IL45804A - Process for the preparation of N-trimethylsilylacetamide - Google Patents

Process for the preparation of N-trimethylsilylacetamide

Info

Publication number: IL45804A
Authority: IL; Israel
Prior art keywords: reaction; carried out; acetamide; ammonia; period
Prior art date: 1973-11-14

Application number

IL45804A

Other languages

English (en)

Hebrew (he)

Other versions

IL45804A0 (en

Original Assignee

Lilly Co Eli

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-11-14

Filing date

1974-10-07

Publication date

1976-11-30

1974-10-07 Application filed by Lilly Co Eli filed Critical Lilly Co Eli

1974-12-31 Publication of IL45804A0 publication Critical patent/IL45804A0/xx

1976-11-30 Publication of IL45804A publication Critical patent/IL45804A/en

Links

238000004519 manufacturing process Methods 0.000 title claims 3
LWFWUJCJKPUZLV-UHFFFAOYSA-N n-trimethylsilylacetamide Chemical compound CC(=O)N[Si](C)(C)C LWFWUJCJKPUZLV-UHFFFAOYSA-N 0.000 title claims 2
238000000034 method Methods 0.000 claims 10
DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 claims 7
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 6
FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 claims 6
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical group ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims 3
229910021529 ammonia Inorganic materials 0.000 claims 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
239000002253 acid Substances 0.000 claims 2
IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 claims 2
239000000203 mixture Substances 0.000 claims 2
239000011541 reaction mixture Substances 0.000 claims 2
239000002904 solvent Substances 0.000 claims 2
239000012442 inert solvent Substances 0.000 claims 1
229910052757 nitrogen Inorganic materials 0.000 claims 1
238000010992 reflux Methods 0.000 claims 1
239000005051 trimethylchlorosilane Substances 0.000 claims 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/10—Compounds having one or more C—Si linkages containing nitrogen having a Si-N linkage

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)

IL45804A 1973-11-14 1974-10-07 Process for the preparation of N-trimethylsilylacetamide IL45804A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US00415697A US3839387A (en)	1973-11-14	1973-11-14	Process for preparing n-trimethyl-silylacetamide

Publications (2)

Publication Number	Publication Date
IL45804A0 IL45804A0 (en)	1974-12-31
IL45804A true IL45804A (en)	1976-11-30

Family

ID=23646801

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IL45804A IL45804A (en)	1973-11-14	1974-10-07	Process for the preparation of N-trimethylsilylacetamide

Country Status (13)

Country	Link
US (1)	US3839387A (fr)
JP (1)	JPS5082022A (fr)
BE (1)	BE821854A (fr)
CA (1)	CA1039737A (fr)
CH (1)	CH599229A5 (fr)
DE (1)	DE2453365A1 (fr)
ES (1)	ES431956A1 (fr)
FR (1)	FR2250760B1 (fr)
GB (1)	GB1485805A (fr)
IE (1)	IE39680B1 (fr)
IL (1)	IL45804A (fr)
IT (1)	IT1025664B (fr)
NL (1)	NL7414643A (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2923604A1 (de) *	1979-06-11	1980-12-18	Wacker Chemie Gmbh	Verfahren zur herstellung von silicium enthaltenden derivaten des acetamids
DE3443961C2 (de) *	1984-12-01	1986-12-11	Dynamit Nobel Ag, 5210 Troisdorf	Verfahren zur gleichzeitigen Herstellung von Carbonsäuretrimethylsilylestern und Trimethylsilylcarbonsäureamiden
DE3443960C2 (de) *	1984-12-01	1986-12-11	Dynamit Nobel Ag, 5210 Troisdorf	Verfahren zur Herstellung von Bis-trimethylsilylamiden aus Carbonsäureamiden
USRE32717E (en) *	1985-08-20	1988-07-19	Shin-Etsu Chemical Co., Ltd.	Method for the preparation of N-methyl-N-trimethylsilyl trifluoroacetamide
US4663471A (en) *	1986-08-14	1987-05-05	Shin-Etsu Chemical Co., Ltd.	Method for the preparation of N-methyl-N-trimethylsilyl trifluoroacetamide
FR2757167B1 (fr) *	1996-12-12	1999-01-22	Rhodia Chimie Sa	Synthese de bis silylamide et composition obtenue

1973
- 1973-11-14 US US00415697A patent/US3839387A/en not_active Expired - Lifetime
1974
- 1974-09-30 IE IE2023/74A patent/IE39680B1/xx unknown
- 1974-10-07 IL IL45804A patent/IL45804A/en unknown
- 1974-10-17 CA CA211,680A patent/CA1039737A/fr not_active Expired
- 1974-10-25 CH CH1432174A patent/CH599229A5/xx not_active IP Right Cessation
- 1974-11-05 BE BE150208A patent/BE821854A/fr unknown
- 1974-11-05 FR FR7436730A patent/FR2250760B1/fr not_active Expired
- 1974-11-08 NL NL7414643A patent/NL7414643A/xx not_active Application Discontinuation
- 1974-11-11 DE DE19742453365 patent/DE2453365A1/de not_active Withdrawn
- 1974-11-13 IT IT29393/74A patent/IT1025664B/it active
- 1974-11-13 GB GB49053/74A patent/GB1485805A/en not_active Expired
- 1974-11-14 ES ES431956A patent/ES431956A1/es not_active Expired
- 1974-11-14 JP JP49131839A patent/JPS5082022A/ja active Pending

Also Published As

Publication number	Publication date
IL45804A0 (en)	1974-12-31
IE39680L (en)	1975-05-14
ES431956A1 (es)	1976-10-16
IE39680B1 (en)	1978-12-06
GB1485805A (en)	1977-09-14
FR2250760A1 (fr)	1975-06-06
FR2250760B1 (fr)	1977-10-28
JPS5082022A (fr)	1975-07-03
NL7414643A (nl)	1975-05-16
CA1039737A (fr)	1978-10-03
CH599229A5 (fr)	1978-05-12
IT1025664B (it)	1978-08-30
DE2453365A1 (de)	1975-05-15
BE821854A (fr)	1975-05-05
US3839387A (en)	1974-10-01

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