ES2179927T3 - Procedimiento para la obtencion de un recubrimiento graduado constituido por fases de fosfato de calcio y fases de oxidos metalicos sobre implantes metalicos. - Google Patents
Procedimiento para la obtencion de un recubrimiento graduado constituido por fases de fosfato de calcio y fases de oxidos metalicos sobre implantes metalicos.Info
- Publication number
- ES2179927T3 ES2179927T3 ES96901711T ES96901711T ES2179927T3 ES 2179927 T3 ES2179927 T3 ES 2179927T3 ES 96901711 T ES96901711 T ES 96901711T ES 96901711 T ES96901711 T ES 96901711T ES 2179927 T3 ES2179927 T3 ES 2179927T3
- Authority
- ES
- Spain
- Prior art keywords
- phases
- pct
- metal oxide
- implants
- procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000007943 implant Substances 0.000 title abstract 3
- 235000011010 calcium phosphates Nutrition 0.000 title abstract 2
- 239000011248 coating agent Substances 0.000 title abstract 2
- 238000000576 coating method Methods 0.000 title abstract 2
- 229910044991 metal oxide Inorganic materials 0.000 title abstract 2
- 150000004706 metal oxides Chemical class 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 title abstract 2
- 229910000389 calcium phosphate Inorganic materials 0.000 title 1
- 239000001506 calcium phosphate Substances 0.000 title 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract 1
- 229910001069 Ti alloy Inorganic materials 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 230000001464 adherent effect Effects 0.000 abstract 1
- 229910001424 calcium ion Inorganic materials 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D9/00—Electrolytic coating other than with metals
- C25D9/04—Electrolytic coating other than with metals with inorganic materials
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L27/00—Materials for grafts or prostheses or for coating grafts or prostheses
- A61L27/28—Materials for coating prostheses
- A61L27/30—Inorganic materials
- A61L27/32—Phosphorus-containing materials, e.g. apatite
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F2310/00—Prostheses classified in A61F2/28 or A61F2/30 - A61F2/44 being constructed from or coated with a particular material
- A61F2310/00389—The prosthesis being coated or covered with a particular material
- A61F2310/00592—Coating or prosthesis-covering structure made of ceramics or of ceramic-like compounds
- A61F2310/00796—Coating or prosthesis-covering structure made of a phosphorus-containing compound, e.g. hydroxy(l)apatite
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S623/00—Prosthesis, i.e. artificial body members, parts thereof, or aids and accessories therefor
- Y10S623/901—Method of manufacturing prosthetic device
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Transplantation (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Electrochemistry (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Materials For Medical Uses (AREA)
- Prostheses (AREA)
Abstract
LA INVENCION SE REFIERE A UN PROCESO PARA LA PRODUCCION DE UN RECUBRIMIENTO GRADUADO DE FASES DE FOSFATO DE CALCIO Y FASES DE OXIDO METALICO EN IMPLANTES DE METAL, EN CONCRETO LOS FABRICADOS DE TITANIO O ALEACIONES DE TITANIO, PARA SU USO COMO IMPLANTES DENTALES, DE MANDIBULA O DE ARTICULACIONES. UNA SOLUCION QUE CONTIENE IONES DE CALCIO E IONES DE FOSFATO SE UTILIZA COMO ELECTROLITO CUYO PH ES ENTRE LIGERAMENTE ACIDICO Y APROXIMADAMENTE NEUTRO. LOS ELECTRODOS DEL SUSTRATO SE POLARIZAN DE MODO ALTERNO DE FORMA CATODICA Y ANODICA. LA CAPA SE DEPOSITA DE MODO GRADUADO ES ADHERENTE, TIENE UNA ESTRUCTURA FINA Y SE DISTINGUE POR UN ELEVADO GRADO DE BIOCOMPATIBILIDAD.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19504386A DE19504386C2 (de) | 1995-02-10 | 1995-02-10 | Verfahren zur Herstellung einer gradierten Beschichtung aus Calciumphosphatphasen und Metalloxidphasen auf metallischen Implantaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2179927T3 true ES2179927T3 (es) | 2003-02-01 |
