ES2609331T3 - Proceso de fluoración en fase líquida - Google Patents
Proceso de fluoración en fase líquida Download PDFInfo
- Publication number
- ES2609331T3 ES2609331T3 ES10726568.8T ES10726568T ES2609331T3 ES 2609331 T3 ES2609331 T3 ES 2609331T3 ES 10726568 T ES10726568 T ES 10726568T ES 2609331 T3 ES2609331 T3 ES 2609331T3
- Authority
- ES
- Spain
- Prior art keywords
- liquid phase
- chloro
- mixture
- tetrachloropropene
- trifluoropropene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000007791 liquid phase Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000004334 fluoridation Methods 0.000 title 1
- UMGQVBVEWTXECF-UHFFFAOYSA-N 1,1,2,3-tetrachloroprop-1-ene Chemical compound ClCC(Cl)=C(Cl)Cl UMGQVBVEWTXECF-UHFFFAOYSA-N 0.000 abstract 2
- CFXQEHVMCRXUSD-UHFFFAOYSA-N 1,2,3-Trichloropropane Chemical compound ClCC(Cl)CCl CFXQEHVMCRXUSD-UHFFFAOYSA-N 0.000 abstract 2
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- WZLFPVPRZGTCKP-UHFFFAOYSA-N 1,1,1,3,3-pentafluorobutane Chemical compound CC(F)(F)CC(F)(F)F WZLFPVPRZGTCKP-UHFFFAOYSA-N 0.000 abstract 1
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 abstract 1
- NPNPZTNLOVBDOC-UHFFFAOYSA-N 1,1-difluoroethane Chemical compound CC(F)F NPNPZTNLOVBDOC-UHFFFAOYSA-N 0.000 abstract 1
- FQAMAOOEZDRHHB-UHFFFAOYSA-N 1,2,2-trichloro-1,1-difluoroethane Chemical compound FC(F)(Cl)C(Cl)Cl FQAMAOOEZDRHHB-UHFFFAOYSA-N 0.000 abstract 1
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 abstract 1
- POPRFGQIJQMYNL-UHFFFAOYSA-N 1,3-dichloro-1-fluorobutane Chemical compound CC(Cl)CC(F)Cl POPRFGQIJQMYNL-UHFFFAOYSA-N 0.000 abstract 1
- YACLCMMBHTUQON-UHFFFAOYSA-N 1-chloro-1-fluoroethane Chemical compound CC(F)Cl YACLCMMBHTUQON-UHFFFAOYSA-N 0.000 abstract 1
- SMCNZLDHTZESTK-UHFFFAOYSA-N 2-chloro-1,1,1,2-tetrafluoropropane Chemical compound CC(F)(Cl)C(F)(F)F SMCNZLDHTZESTK-UHFFFAOYSA-N 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000003682 fluorination reaction Methods 0.000 abstract 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/0706—Purification ; Separation of hydrogen chloride
- C01B7/0712—Purification ; Separation of hydrogen chloride by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/21—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms with simultaneous increase of the number of halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/04—Chloro-alkenes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Proceso de fluoración de que comprende 1,1,2,3-tetracloropropeno: (i) poner en contacto 1,1,2,3-tetracloropropeno con fluoruro de hidrógeno en una fase líquida en un disolvente bajo condiciones suficientes para formar una mezcla de reacción que comprende 2-cloro-3,3,3-trifluoropropeno, estando dicho seleccionado entre 1,2-dicloroetano, 1,2,3-tricloropropano, 1-cloro-1-fluoroetano, 1,1-difluoroetano, 1,1-dicloroetano y 1,3-dicloro-1-fluorobutano, 1,1,1, 3,3-pentafluorobutano y 1,1,2-tricloro-2,2-difluoroetano, o una mezcla de los mismos; (ii) separar la mezcla de reacción en una primera corriente que comprende HCl, y que comprende una segunda corriente de HF, 2-cloro-3,3,3-trifluoropropeno y 1,1,1,2-tetrafluoro-2-cloropropano.
