ID26736A - Proses produksi dan proses pemurnian bis- -hidroksietil tereftalat - Google Patents
Proses produksi dan proses pemurnian bis- -hidroksietil tereftalatInfo
- Publication number
- ID26736A ID26736A IDW20001563A ID20001563A ID26736A ID 26736 A ID26736 A ID 26736A ID W20001563 A IDW20001563 A ID W20001563A ID 20001563 A ID20001563 A ID 20001563A ID 26736 A ID26736 A ID 26736A
- Authority
- ID
- Indonesia
- Prior art keywords
- bis
- beta
- hydroxyethyl terephthalate
- mixture
- hydroxyethyl
- Prior art date
Links
- -1 BIS-HYDROXYETHYL Chemical class 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 5
- 238000000034 method Methods 0.000 abstract 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 3
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 abstract 2
- 150000001450 anions Chemical class 0.000 abstract 2
- 150000001768 cations Chemical class 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 150000002500 ions Chemical class 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229920000728 polyester Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/80—Phthalic acid esters
- C07C69/82—Terephthalic acid esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J11/00—Recovery or working-up of waste materials
- C08J11/04—Recovery or working-up of waste materials of polymers
- C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
- C08J11/18—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material
- C08J11/22—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds
- C08J11/24—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds containing hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22080499A JP2001048837A (ja) | 1999-08-04 | 1999-08-04 | イオン含有量の少ないビス−β−ヒドロキシエチルテレフタレートの製造法 |
| JP22266399A JP3782905B2 (ja) | 1999-08-05 | 1999-08-05 | 粗ビス−β−ヒドロキシエチルテレフタレートの精製方法および精製ビス−β−ヒドロキシエチルテレフタレート |
| JP22266499A JP3782906B2 (ja) | 1999-08-05 | 1999-08-05 | 粗ビス−β−ヒドロキシエチルテレフタレート精製方法 |
| JP22603399A JP3782907B2 (ja) | 1999-08-10 | 1999-08-10 | ビス−β−ヒドロキシエチルテレフタレートおよび/またはその低縮合物の製造法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ID26736A true ID26736A (id) | 2001-02-08 |
Family
ID=27476978
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IDW20001563A ID26736A (id) | 1999-08-04 | 1999-12-24 | Proses produksi dan proses pemurnian bis- -hidroksietil tereftalat |
Country Status (13)
| Country | Link |
|---|---|
| US (2) | US6630601B1 (es) |
| EP (1) | EP1120394B1 (es) |
| KR (3) | KR100740059B1 (es) |
| CN (3) | CN1511823A (es) |
| AT (1) | ATE275538T1 (es) |
| AU (1) | AU764053B2 (es) |
| CA (1) | CA2318761A1 (es) |
| DE (1) | DE69920025T2 (es) |
| ES (1) | ES2228142T3 (es) |
| HK (1) | HK1040236A1 (es) |
| ID (1) | ID26736A (es) |
| TW (1) | TW506968B (es) |
| WO (1) | WO2001010812A1 (es) |
Families Citing this family (49)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001122825A (ja) * | 1999-10-28 | 2001-05-08 | Japan Organo Co Ltd | 粗ビスヒドロキシアルキルテレフタレートの精製方法 |
| WO2001056970A1 (en) * | 2000-02-04 | 2001-08-09 | Aies Co., Ltd. | PROCESS FOR PRODUCTION OF HIGH-PURITY BIS-β-HYDROXYETHYL TEREPHTHALATE |
| CA2419625A1 (en) * | 2000-07-31 | 2003-01-29 | Aies Co., Ltd. | Bis-.beta.-hydroxyethyl terephthalate |
| JPWO2003051815A1 (ja) * | 2001-12-18 | 2005-04-28 | 株式会社アイエス | ポリエステルのエチレングリコール分解生成溶液の脱イオン処理方法 |