Family
ID=7753614
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES96901711T Expired - Lifetime ES2179927T3 (es) | 1995-02-10 | 1996-02-06 | Procedimiento para la obtencion de un recubrimiento graduado constituido por fases de fosfato de calcio y fases de oxidos metalicos sobre implantes metalicos. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5723038A (es) |
| EP (1) | EP0756499B1 (es) |
| JP (1) | JP3502638B2 (es) |
| KR (1) | KR970702079A (es) |
| AT (1) | ATE221789T1 (es) |
| AU (1) | AU4618896A (es) |
| DE (2) | DE19504386C2 (es) |
| DK (1) | DK0756499T3 (es) |
| ES (1) | ES2179927T3 (es) |
| PT (1) | PT756499E (es) |
| WO (1) | WO1996024391A1 (es) |
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10102288A (ja) * | 1996-09-24 | 1998-04-21 | Queen Mary & Westfield College | リン酸カルシウム化合物のコーティング方法 |
| ATE220565T1 (de) | 1996-12-23 | 2002-08-15 | Stiftung Robert Mathys H C Dr | Bioaktive oberflächenschicht für knochenimplantate |
| SE513556C2 (sv) * | 1997-11-11 | 2000-10-02 | Nobel Biocare Ab | Implantatelement med tunt ytskickt applicerat genom het isostatisk pressning |
| US6045683A (en) * | 1997-12-01 | 2000-04-04 | University Of Alabama In Huntsville | Modified brushite surface coating, process therefor, and low temperature conversion to hydroxyapatite |
| EP0987031B1 (en) * | 1998-09-15 | 2003-04-02 | IsoTis N.V. | Method for coating medical implants |
| CA2365901A1 (en) | 1999-04-14 | 2000-10-19 | Musc Foundation For Research Development | Tissue-specific and pathogen-specific toxic agents and ribozymes |
| DE10006992B4 (de) * | 2000-02-16 | 2006-10-12 | Aesculap Ag & Co. Kg | Verfahren zur Beschichtung eines Implantats und Implantat mit Beschichtung |
| SE516282C2 (sv) * | 2000-04-04 | 2001-12-10 | Nobel Biocare Ab | Implantat försett med anslutnings- och hålisättningsdelar samt förfarande vid dylikt implantat |
| DE10029520A1 (de) | 2000-06-21 | 2002-01-17 | Merck Patent Gmbh | Beschichtung für metallische Implantatmaterialien |
| GB0015479D0 (en) * | 2000-06-23 | 2000-08-16 | Univ London | Transcutaneous Prosthesis |
| AU5985500A (en) * | 2000-07-17 | 2002-01-30 | Dot Gmbh | Bioactive calcium phosphate composite layers electrochemically deposited on implants |
| KR100388074B1 (ko) * | 2000-09-04 | 2003-06-18 | 주식회사 오스코텍 | 칼슘 포스페이트 초박막 코팅된 임플란트 |
| US7192445B2 (en) * | 2000-12-06 | 2007-03-20 | Astra Tech Ab | Medical prosthetic devices and implants having improved biocompatibility |
| ATE399571T1 (de) | 2001-06-06 | 2008-07-15 | Biomet Merck Gmbh | Apatitbeschichteter metallischer werkstoff, verfahren zu dessen herstellung sowie verwendung |
| GB0208642D0 (en) | 2002-04-16 | 2002-05-22 | Accentus Plc | Metal implants |
| US7740481B2 (en) * | 2002-06-21 | 2010-06-22 | Politecnico Di Milano | Osteointegrative interface for implantable prostheses and a method for the treatment of the osteointegrative interface |
| ITMI20021377A1 (it) * | 2002-06-21 | 2003-12-22 | Milano Politecnico | Interfaccia ostointegrativa per protesi impiantabili e metodo per il trattamento di detta interfaccia ostointegrativa |
