ES2182335T3 - Procedimiento para la obtencion de 2-ciclododecil-1-propanol. - Google Patents
Procedimiento para la obtencion de 2-ciclododecil-1-propanol.Info
- Publication number
- ES2182335T3 ES2182335T3 ES98932116T ES98932116T ES2182335T3 ES 2182335 T3 ES2182335 T3 ES 2182335T3 ES 98932116 T ES98932116 T ES 98932116T ES 98932116 T ES98932116 T ES 98932116T ES 2182335 T3 ES2182335 T3 ES 2182335T3
- Authority
- ES
- Spain
- Prior art keywords
- propionic acid
- propanol
- cyclododecyl
- cyclododecil
- procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N 1-propanol Substances CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 title 1
- IAYHEAJJFYJHJI-UHFFFAOYSA-N 2-cyclododecylpropanoic acid Chemical compound OC(=O)C(C)C1CCCCCCCCCCC1 IAYHEAJJFYJHJI-UHFFFAOYSA-N 0.000 abstract 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 abstract 2
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 abstract 2
- WKHTUDYDJUHYMK-UHFFFAOYSA-N 2-cyclododecylpropan-1-ol Chemical compound OCC(C)C1CCCCCCCCCCC1 WKHTUDYDJUHYMK-UHFFFAOYSA-N 0.000 abstract 1
- 241000208836 Adoxa moschatellina Species 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 abstract 1
- HYPABJGVBDSCIT-UPHRSURJSA-N cyclododecene Chemical compound C1CCCCC\C=C/CCCC1 HYPABJGVBDSCIT-UPHRSURJSA-N 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 239000003999 initiator Substances 0.000 abstract 1
- 235000019260 propionic acid Nutrition 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/13—Monohydroxylic alcohols containing saturated rings
- C07C31/133—Monohydroxylic alcohols containing saturated rings monocyclic
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
- C07C51/353—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by isomerisation; by change of size of the carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
- C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
- C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C67/347—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
- C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La invención se refiere a un procedimiento ventajoso para la producción industrial de 2-ciclododecil-propanol, codiciada sustancia olorosa de la raíz del almizcle, mediante la reacción de ciclododeceno en la presencia de cantidades catalíticas de un iniciador radicalar con un excedente de ácido propiónico o de un derivado del ácido propiónico y la subsecuente hidrogenación catalítica del ácido 2-ciclododecil propiónico o de los correspondientes derivados del ácido 2-ciclododecil propiónico formados.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19725533A DE19725533A1 (de) | 1997-06-17 | 1997-06-17 | Verfahren zur Herstellung von 2-Cyclododecyl-1-propanol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2182335T3 true ES2182335T3 (es) | 2003-03-01 |
Family
ID=7832703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES98932116T Expired - Lifetime ES2182335T3 (es) | 1997-06-17 | 1998-06-04 | Procedimiento para la obtencion de 2-ciclododecil-1-propanol. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US6303836B1 (es) |
| EP (1) | EP0993427B1 (es) |
| JP (1) | JP2002504129A (es) |
| KR (1) | KR20010013841A (es) |
| CN (1) | CN1107044C (es) |
| AU (1) | AU8212898A (es) |
| BR (1) | BR9810438A (es) |
| CA (1) | CA2290780A1 (es) |
| DE (2) | DE19725533A1 (es) |
| ES (1) | ES2182335T3 (es) |
| IL (1) | IL132968A0 (es) |
| WO (1) | WO1998057914A1 (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0926121A1 (en) * | 1997-10-28 | 1999-06-30 | Quest International B.V. | Reaction of alkenes with epoxides, the products thereof and their use as fragrance compounds |
| DE10023256A1 (de) | 2000-05-12 | 2001-11-15 | Basf Ag | (+)-und(-)-2-Cyclododecylpropanol und (+)-und(-)-2-Cyclododecylpropionsäure sowie deren Herstellung und Verwendung |
| DE10229474A1 (de) * | 2002-07-01 | 2004-01-15 | Symrise Gmbh & Co. Kg | Neue Riechstoffe und Verfahren zu ihrer Herstellung |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2630835A1 (de) * | 1976-07-09 | 1978-01-19 | Basf Ag | Neue moschusartige riechstoffe und verfahren zu deren herstellung |
| DE3703585A1 (de) * | 1987-02-06 | 1988-08-18 | Consortium Elektrochem Ind | Alkohole und ether mit cyclododecyl- und cyclododecenylgruppen, deren herstellung und verwendung als duftstoffe |
-
1997
- 1997-06-17 DE DE19725533A patent/DE19725533A1/de not_active Withdrawn
-
1998
- 1998-06-04 ES ES98932116T patent/ES2182335T3/es not_active Expired - Lifetime
- 1998-06-04 EP EP98932116A patent/EP0993427B1/de not_active Expired - Lifetime
- 1998-06-04 BR BR9810438-1A patent/BR9810438A/pt not_active IP Right Cessation
- 1998-06-04 CA CA002290780A patent/CA2290780A1/en not_active Abandoned
- 1998-06-04 AU AU82128/98A patent/AU8212898A/en not_active Abandoned
- 1998-06-04 JP JP50366299A patent/JP2002504129A/ja active Pending
- 1998-06-04 DE DE59805432T patent/DE59805432D1/de not_active Expired - Lifetime
- 1998-06-04 US US09/424,258 patent/US6303836B1/en not_active Expired - Fee Related
- 1998-06-04 WO PCT/EP1998/003339 patent/WO1998057914A1/de not_active Ceased
- 1998-06-04 KR KR1019997011862A patent/KR20010013841A/ko not_active Withdrawn
- 1998-06-04 CN CN98806314A patent/CN1107044C/zh not_active Expired - Fee Related
- 1998-06-04 IL IL13296898A patent/IL132968A0/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN1260773A (zh) | 2000-07-19 |
| BR9810438A (pt) | 2000-09-19 |
| DE59805432D1 (de) | 2002-10-10 |
| DE19725533A1 (de) | 1998-12-24 |
| CN1107044C (zh) | 2003-04-30 |
| KR20010013841A (ko) | 2001-02-26 |
| AU8212898A (en) | 1999-01-04 |
| EP0993427B1 (de) | 2002-09-04 |
| WO1998057914A1 (de) | 1998-12-23 |
| US6303836B1 (en) | 2001-10-16 |
| CA2290780A1 (en) | 1998-12-23 |
| IL132968A0 (en) | 2001-03-19 |
| EP0993427A1 (de) | 2000-04-19 |
| JP2002504129A (ja) | 2002-02-05 |
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