ES2177409A1 - Procedimiento para la obtencion de 1,4-dihidropiridinas substituida utiles para el tratamiento de la hipertension. - Google Patents
Procedimiento para la obtencion de 1,4-dihidropiridinas substituida utiles para el tratamiento de la hipertension.Info
- Publication number
- ES2177409A1 ES2177409A1 ES200001967A ES200001967A ES2177409A1 ES 2177409 A1 ES2177409 A1 ES 2177409A1 ES 200001967 A ES200001967 A ES 200001967A ES 200001967 A ES200001967 A ES 200001967A ES 2177409 A1 ES2177409 A1 ES 2177409A1
- Authority
- ES
- Spain
- Prior art keywords
- treatment
- acetoacetate
- production
- pyridine derivatives
- evaporation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 206010020772 Hypertension Diseases 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000003222 pyridines Chemical class 0.000 title abstract 2
- WDJHALXBUFZDSR-UHFFFAOYSA-M acetoacetate Chemical compound CC(=O)CC([O-])=O WDJHALXBUFZDSR-UHFFFAOYSA-M 0.000 title 1
- RLKBOGLIOLFMEK-NSCUHMNNSA-N amino (e)-but-2-enoate Chemical compound C\C=C\C(=O)ON RLKBOGLIOLFMEK-NSCUHMNNSA-N 0.000 title 1
- 230000008020 evaporation Effects 0.000 title 1
- 238000001704 evaporation Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 title 1
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- YNGDWRXWKFWCJY-UHFFFAOYSA-N 1,4-Dihydropyridine Chemical class C1C=CNC=C1 YNGDWRXWKFWCJY-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Pyridine Compounds (AREA)
Abstract
Procedimiento para la obtención de 1,4-Dihidropiridinas substituidas útiles para el tratamiento de la hipertensión. El procedimiento se caracteriza por el hecho de que comprende la reacción entre un 2-metilidenacetoacetato de alquilo de fórmula V y un 3-aminocrotonato de alquilo de fórmula VI adsorbidos sobre una superficie sólida. Ventajosamente dicha superficie sólida es un agente poroso. El procedimiento comprende (a) adsorber dichos reactivos sobre dicho agente poroso mediante: (i) la disolución de dichos reactivos en un disolvente orgánico; (ii) la adición de dicho agente poroso; y (iii) la evaporación de dicho disolvente a sequedad; (b) calentar el sólido resultante de la etapa anterior; (c) extraer el producto; y (d) purificar el producto.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200001967A ES2177409B1 (es) | 2000-08-02 | 2000-08-02 | Procedimiento para la obtencion de 1,4-dihidropiridinas substituida utiles para el tratamiento de la hipertension. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200001967A ES2177409B1 (es) | 2000-08-02 | 2000-08-02 | Procedimiento para la obtencion de 1,4-dihidropiridinas substituida utiles para el tratamiento de la hipertension. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2177409A1 true ES2177409A1 (es) | 2002-12-01 |
| ES2177409B1 ES2177409B1 (es) | 2003-08-01 |
Family
ID=8494565
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES200001967A Expired - Fee Related ES2177409B1 (es) | 2000-08-02 | 2000-08-02 | Procedimiento para la obtencion de 1,4-dihidropiridinas substituida utiles para el tratamiento de la hipertension. |
Country Status (1)
| Country | Link |
|---|---|
| ES (1) | ES2177409B1 (es) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7671208B2 (en) | 2007-03-30 | 2010-03-02 | Esteve Quimica, S.A. | Acetone solvate of phthaloyl amlodipine |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2009136A6 (es) * | 1985-08-06 | 1989-09-01 | Boehringer Biochemia Srl | Un compuesto |
| ES2055652A1 (es) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedimiento de obtencion de 2,6-dimetil-4-(2,3-diclorofenil)-1,4-dihidropiridin-3,5-dicarboxilato de 3-etil-5-metil. |
| ES2055655A1 (es) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedimiento de obtencion de 2,6-dimetil-4-(2-nitrofenil)-1,4-dihidropiridin-3,5-dicarboxilato de 3-isobutil-5-metil. |
-
2000
- 2000-08-02 ES ES200001967A patent/ES2177409B1/es not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2009136A6 (es) * | 1985-08-06 | 1989-09-01 | Boehringer Biochemia Srl | Un compuesto |
| ES2055652A1 (es) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedimiento de obtencion de 2,6-dimetil-4-(2,3-diclorofenil)-1,4-dihidropiridin-3,5-dicarboxilato de 3-etil-5-metil. |
| ES2055655A1 (es) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedimiento de obtencion de 2,6-dimetil-4-(2-nitrofenil)-1,4-dihidropiridin-3,5-dicarboxilato de 3-isobutil-5-metil. |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7671208B2 (en) | 2007-03-30 | 2010-03-02 | Esteve Quimica, S.A. | Acetone solvate of phthaloyl amlodipine |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2177409B1 (es) | 2003-08-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 20021201 Kind code of ref document: A1 |
|
| FG2A | Definitive protection |
Ref document number: 2177409B1 Country of ref document: ES |
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| FD1A | Patent lapsed |
Effective date: 20100412 |