Description
9
Claims (1)
-
imagen1 imagen2
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/IB2010/001114 WO2011110889A1 (en) | 2010-03-10 | 2010-03-10 | Process of fluorination in liquid phase |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2609331T3 true ES2609331T3 (es) | 2017-04-19 |
Family
ID=42989491
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES10726568.8T Active ES2609331T3 (es) | 2010-03-10 | 2010-03-10 | Proceso de fluoración en fase líquida |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US8889925B2 (es) |
| EP (1) | EP2545021B1 (es) |
| ES (1) | ES2609331T3 (es) |
| HU (1) | HUE032122T2 (es) |
| PL (1) | PL2545021T3 (es) |
| WO (1) | WO2011110889A1 (es) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20170253545A1 (en) | 2007-01-03 | 2017-09-07 | Honeywell International Inc. | Process for producing 2,3,3,3-tetrafluoropropene |
| US9670117B2 (en) | 2007-01-03 | 2017-06-06 | Honeywell International Inc. | Process for producing 2,3,3,3-tetrafluoropropene |
| JP5459320B2 (ja) * | 2009-05-13 | 2014-04-02 | ダイキン工業株式会社 | 塩素含有フルオロカーボン化合物の製造方法 |
| US8889925B2 (en) * | 2010-03-10 | 2014-11-18 | Arkema France | Process of fluorination in liquid phase |
| JP5884130B2 (ja) | 2010-10-25 | 2016-03-15 | アルケマ フランス | 2−クロロ−3,3,3−トリフルオロプロペンの液相フッ素化で2−クロロ−1,1,1,2−テトラフルオロプロペンを製造する方法 |
| CN103201242A (zh) * | 2010-11-15 | 2013-07-10 | 阿克马法国公司 | 通过五氯丙烷的液相氟化制造2-氯-3,3,3-三氟丙烯(hcfo 1233xf)的方法 |
| US9890096B2 (en) | 2011-01-19 | 2018-02-13 | Honeywell International Inc. | Methods of making 2,3,3,3-tetrafluoro-2-propene |
| PL2773605T3 (pl) * | 2011-11-04 | 2026-04-27 | Honeywell International, Inc. | Sposób wytwarzania 2,3,3,3-tetrafluoropropenu |
| IN2014DN06917A (es) | 2012-02-10 | 2015-05-15 | Haiyou Wang | |
| MX344552B (es) * | 2012-02-29 | 2016-12-20 | Honeywell Int Inc | Proceso para producir 2, 3, 3, 3 - tetrafluoropropeno. |
| US8889929B2 (en) | 2013-02-19 | 2014-11-18 | Honeywell International Inc. | Process to make 1,1,2,3-tetrachloropropene from 1,1,3-trichloropropene and/or 3,3,3-trichloropropene |
| US9334206B2 (en) | 2013-03-15 | 2016-05-10 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
| US9272967B2 (en) * | 2013-10-15 | 2016-03-01 | Honeywell International Inc. | Process for producing 1-chloro-3,3,3-trifluoropropene in an ionic liquid |
| JP6098608B2 (ja) * | 2014-10-07 | 2017-03-22 | ダイキン工業株式会社 | フッ素基を含有するハロオレフィン化合物の製造方法及び組成物 |
| JP6210073B2 (ja) | 2015-01-21 | 2017-10-11 | ダイキン工業株式会社 | フルオロプロペンの製造方法 |
| FR3064622B1 (fr) | 2017-03-28 | 2019-03-22 | Arkema France | Procede de recuperation d'acide fluorhydrique |
| CN110372471A (zh) * | 2019-07-26 | 2019-10-25 | 西安近代化学研究所 | 六氯丁二烯的催化转化方法 |
| US11806698B2 (en) * | 2020-05-01 | 2023-11-07 | Uop Llc | System for ionic liquid catalyst regeneration |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2787646A (en) * | 1953-09-03 | 1957-04-02 | Haszeldine Robert Neville | Organic halogen compounds and methods of making same |
| JPS5946211B2 (ja) * | 1975-12-29 | 1984-11-10 | ダイキン工業株式会社 | 1− クロロ −1,1− ジフルオロエタンマタハ / オヨビ 1,1,1− トリフルオロエタンオセイゾウスルホウホウ |
| US4885416A (en) * | 1985-10-18 | 1989-12-05 | E. I. Du Pont De Nemours And Company | Fluorination process |
| BE1007393A3 (fr) * | 1993-08-04 | 1995-06-06 | Solvay | Procede pour la preparation de 1-chloro-1-fluoroethane et/ou de 1,1-difluoroethane. |
| US5714754A (en) * | 1994-03-04 | 1998-02-03 | Nicholas; John Jacob | Remote zone operation of lighting systems for above-ground enclosed or semi-enclosed parking structures |
| US5616819A (en) | 1995-08-28 | 1997-04-01 | Laroche Industries Inc. | Process for preparing fluorinated aliphatic compounds |
| US5969198A (en) | 1997-06-27 | 1999-10-19 | Alliedsignal Inc. | Process for the preparation of 1,1,1,3,3-pentafluoropropane |
| GB0113080D0 (en) * | 2001-05-30 | 2001-07-18 | Kvaerner Process Tech Ltd | Process |