| CN1264804C (zh) * | 2002-06-04 | 2006-07-19 | 株式会社爱维塑 | 对苯二甲酸二(2-羟乙基)酯的精制方法 |
| WO2005035621A1 (ja) | 2003-10-08 | 2005-04-21 | Aies Co., Ltd. | 成形用ポリエチレンテレフタレートおよびその製造方法 |
| US7192988B2 (en) * | 2004-09-30 | 2007-03-20 | Invista North America S.Ar.L. | Process for recycling polyester materials |
| US8541477B2 (en) | 2011-03-04 | 2013-09-24 | International Business Machines Corporation | Methods of depolymerizing terephthalate polyesters |
| CN102816069B (zh) * | 2012-08-16 | 2014-06-18 | 无锡格瑞恩环保科技有限公司 | 对苯二甲酸二(2-羟乙基)酯的制备方法 |
| EP3140281B1 (en) * | 2014-05-05 | 2018-03-14 | Resinate Materials Group, Inc. | Improved recycle-content polyester polyols |
| WO2015171433A1 (en) | 2014-05-05 | 2015-11-12 | Resinate Materials Group, Inc. | Polyester polyols from thermoplastic polyesters and dimer fatty acids |
| US10414859B2 (en) | 2014-08-20 | 2019-09-17 | Resinate Materials Group, Inc. | High recycle content polyester polyols |
| WO2016069622A1 (en) | 2014-10-29 | 2016-05-06 | Resinate Materials Group, Inc. | High recycle content polyester polyols from hydroxy-functional ketal acids, esters or amides |
| BR112017015646A2 (pt) | 2015-01-21 | 2018-03-13 | Resinate Mat Group Inc | poliois de alto teor reciclável de poliésteres termoplásticos e lignina ou tanino |
| WO2016153780A1 (en) | 2015-03-20 | 2016-09-29 | Resinate Materials Group, Inc. | Cycloaliphatic polyester polyols from thermoplastic polyesters |
| US9522976B2 (en) | 2015-03-20 | 2016-12-20 | Resinate Materials Group, Inc. | Cycloaliphatic polyester polyols from thermoplastic polyesters |
| EP3283545A1 (en) | 2015-04-14 | 2018-02-21 | Resinate Materials Group, Inc. | Polyester polyols with increased clarity |
| US20170001946A1 (en) * | 2015-07-02 | 2017-01-05 | Sadesh Sookraj | Terephthalate derivatives and compositions thereof |
| WO2017058504A1 (en) | 2015-10-02 | 2017-04-06 | Resinate Materials Group, Inc. | High performance coatings |
| FR3092323B1 (fr) | 2019-02-01 | 2021-06-04 | Ifp Energies Now | Procédé de production d’un polyester téréphtalate à partir d’un mélange monomérique comprenant un diester |
| FR3092324B1 (fr) * | 2019-02-01 | 2021-04-23 | Ifp Energies Now | Procédé de production d’un polyester téréphtalate intégrant un procédé de dépolymérisation |
| NL2023686B1 (en) * | 2019-08-22 | 2021-04-13 | Ioniqa Tech B V | Composition of BHET and use thereof |
| US12522695B2 (en) | 2019-10-08 | 2026-01-13 | Eastman Chemical Company | Catalyst systems for crystallizable reactor grade resins with recycled content |
| KR102431854B1 (ko) * | 2019-11-08 | 2022-08-10 | 코오롱인더스트리 주식회사 | 스펀본드 부직포 및 이를 이용한 타일카페트 |
| FR3105235B1 (fr) | 2019-12-19 | 2022-10-07 | Ifp Energies Now | Procédé amélioré de dépolymérisation d’un polyester comprenant du polyéthylène téréphtalate |
| FR3105236B1 (fr) | 2019-12-19 | 2022-12-16 | Ifp Energies Now | Procédé optimisé de dépolymérisation d’un polyester comprenant du polyéthylène téréphtalate |
| IT201900025039A1 (it) | 2019-12-20 | 2021-06-20 | Garbo S R L | Processo per purificare il bis(2-idrossietil)tereftalato. |
| FR3106134B1 (fr) | 2020-01-09 | 2022-12-16 | Ifp Energies Now | Procédé optimisé de dépolymérisation par glycolyse d’un polyester comprenant du polyéthylène téréphtalate |