| US20040053197A1 (en) * | 2002-09-16 | 2004-03-18 | Zoran Minevski | Biocompatible implants |
| US6974532B2 (en) * | 2003-05-01 | 2005-12-13 | New York University | Method for producing adherent coatings of calcium phosphate phases on titanium and titanium alloy substrates by electrochemical deposition |
| US7029566B2 (en) * | 2003-09-12 | 2006-04-18 | Chinese Petroleum Corporation | Process of forming HA/ZrO2 complex coating on Co—Cr—Mo alloy |
| GB0405680D0 (en) * | 2004-03-13 | 2004-04-21 | Accentus Plc | Metal implants |
| KR100714244B1 (ko) | 2004-04-26 | 2007-05-02 | 한국기계연구원 | 생체용 골유도성 금속 임플란트 및 그 제조방법 |
| CA2654235C (en) * | 2006-06-12 | 2015-01-06 | Accentus Plc | Metal implant comprising an anodised oxide surface coated with a ceramic, and with biocidal metal ions |
| US8057843B2 (en) * | 2006-08-22 | 2011-11-15 | Thommen Medical Ag | Implant, in particular dental implant |
| US20100136083A1 (en) * | 2007-01-15 | 2010-06-03 | Accentus Plc | Metal Implants |
| US8858775B2 (en) | 2007-10-03 | 2014-10-14 | Accentus Medical Limited | Method of manufacturing metal with biocidal properties |
| GB0720982D0 (en) * | 2007-10-25 | 2007-12-05 | Plasma Coatings Ltd | Method of forming a bioactive coating |
| CN102014975A (zh) | 2008-02-29 | 2011-04-13 | 史密夫和内修有限公司 | 用于生物医学应用的梯度涂层 |
| DE102008026558B4 (de) | 2008-06-03 | 2010-04-01 | Königsee Implantate und Instrumente zur Osteosynthese GmbH | Elektrochemisches Tauchverfahren in einem wässrigen Elektrolyt zur Erzeugung einer biologisch degradationsstabilen Oberflächenschicht auf Grundkörpern aus Titan oder Titanbasislegierungen |
| DE102008026557A1 (de) | 2008-06-03 | 2009-12-17 | Königsee Implantate und Instrumente zur Osteosynthese GmbH | Elektrochemisch hergestellte, biologisch degradationsstabile, duktile und haftfeste Titanoxid-Oberflächenschicht auf Titan oder Titanbasislegierungen |
| WO2009147819A1 (ja) * | 2008-06-03 | 2009-12-10 | 学校法人中部大学 | 骨修復材料及びその製造方法 |
| US8696759B2 (en) | 2009-04-15 | 2014-04-15 | DePuy Synthes Products, LLC | Methods and devices for implants with calcium phosphate |
| DE102009041248A1 (de) * | 2009-09-04 | 2011-05-05 | Innotere Gmbh | Bioaktiv beschichtete Metallimplantate und Verfahren zu deren Herstellung |
| US20110089041A1 (en) * | 2009-10-19 | 2011-04-21 | Biomet Manufacturing Corp. | Methods of depositing discrete hydroxyapatite regions on medical implants |
| JP2013508262A (ja) | 2009-10-26 | 2013-03-07 | ラトガース,ザ ステート ユニバーシティ オブ ニュー ジャージー | 制御可能なサイズおよび形態を有するハイドロキシアパタイト |
| US8475536B2 (en) | 2010-01-29 | 2013-07-02 | DePuy Synthes Products, LLC | Methods and devices for implants with improved cement adhesion |
| ES2699495T3 (es) | 2011-02-08 | 2019-02-11 | Cambridge Nanotherm Ltd | Sustrato de metal aislado |
| DE102012001260B4 (de) | 2012-01-23 | 2015-04-02 | Dot Gmbh | Antibakterielle und osteoinduktive Implantatbeschichtung |
| DE102012021003B4 (de) * | 2012-10-26 | 2015-02-12 | Otto Bock Healthcare Products Gmbh | Perkutanes lmplantat und Verfahren zum Herstellen eines solchen lmplantates |
| DE102014105732B3 (de) | 2014-04-23 | 2015-04-09 | Syntellix Ag | Verfahren zur Oberflächenbehandlung eines biokorrodierbaren Implantats und nach dem Verfahren erhaltenes Implantat |
| CN104790007B (zh) * | 2015-04-21 | 2017-03-29 | 浙江大学 | 医用金属植入体表面的矿化胶原涂层的制备方法 |
| CN105648497B (zh) * | 2016-01-13 | 2018-06-26 | 西安交通大学 | 一种钛表面钛酸锌-氧化钛复合抗菌涂层及其制备方法 |
| CN108760966A (zh) * | 2018-05-29 | 2018-11-06 | 四川维思达医疗器械有限公司 | 一种确定磷酸钙电化学涂层中电解液条件的方法 |