| US8664455B2 (en) | 2008-08-08 | 2014-03-04 | Honeywell International Inc. | Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb) |
| US8071825B2 (en) * | 2006-01-03 | 2011-12-06 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| FR2916755B1 (fr) * | 2007-05-31 | 2009-08-21 | Arkema France | Procede de preparation d'(hydro)(chloro)(fluoro)olefines |
| US8563789B2 (en) * | 2007-06-27 | 2013-10-22 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| US9035111B2 (en) | 2007-08-22 | 2015-05-19 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| JP5767231B2 (ja) * | 2009-10-09 | 2015-08-19 | ダウ グローバル テクノロジーズ エルエルシー | 塩素化及び/又はフッ素化されたプロペン及びより高級なアルケンを製造するプロセス |
| US8889925B2 (en) * | 2010-03-10 | 2014-11-18 | Arkema France | Process of fluorination in liquid phase |
-
2010
- 2010-03-10 US US13/583,293 patent/US8889925B2/en not_active Expired - Fee Related
- 2010-03-10 EP EP10726568.8A patent/EP2545021B1/en not_active Not-in-force
- 2010-03-10 ES ES10726568.8T patent/ES2609331T3/es active Active
- 2010-03-10 HU HUE10726568A patent/HUE032122T2/hu unknown
- 2010-03-10 PL PL10726568T patent/PL2545021T3/pl unknown
- 2010-03-10 WO PCT/IB2010/001114 patent/WO2011110889A1/en not_active Ceased
-
2014
- 2014-10-08 US US14/509,623 patent/US9315431B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP2545021B1 (en) | 2016-09-28 |
| PL2545021T3 (pl) | 2017-03-31 |
| HUE032122T2 (hu) | 2017-08-28 |
| US20130041191A1 (en) | 2013-02-14 |
| US20150094502A1 (en) | 2015-04-02 |
| US9315431B2 (en) | 2016-04-19 |
| EP2545021A1 (en) | 2013-01-16 |
| WO2011110889A1 (en) | 2011-09-15 |
| US8889925B2 (en) | 2014-11-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES2609331T3 (es) | Proceso de fluoración en fase líquida | |
| ES2556955T3 (es) | Fluoración catalítica en fase gaseosa de 243db para dar 1234yf | |
| ES2547871T3 (es) | Fluoración catalítica en fase gaseosa de 1230xa para dar 1234yf | |
| ES2647547T3 (es) | Procedimiento para preparar un gel reticulado | |
| ES2699153T3 (es) | Procedimientos para la separación de 3,3,3-trifluoropropeno y fluoruro de hidrógeno | |
| CN101541715B (zh) | 通过共沸蒸馏将氟代烯烃与氟化氢分离的方法 | |
| ES2758087T3 (es) | Método para separar compuestos organofluorados empleando una membrana | |
| ES2392884T3 (es) | Procedimiento para separar una fluoroolefina de HF mediante extracción líquido-líquido | |
| KR101851887B1 (ko) | 공비 증류에 의한 플루오르화수소로부터의 1,3,3,3-테트라플루오로프로펜의 분리 방법 | |
| RU2013123286A (ru) | Способ получения 2,3,3,3-тетрафторпропена | |
| WO2012148695A3 (en) | INTEGRATED PROCESS TO CO-PRODUCE 1,1,1,3,3-PENTAFLUOROPROPANE, TRANS-1-CHLORO-3,3,3-TRIFLUOROPROPENE and TRANS-1,3,3,3-TETRAFLUOROPROPENE | |
| WO2012009114A3 (en) | Method for prolonging a catalyst's life during hydrofluorination | |
| MX2013002467A (es) | Proceso integrado para co-producir trans-1-cloro-3,3,3-trifluoropr openo, trans-1,3,3,3-tetrafluoropropeno y 1,1,1,3,3-pentafluoropro pano. | |
| MX2009003492A (es) | Composiciones azeotropicas de 2-cloro-3,3,3-trifluoropropeno (hcfc-1233xf), 2-cloro-1,1,1,2-tetrafluoropropano (hcfc-244bb), y fluoruro de hidrogeno (hf). | |
| ES2329867T1 (es) | Procedimiento integrado para producir 2,3,3,3-tetrafluoropropano. | |
| AR088210A1 (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno | |
| JP2011513228A5 (es) | ||
| IN2014DN07744A (es) | ||
| AR088658A1 (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno | |
| AR088342A1 (es) | Proceso para producir 2,3,3,3-tetrafluorpropeno | |
| ES2547073T3 (es) | Método para preparar 1,1-difluoroetano | |
| WO2009069750A1 (ja) | 含フッ素化合物の製造方法 | |
| ES2787373T3 (es) | Método de producción de una composición que contiene 1,2-dicloro-3,3,3-trifluoropropeno (HCFO-1223xd) y/o 1,1,2-tricoloro-3,3,3-trifluoropropeno (CFO-1213xa) | |
| WO2008030438A3 (en) | A process and methods of purification for the manufacture fluorocarbons | |
| EP3805189B1 (en) | Method for producing fluorine group-containing haloolefin 1233xf |