| US11845863B2 (en) | 2020-05-04 | 2023-12-19 | Carlisle Construction Materials, LLC | Polyurethane dispersions and their use to produce coatings and adhesives |
| KR102583652B1 (ko) * | 2020-10-26 | 2023-09-26 | 에스케이케미칼 주식회사 | 재사용 단량체를 포함하는 폴리에스테르 공중합체의 제조 방법 |
| KR102583653B1 (ko) * | 2020-11-11 | 2023-09-26 | 에스케이케미칼 주식회사 | 재사용 단량체를 포함하는 폴리에스테르 공중합체 |
| CN114656684A (zh) * | 2020-12-23 | 2022-06-24 | 科泽新材料有限公司 | 一种利用废旧pet聚酯制备高纯再生pet聚酯的方法 |
| GB2604098B (en) * | 2021-02-12 | 2025-02-19 | Poseidon Plastics Ltd | Polymerisation |
| CN115141363A (zh) * | 2021-03-30 | 2022-10-04 | 科泽新材料股份有限公司 | 一种利用废聚酯制备再生阳离子聚酯的方法 |
| FR3124186B1 (fr) | 2021-06-17 | 2024-04-12 | Ifp Energies Now | Procédé de preparation d’un monomere diester purifie et decolore par dépolymérisation d’une charge polyester |
| KR20230004123A (ko) * | 2021-06-30 | 2023-01-06 | 에스케이케미칼 주식회사 | 재사용 단량체를 포함하는 폴리에스테르 공중합체 |
| TWI810624B (zh) | 2021-08-05 | 2023-08-01 | 財團法人工業技術研究院 | 降解聚對苯二甲酸乙二酯之方法 |
| KR20230050891A (ko) * | 2021-10-08 | 2023-04-17 | 에스케이케미칼 주식회사 | 재사용 단량체를 포함하는, 압출 가공성이 개선된 폴리에스테르 공중합체 |
| KR20230072045A (ko) * | 2021-11-17 | 2023-05-24 | 에스케이케미칼 주식회사 | 재사용 비스-2-히드록시에틸테레프탈레이트를 사용한 폴리에스테르 공중합체의 제조 방법 |
| FR3130278B1 (fr) | 2021-12-10 | 2025-08-22 | Ifp Energies Now | Procede de production d’un polyester ayant une temperature de cristallisation reduite |
| FR3130804B1 (fr) | 2021-12-17 | 2025-09-26 | Ifp Energies Now | Bis(2-hydroxyethyle) terephtalate ayant une teneur en azote faible |
| KR20230132222A (ko) | 2022-03-08 | 2023-09-15 | 에스케이케미칼 주식회사 | 재생 비스-2-히드록시에틸테레프탈레이트를 이용한 폴리에스테르 수지 및 이를 포함하는 물품 |
| KR102751922B1 (ko) | 2022-04-20 | 2025-01-09 | 에스케이케미칼 주식회사 | 재생 비스(2-히드록시에틸)테레프탈레이트를 포함하는 폴리에스테르 수지 및 이를 이용한 필름 |
| US20250353985A1 (en) | 2022-05-10 | 2025-11-20 | Polymeterix AG | Monomer recycling of polyesters |
| EP4276131A1 (en) | 2022-05-10 | 2023-11-15 | Polymetrix AG | Method for the preparation of a polyester |
| IT202200016851A1 (it) | 2022-08-05 | 2024-02-05 | Chempet Srl | Processo per purificare bis(2-idrossietil)tereftalato ottenuto da depolimerizzazione di rifiuti contenenti polietilene tereftalato. |
| KR20240024420A (ko) * | 2022-08-16 | 2024-02-26 | 에스케이케미칼 주식회사 | 폴리에스테르 수지 혼합물, 이의 제조방법 및 이로부터 제조된 폴리에스테르 필름 |
| EP4421116A1 (en) * | 2023-02-22 | 2024-08-28 | Plasta Rei S.r.l. | Production of recycled polyesters from polyester waste through chemical recycling methodology |
| EP4549486A1 (en) | 2023-10-31 | 2025-05-07 | Polymetrix AG | Monomer recycling of polyesters |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL6802856A (es) | 1967-03-08 | 1968-09-09 | ||
| JPS4541215B1 (es) * | 1967-04-14 | 1970-12-24 | ||
| US3668235A (en) * | 1969-12-24 | 1972-06-06 | Teijin Ltd | Process for drying bis-({62 -hydroxyethyl) terephthalate |
| US3884850A (en) | 1970-02-13 | 1975-05-20 | Fiber Industries Inc | Continuous atmospheric depolymerization of polyester |
| JPS4915255B1 (es) * | 1970-07-23 | 1974-04-13 | ||
| JPS4886841A (es) | 1972-02-29 | 1973-11-15 | ||
| JPS4915255A (es) | 1972-06-03 | 1974-02-09 | ||
| JPS4936646A (es) | 1972-08-10 | 1974-04-05 | ||
| JPS5221498B2 (es) * | 1973-02-07 | 1977-06-10 | ||
| GB1513245A (en) * | 1974-06-18 | 1978-06-07 | Girling Ltd | Actuator assembly for vehicle brakes |