| DE102020111669A1 (de) | 2020-04-29 | 2021-11-04 | Rheinisch-Westfälische Technische Hochschule (Rwth) Aachen | Gradierte Dünnschichtsysteme aus Metall-Keramik-Verbundwerkstoffen für die Beschichtung kardiovaskulärer Implantate |
| CN115444981B (zh) * | 2021-06-09 | 2023-11-10 | 中国科学院上海硅酸盐研究所 | 具有生物抗氧化和促成骨性能的羟基磷灰石-二氧化锰复合涂层及其制备方法和应用 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5214095A (en) * | 1975-07-23 | 1977-02-02 | Sumitomo Chemical Co | Implant in bone |
| DE2827529C2 (de) * | 1978-06-23 | 1982-09-30 | Battelle-Institut E.V., 6000 Frankfurt | Implantierbarer Knochenersatzwerkstoff bestehend aus einem Metallkern und aus bioaktiven, gesinterten Calciumphosphat-Keramik-Partikeln und ein Verfahren zu seiner Herstellung |
| US4666567A (en) * | 1981-07-31 | 1987-05-19 | The Boeing Company | Automated alternating polarity pulse electrolytic processing of electrically conductive substances |
| US4478689A (en) * | 1981-07-31 | 1984-10-23 | The Boeing Company | Automated alternating polarity direct current pulse electrolytic processing of metals |
| DD246028A1 (de) * | 1986-02-12 | 1987-05-27 | Karl Marx Stadt Tech Hochschul | Keramisiertes metallimplantat |
| DD246476A1 (de) * | 1986-03-12 | 1987-06-10 | Karl Marx Stadt Tech Hochschul | Einteilige zementfrei verankerbare biokompatible hueftgelenkpfanne |
| US5310464A (en) * | 1991-01-04 | 1994-05-10 | Redepenning Jody G | Electrocrystallization of strongly adherent brushite coatings on prosthetic alloys |
| US5205921A (en) * | 1991-02-04 | 1993-04-27 | Queen's University At Kingston | Method for depositing bioactive coatings on conductive substrates |
| JP3081316B2 (ja) * | 1991-11-19 | 2000-08-28 | 石福金属興業株式会社 | インプラント材の表面処理方法 |
| HU213001B (en) * | 1992-04-10 | 1997-01-28 | Tavkoezlesi Innovacios Rt | Process for obtaining tissue-protective deposit on implants prepared from titanium and/or titanium-base microalloy |
| CA2073781A1 (en) * | 1992-07-13 | 1994-01-14 | Morteza Shirkhanzadeh | Process for forming bioactive composite coatings on implantable devices |
| DE4303575C1 (de) * | 1993-02-08 | 1994-04-14 | Electro Chem Eng Gmbh | Verfahren zur Herstellung apatitbeschichteter Metallimplantate |
-
1995
- 1995-02-10 DE DE19504386A patent/DE19504386C2/de not_active Expired - Lifetime
-
1996
- 1996-02-06 PT PT96901711T patent/PT756499E/pt unknown
- 1996-02-06 WO PCT/DE1996/000197 patent/WO1996024391A1/de not_active Ceased
- 1996-02-06 DK DK96901711T patent/DK0756499T3/da active
- 1996-02-06 ES ES96901711T patent/ES2179927T3/es not_active Expired - Lifetime
- 1996-02-06 AT AT96901711T patent/ATE221789T1/de active
- 1996-02-06 KR KR1019960705671A patent/KR970702079A/ko not_active Withdrawn
- 1996-02-06 JP JP52389896A patent/JP3502638B2/ja not_active Expired - Lifetime
- 1996-02-06 AU AU46188/96A patent/AU4618896A/en not_active Abandoned
- 1996-02-06 EP EP96901711A patent/EP0756499B1/de not_active Expired - Lifetime
- 1996-02-06 US US08/718,445 patent/US5723038A/en not_active Expired - Lifetime
- 1996-02-06 DE DE59609528T patent/DE59609528D1/de not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| ATE221789T1 (de) | 2002-08-15 |
| WO1996024391A1 (de) | 1996-08-15 |
| US5723038A (en) | 1998-03-03 |
| JP3502638B2 (ja) | 2004-03-02 |
| DE59609528D1 (de) | 2002-09-12 |
| DE19504386C2 (de) | 1997-08-28 |
| EP0756499A1 (de) | 1997-02-05 |
| PT756499E (pt) | 2002-12-31 |
| KR970702079A (ko) | 1997-05-13 |
| JPH10503108A (ja) | 1998-03-24 |
| DK0756499T3 (da) | 2002-10-14 |
| DE19504386A1 (de) | 1996-08-22 |
| EP0756499B1 (de) | 2002-08-07 |
| AU4618896A (en) | 1996-08-27 |
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