JP2000219775A5 - - Google Patents
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- Publication number
- JP2000219775A5 JP2000219775A5 JP2000020188A JP2000020188A JP2000219775A5 JP 2000219775 A5 JP2000219775 A5 JP 2000219775A5 JP 2000020188 A JP2000020188 A JP 2000020188A JP 2000020188 A JP2000020188 A JP 2000020188A JP 2000219775 A5 JP2000219775 A5 JP 2000219775A5
- Authority
- JP
- Japan
- Prior art keywords
- flame
- retardant
- formula
- nitrogen compounds
- unsaturated polyester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 6
- 239000003063 flame retardant Substances 0.000 description 6
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- YUWBVKYVJWNVLE-UHFFFAOYSA-N [N].[P] Chemical class [N].[P] YUWBVKYVJWNVLE-UHFFFAOYSA-N 0.000 description 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
- 229910052794 bromium Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 description 2
- 150000004692 metal hydroxides Chemical class 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910017464 nitrogen compound Inorganic materials 0.000 description 2
- 150000002830 nitrogen compounds Chemical class 0.000 description 2
- ACVYVLVWPXVTIT-UHFFFAOYSA-M phosphinate Chemical compound [O-][PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-M 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 229920006337 unsaturated polyester resin Polymers 0.000 description 2
- DJKGDNKYTKCJKD-BPOCMEKLSA-N (1s,4r,5s,6r)-1,2,3,4,7,7-hexachlorobicyclo[2.2.1]hept-2-ene-5,6-dicarboxylic acid Chemical compound ClC1=C(Cl)[C@]2(Cl)[C@H](C(=O)O)[C@H](C(O)=O)[C@@]1(Cl)C2(Cl)Cl DJKGDNKYTKCJKD-BPOCMEKLSA-N 0.000 description 1
- SRGHNZAKTQALEA-UHFFFAOYSA-N 2,2-dimethylpropane-1,3-diol dihydrobromide Chemical compound Br.Br.OCC(C)(C)CO SRGHNZAKTQALEA-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 244000124853 Perilla frutescens Species 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- DJKGDNKYTKCJKD-UHFFFAOYSA-N chlorendic acid Chemical compound ClC1=C(Cl)C2(Cl)C(C(=O)O)C(C(O)=O)C1(Cl)C2(Cl)Cl DJKGDNKYTKCJKD-UHFFFAOYSA-N 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229920006305 unsaturated polyester Polymers 0.000 description 1
Description
【請求項１９】 請求項１〜１６のいずれか一つに記載の難燃性熱硬化性材料を製造する方法において、式（Ｉ）で表されるホスフィン酸塩および／または式（II）のジホスフィン酸塩および／またはそれのポリマーからの難燃剤を含有する熱硬化性樹脂を金属水酸化物、窒素化合物および燐−窒素化合物よりなる物質群から選択される少なくとも１種類の相乗作用成分と混合しそして得られる混合物を５０〜１５０ｂａｒの圧力および１４０〜１６０℃の温度で加工してプレプレッグスを得ることを特徴とする、上記方法。
臭素含有−または塩素含有酸および／またはアルコール成分が難燃性不飽和ポリエステル樹脂を製造するために使用されることは公知である。これらの成分の例にはヘキサクロロエンドメチレン−テトラヒドロフタル酸（ＨＥＴ酸）、四臭化フタル酸および二臭化ネオペンチルグリコールがある。三酸化アンチモンも相乗剤としてよく使用される。
特開平５−２４５８３８号公報（ＣＡ１９９３：６７２７００）では、水酸化アルミニウム、赤燐および三酸化アンチモンを臭素化樹脂と併用して難燃性を改善している。臭素含有−および塩素含有樹脂の欠点は腐蝕性ガスを炎の中で発生しそしてこれが電子部品、例えば軌道車両のリレーに重大な損傷を与え得ることである。不利な条件ではポリ塩素化−または臭素化ジベンゾダイオキシン類およびフラン類も生成し得る。それ故に難燃性でそしてハロゲン不含の不飽和ポリエステル樹脂および不飽和ポリエステル成形材料が求められている。
本発明の難燃性熱硬化性材料の別の製造方法は、式（Ｉ）で表されるホスフィン酸塩および／または式（II）のジホスフィン酸塩および／またはそれのポリマーからの難燃剤を含有する熱硬化性樹脂を金属水酸化物、窒素化合物および燐−窒素化合物よりなる物質群から選択される少なくとも１種類の相乗作用成分と混合しそして得られる混合物を５０〜１５０ｂａｒの圧力および１４０〜１６０℃の温度で加工してプレプレッグを得ることを特徴としている。