| DE2504156A1 (de) | 1975-02-01 | 1976-08-05 | Dynamit Nobel Ag | Niedermolekulare terephthalsaeure- aethylenglykolester, ihre herstellung und verwendung |
| US4046688A (en) * | 1975-10-21 | 1977-09-06 | Rohm And Haas Company | Removal of antimony from industrial streams |
| US4078143A (en) * | 1976-01-09 | 1978-03-07 | E. I. Du Pont De Nemours And Company | Process for depolymerizing waste ethylene terephthalate polyester |
| US4620032A (en) * | 1984-12-11 | 1986-10-28 | Celanese Corporation | Depolymerization of condensation polymers involving a pre-molecular weight reduction step |
| JP3303370B2 (ja) * | 1992-12-01 | 2002-07-22 | 東レ株式会社 | 芳香族ポリエステルの解重合方法 |
| DE19638549A1 (de) | 1996-09-20 | 1998-03-26 | Zimmer Ag | Zeolith-Katalysator zur Polykondensation von Polyester |
| DE19643479B4 (de) * | 1996-10-22 | 2006-04-20 | Zimmer Ag | Verfahren zur Herstellung von Polyethylenterephthalat aus Polyethylenterephthalat-Abfall |
-
1999
- 1999-12-24 KR KR1020067019510A patent/KR100740059B1/ko not_active Expired - Lifetime
- 1999-12-24 CN CNA2004100013328A patent/CN1511823A/zh active Pending
- 1999-12-24 CN CNB998114219A patent/CN1195727C/zh not_active Expired - Lifetime
- 1999-12-24 KR KR1020007009039A patent/KR100701842B1/ko not_active Expired - Lifetime
- 1999-12-24 KR KR1020067019511A patent/KR100740060B1/ko not_active Expired - Lifetime
- 1999-12-24 ID IDW20001563A patent/ID26736A/id unknown
- 1999-12-24 ES ES99961372T patent/ES2228142T3/es not_active Expired - Lifetime
- 1999-12-24 CN CNA2004100013313A patent/CN1511821A/zh active Pending
- 1999-12-24 CA CA002318761A patent/CA2318761A1/en not_active Abandoned
- 1999-12-24 US US09/622,518 patent/US6630601B1/en not_active Expired - Lifetime
- 1999-12-24 DE DE69920025T patent/DE69920025T2/de not_active Expired - Lifetime
- 1999-12-24 AU AU18005/00A patent/AU764053B2/en not_active Expired
- 1999-12-24 HK HK02101199.5A patent/HK1040236A1/zh unknown
- 1999-12-24 WO PCT/JP1999/007284 patent/WO2001010812A1/ja not_active Ceased
- 1999-12-24 AT AT99961372T patent/ATE275538T1/de not_active IP Right Cessation
- 1999-12-24 EP EP99961372A patent/EP1120394B1/en not_active Expired - Lifetime
-
2000
- 2000-01-03 TW TW089100024A patent/TW506968B/zh not_active IP Right Cessation
-
2003
- 2003-07-18 US US10/623,002 patent/US7193104B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| KR20060107859A (ko) | 2006-10-16 |
| KR20060107858A (ko) | 2006-10-16 |
| US20040019234A1 (en) | 2004-01-29 |
| ES2228142T3 (es) | 2005-04-01 |
| EP1120394B1 (en) | 2004-09-08 |
| KR100740060B1 (ko) | 2007-07-16 |
| DE69920025T2 (de) | 2005-09-08 |
| CN1511823A (zh) | 2004-07-14 |
| CN1511821A (zh) | 2004-07-14 |
| CN1195727C (zh) | 2005-04-06 |
| EP1120394A1 (en) | 2001-08-01 |
| AU764053B2 (en) | 2003-08-07 |
| TW506968B (en) | 2002-10-21 |
| CN1320113A (zh) | 2001-10-31 |
| CA2318761A1 (en) | 2001-02-04 |
| WO2001010812A9 (en) | 2001-04-26 |
| EP1120394A4 (en) | 2002-07-24 |
| KR100701842B1 (ko) | 2007-04-02 |
| KR20010086254A (ko) | 2001-09-10 |
| HK1040236A1 (zh) | 2002-05-31 |
| US7193104B2 (en) | 2007-03-20 |
| US6630601B1 (en) | 2003-10-07 |
| DE69920025D1 (de) | 2004-10-14 |
| KR100740059B1 (ko) | 2007-07-16 |
| WO2001010812A1 (en) | 2001-02-15 |
| ATE275538T1 (de) | 2004-09-15 |
| AU1800500A (en) | 2001-03-05 |
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