ES2182019T3 - Proceso para preparar urea granular. - Google Patents

Proceso para preparar urea granular.

Info

Publication number
ES2182019T3
ES2182019T3 ES97900462T ES97900462T ES2182019T3 ES 2182019 T3 ES2182019 T3 ES 2182019T3 ES 97900462 T ES97900462 T ES 97900462T ES 97900462 T ES97900462 T ES 97900462T ES 2182019 T3 ES2182019 T3 ES 2182019T3
Authority
ES
Spain
Prior art keywords
urea
solution
procedure
formaldehyde
granular urea
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97900462T
Other languages
English (en)
Inventor
Hidetsugu Fujii
Haruyuki Morikawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toyo Engineering Corp
Original Assignee
Toyo Engineering Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=11919135&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2182019(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Toyo Engineering Corp filed Critical Toyo Engineering Corp
Application granted granted Critical
Publication of ES2182019T3 publication Critical patent/ES2182019T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • C05C9/005—Post-treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/14—Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
  • Glanulating (AREA)
  • Fertilizers (AREA)

Abstract

LA PRESENTE INVENCION DESCRIBE UN PROCEDIMIENTO PARA PREPARAR UREA GRANULAR, QUE RESUELVE EL PROBLEMA DE ELIMINAR LA HUMEDAD EN UN PROCEDIMIENTO EN TORRE PARA LA FORMACION DE GRANULOS, Y EL PROBLEMA DE CONCENTRAR EL FORMALDEHIDO DILUIDO EN LA GRANULACION MEDIANTE UN PROCEDIMIENTO DE LECHO FLUIDO BORBOTANTE CUANDO LA UREA SE GRANULA EN PRESENCIA DE FORMALDEHIDO. ES DECIR, LA INVENCION SUMINISTRA UN PROCEDIMIENTO PARA PREPARAR UREA GRANULAR A PARTIR DE GOTAS LIQUIDAS O DE GOTAS PULVERIZADAS DE UNA SOLUCION DE UREA, EN EL CUAL LA SOLUCION DE UREA SE DIVIDE EN DOS PORCIONES, UNA SOLUCION DE UREA A Y UNA SOLUCION DE UREA B, Y SE PREPARA UNA SOLUCION DE UREA MEZCLANDO UNA SOLUCION DE FORMALDEHIDO ACUOSO CON LA SOLUCION DE UREA A, CONCENTRANDO LA ANTERIOR SOLUCION MEZCLADA Y LUEGO MEZCLANDOLA CON LA SOLUCION DE UREA B.
ES97900462T 1996-02-01 1997-01-21 Proceso para preparar urea granular. Expired - Lifetime ES2182019T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP01654196A JP3667418B2 (ja) 1996-02-01 1996-02-01 粒状尿素の製造方法

Publications (1)

Publication Number Publication Date
ES2182019T3 true ES2182019T3 (es) 2003-03-01

Family

ID=11919135

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97900462T Expired - Lifetime ES2182019T3 (es) 1996-02-01 1997-01-21 Proceso para preparar urea granular.

Country Status (15)

