producto, compuesta sustancialmente por el producto de hidrogenación retornado, por agua y por hidrógeno, los dinitrocompuestos y/o polinitrocompuestos aromáticos y b) el calor de la reacción se evacua mediante un intercambiador de calor exterior y c) una parte de la corriente del producto se retira de forma continua del sistema de reactor.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19745465A DE19745465A1 (de) | 1997-10-15 | 1997-10-15 | Kontinuierliches Verfahren zur Herstellung von aromatischen Aminen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2174497T3 true ES2174497T3 (es) | 2002-11-01 |
Family
ID=7845567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES98951488T Expired - Lifetime ES2174497T3 (es) | 1997-10-15 | 1998-10-02 | Procedimiento continuo para la fabricacion de aminas aromaticas. |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP1023261B1 (es) |
| KR (1) | KR100566450B1 (es) |
| CN (1) | CN1165513C (es) |
| AU (1) | AU9748298A (es) |
| BR (1) | BR9813052A (es) |
| CA (1) | CA2306935A1 (es) |
| DE (2) | DE19745465A1 (es) |
| ES (1) | ES2174497T3 (es) |
| TW (1) | TW443998B (es) |
| WO (1) | WO1999019292A1 (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1318602B1 (it) * | 2000-06-29 | 2003-08-27 | Enichem Spa | Procedimento per la produzione di ammine aromatiche. |
| US6521791B1 (en) | 2001-11-09 | 2003-02-18 | Air Products And Chemicals, Inc. | Process for regenerating a monolith hydrogenation catalytic reactor |
| WO2025176643A1 (en) * | 2024-02-19 | 2025-08-28 | Basf Se | Combined nitro compound hydrogenation and catalyst regeneration process; process for catalyst activation; catalysts obtained by these processes and their use in nitro compound hydrogenation; reaction system |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2135155A1 (de) * | 1971-07-14 | 1973-02-22 | Bayer Ag | Katalysator zur reduktion von nitroverbindungen |
| DE3315191A1 (de) * | 1983-04-27 | 1984-10-31 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen herstellung von aromatischen diaminen unter gleichzeitiger erzeugung von dampf |
| DE4323687A1 (de) * | 1993-07-15 | 1995-01-19 | Bayer Ag | Kontinuierliches Verfahren zur Herstellung von aromatischen Aminen |
| DE4428017A1 (de) * | 1994-08-08 | 1996-02-15 | Bayer Ag | Verfahren zur Herstellung von aromatischen Aminen |
| FR2741877B1 (fr) * | 1995-12-01 | 1998-02-13 | Rhone Poulenc Chimie | Procede d'hydrogenation de composes nitres aromatiques |
-
1997
- 1997-10-15 DE DE19745465A patent/DE19745465A1/de not_active Withdrawn
-
1998
- 1998-09-25 TW TW087115933A patent/TW443998B/zh not_active IP Right Cessation
- 1998-10-02 CA CA002306935A patent/CA2306935A1/en not_active Abandoned
- 1998-10-02 BR BR9813052-8A patent/BR9813052A/pt not_active IP Right Cessation
- 1998-10-02 EP EP98951488A patent/EP1023261B1/de not_active Expired - Lifetime
- 1998-10-02 AU AU97482/98A patent/AU9748298A/en not_active Abandoned
- 1998-10-02 ES ES98951488T patent/ES2174497T3/es not_active Expired - Lifetime
- 1998-10-02 CN CNB988102986A patent/CN1165513C/zh not_active Expired - Fee Related
- 1998-10-02 WO PCT/EP1998/006275 patent/WO1999019292A1/de not_active Ceased
- 1998-10-02 KR KR1020007003984A patent/KR100566450B1/ko not_active Expired - Fee Related
- 1998-10-02 DE DE59803298T patent/DE59803298D1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| BR9813052A (pt) | 2000-08-15 |
| TW443998B (en) | 2001-07-01 |
| DE59803298D1 (de) | 2002-04-11 |
| AU9748298A (en) | 1999-05-03 |
| CN1276780A (zh) | 2000-12-13 |
| KR20010015758A (ko) | 2001-02-26 |
| EP1023261A1 (de) | 2000-08-02 |
| KR100566450B1 (ko) | 2006-03-31 |
| CN1165513C (zh) | 2004-09-08 |
| HK1033304A1 (en) | 2001-08-24 |
| WO1999019292A1 (de) | 1999-04-22 |
| CA2306935A1 (en) | 1999-04-22 |
| EP1023261B1 (de) | 2002-03-06 |
| DE19745465A1 (de) | 1999-04-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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