Country Link
US (1) US5965071A (es)
EP (1) EP0819106B1 (es)
JP (1) JP3667418B2 (es)
CN (1) CN1098234C (es)
AR (1) AR005588A1 (es)
AU (1) AU705068B2 (es)
BR (1) BR9702047A (es)
CA (1) CA2215596C (es)
DE (1) DE69716177T2 (es)
ES (1) ES2182019T3 (es)
ID (1) ID15864A (es)
LT (1) LT4340B (es)
RU (1) RU2134251C1 (es)
SA (1) SA97170602B1 (es)
WO (1) WO1997028100A1 (es)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004005907B4 (de) * 2004-02-05 2006-01-05 Uhde Gmbh Anlage zur Herstellung von biuretarmem harnstoffhaltigem Düngemittelgranulat
NL1025805C2 (nl) * 2004-03-25 2005-09-27 Dsm Ip Assets Bv Werkwijze voor de granulatie van ureum.
US7862642B2 (en) * 2006-12-14 2011-01-04 Georgia-Pacific Chemicals Llc Extended-release urea-based granular fertilizer
EP2489429A1 (en) * 2011-02-21 2012-08-22 Urea Casale S.A. Fluid bed granulation of urea and related apparatus
CN102976499B (zh) * 2012-12-03 2013-12-04 北京师范大学 同时缓释氮和吸附-生物降解石油烃的复合板制备方法
EP2745901A1 (en) * 2012-12-19 2014-06-25 Urea Casale SA Method for transforming a prilling tower, in particular in a plant for the synthesis of urea
CN103011982B (zh) * 2012-12-29 2014-12-31 金正大生态工程集团股份有限公司 一种脲醛缓释复合肥料的工业化生产方法和装置
GB201502894D0 (en) 2015-02-20 2015-04-08 Johnson Matthey Plc Process
GB201502893D0 (en) 2015-02-20 2015-04-08 Johnson Matthey Plc Process
US10519103B2 (en) 2015-04-01 2019-12-31 Toyo Engineering Corporation Urea production method
CN105461361B (zh) * 2015-12-25 2019-05-14 北方华锦化学工业股份有限公司 多路蒸发尿素造粒系统
DE102017108842A1 (de) 2017-04-25 2018-10-25 Thyssenkrupp Ag Verfahren und Vorrichtung zur Herstellung von Harnstoff
CN117756573B (zh) * 2023-12-14 2026-01-02 宁波中科远东催化工程技术有限公司 一种大颗粒尿素的生产方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3112313A (en) 1963-11-26 Process for the production thereof
CH398530A (de) * 1957-10-30 1966-03-15 Montedison Spa Kontinuierliches Verfahren zur Herstellung von haltbaren konzentrierten wässrigen Harnstoff, Formaldehyd und Harnstoff-Formaldehyd-Kondensationsprodukte enthaltenden Lösungen
GB926781A (en) * 1959-06-02 1963-05-22 Vulcan Cincinnati Inc Dehydration of urea melts
US3112343A (en) * 1959-08-20 1963-11-26 Chemie Linz Ag Free-flowing, storage stable granular or pelletized urea
US3059280A (en) * 1960-10-27 1962-10-23 Grace W R & Co Urea prilling
US3130225A (en) * 1962-02-12 1964-04-21 Pullman Inc Urea production
US3378584A (en) * 1963-07-05 1968-04-16 Grace W R & Co Process for reducing the caking tendency of crystalline urea
US3686373A (en) * 1970-02-09 1972-08-22 George T Griesheimer Urea-prill anti-caking process
US3970625A (en) * 1973-03-14 1976-07-20 Allied Chemical Corporation Production of urea-formaldehyde concentrates
JPS5034536A (es) 1973-07-27 1975-04-02
CA1101641A (en) * 1977-06-09 1981-05-26 Anton Niks Urea granulation
GB1581761A (en) * 1977-06-09 1980-12-17 Azote Sa Cie Neerlandaise Urea granulation
NO148744C (no) * 1977-09-19 1983-12-07 Norsk Hydro As Fremgangsmaate til fremstilling av urea med hoey mekanisk styrke
JPS6034517B2 (ja) * 1978-03-03 1985-08-09 宇部興産株式会社 流動層で尿素を造粒する方法
DE3013616C2 (de) * 1979-05-11 1984-08-02 VEB Stickstoffwerk Piesteritz, DDR 4602 Wittenberg-Lutherstadt-Piesteritz Verfahren zur Behandlung von Harnstoff sowie ammonium- und nitrathaltigen Düngemitteln
JPS6058193B2 (ja) * 1980-01-31 1985-12-18 宇部興産株式会社 尿素の流動造粒方法
NL8001876A (nl) * 1980-03-29 1981-11-02 Unie Van Kunstmestfab Bv Werkwijze voor het maken van ureumprils en ureumprils verkregen met deze werkwijze.
JPS61216725A (ja) * 1985-03-20 1986-09-26 Mitsui Toatsu Chem Inc 尿素の造粒方法
SU1507761A1 (ru) * 1987-03-19 1989-09-15 Предприятие П/Я А-1676 Способ получени гранулированного карбамида
JPH01286985A (ja) * 1988-05-11 1989-11-17 Mitsui Toatsu Chem Inc 緩効性窒素肥料の製造方法
JPH063729A (ja) 1992-06-18 1994-01-14 Nikon Corp 縦走りフォーカルプレーンシャッタ用遮光羽根の製造方 法
JPH06305869A (ja) * 1993-04-28 1994-11-01 Mitsui Toatsu Chem Inc 緩効性窒素肥料の製造法

Also Published As

Publication number Publication date
JPH09208552A (ja) 1997-08-12
SA97170602B1 (ar) 2006-08-20
AR005588A1 (es) 1999-06-23
EP0819106A1 (en) 1998-01-21
LT4340B (lt) 1998-05-25
EP0819106B1 (en) 2002-10-09
US5965071A (en) 1999-10-12
CN1098234C (zh) 2003-01-08
LT97156A (en) 1998-02-25
AU2017297A (en) 1997-08-22
WO1997028100A1 (en) 1997-08-07
CA2215596A1 (en) 1997-08-07
DE69716177D1 (de) 2002-11-14
CN1178516A (zh) 1998-04-08
JP3667418B2 (ja) 2005-07-06
AU705068B2 (en) 1999-05-13
ID15864A (id) 1997-08-14
BR9702047A (pt) 1998-01-13
CA2215596C (en) 2001-10-16
DE69716177T2 (de) 2003-05-28
RU2134251C1 (ru) 1999-08-10

Similar Documents

Publication Publication Date Title
ES2182019T3 (es) Proceso para preparar urea granular.
KR950702864A (ko) 우레아 과립제의 제조 방법(process for the production of urea granules)
JPH06122581A (ja) 植物用カルシウム付与剤
FI864127A0 (fi) Foerfarande foer framstaellning av goedslingsgranuler som innehaoller urea och ammoniumsulfat.
DK564589A (da) Farmaceutisk ionbytterharpikssammensaetning
YU48414B (sh) Koncentrovani fungicidni preparati postupak za njihovo dobivanje i postupak za njihovu primenu u tretiranju biljaka
RU95106645A (ru) Способ производства гранул мочевины
YU49471B (sh) Uređaj za proizvodnju sulfoureičnog reagensa koji se koristi za dobijanje prirodnog fosfata u pogonu za proizvodnju azotnofosfatnih đubriva
BR9607573A (pt) Sistemas pesticidas granulares
ES2182197T3 (es) Procedimiento para la preparacion de granulados de fertilizantes de urea que contienen diciandiamida.
RU2006131686A (ru) Способ получения гранулированного удобрения, содержащего мочевину
DK678088A (da) Fremgangsmaade til tilvejebringelse af en styret opdeling af vaeskestoevsproejt
CN105801288A (zh) 一种含脲甲醛缓释药肥及其制备方法
CN106083284A (zh) 一种含硫锌磷酸一铵增效肥料及其生产方法
WO1999029639A2 (en) Combination for foliar supplementation of plants with selenium salts and urea
SE9803478L (sv) Förfarande för framställning av näringstillskott för djur
ES2123705T3 (es) Procedimiento para reducir el contenido de amoniaco de un efluente gaseoso procedente de instalaciones de produccion de urea.
JPS5659702A (en) Rearing agent of good rice plant seedling
UY40711A (es) Método para la fabricación de una composición de urea estabilizada
BG105713A (en) Method for preparing an effervescent granulate comprising iron gluconate, granulate thus obtained and tablets
PE55894A1 (es) Procedimiento para obtener a partir de la turba una preparacion con efecto inmunomodulante y que estimula la formacion de citoquina
CN106045684A (zh) 一种自备防结功能的含硫磷铵肥料及其生产方法
CU22024A1 (es) Proceso para la producción de un forraje enriquecido en proteína a partir de la fermentación en estado sólido de la cana de azúcar
Holobradá et al. Absorption and transport of anions by different roots of Zea mays L.
CZ287547B6 (cs) Kapalné organominerální hnojivo na bázi melasových výpalků s obsahem hořčíku