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19903707A DE19903707C2 (de) | 1999-01-30 | 1999-01-30 | Flammwidrige duroplastische Massen |
| DE19903707:8 | 1999-01-30 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2000219775A JP2000219775A (ja) | 2000-08-08 |
| JP2000219775A5 true JP2000219775A5 (ja) | 2007-03-15 |
| JP4871440B2 JP4871440B2 (ja) | 2012-02-08 |
Family
ID=7895885
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000020188A Expired - Lifetime JP4871440B2 (ja) | 1999-01-30 | 2000-01-28 | 難燃性熱硬化性材料 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6420459B1 (ja) |
| EP (1) | EP1024168B1 (ja) |
| JP (1) | JP4871440B2 (ja) |
| AT (1) | ATE238385T1 (ja) |
| DE (2) | DE19903707C2 (ja) |
| ES (1) | ES2195503T3 (ja) |
Families Citing this family (65)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19917428A1 (de) | 1999-04-19 | 2000-10-26 | Clariant Gmbh | Flammwidrige phosphormodifizierte Epoxidharze |
| US6547655B1 (en) * | 2001-06-29 | 2003-04-15 | Schaffner Manufacturing Company, Inc. | Flame-resistant buffing wheel and method |
| TWI278481B (en) * | 2002-04-16 | 2007-04-11 | Hitachi Chemical Co Ltd | Thermosetting resin composition, prepreg and laminate using the same |
| EP1386942A1 (en) * | 2002-07-25 | 2004-02-04 | Clariant GmbH | Flame retardant combination |
| DE10241126A1 (de) * | 2002-09-03 | 2004-03-25 | Clariant Gmbh | Flammschutzmittel-Stabilisator-Kombination für thermoplastische Polymere |
| DE10241373A1 (de) * | 2002-09-06 | 2004-03-18 | Clariant Gmbh | Oberflächenmodifizierte Phosphinsäuresalze |
| DE10241376A1 (de) * | 2002-09-06 | 2004-03-18 | Clariant Gmbh | Kompaktierte Flammschutzmittelzusammensetzung |
| DE10241374B3 (de) * | 2002-09-06 | 2004-02-19 | Clariant Gmbh | Staubarme, pulverförmige Flammschutzmittelzusammensetzung, Verfahren zu deren Herstellung und deren Verwendung, sowie flammgeschützte Polymerformmassen |
| DE10243231B4 (de) * | 2002-09-17 | 2004-10-28 | Clariant Gmbh | Brandschutzbeschichtung |
| DE10244576A1 (de) * | 2002-09-25 | 2004-04-08 | Clariant Gmbh | Flammwidrige duroplastische Massen |
| DE10244578A1 (de) * | 2002-09-25 | 2004-04-08 | Clariant Gmbh | Flammwidrige duroplastische Massen |
| DE10244579A1 (de) * | 2002-09-25 | 2004-04-08 | Clariant Gmbh | Flammwidrige duroplastische Massen |
| DE10304175A1 (de) * | 2003-01-28 | 2004-08-05 | Schock Gmbh | Formbare Masse, die zum Herstellen von Formteilen aushärtbar ist und aus einer solchen Masse hergestelltes Formteil |
| DE10309805B4 (de) | 2003-03-05 | 2005-07-21 | Clariant Gmbh | Flammschutzmittel-Dispersion |
| US7456235B2 (en) * | 2003-04-30 | 2008-11-25 | Henkel Corporation | Flame-retardant composition for coating powders |
| US6936646B2 (en) * | 2003-04-30 | 2005-08-30 | Henkel Corporation | Flame-retardant molding compositions |
| DE10320465A1 (de) * | 2003-05-08 | 2004-12-02 | Clariant Gmbh | Flammschutzmittel-Nanocomposite-Kombination für thermoplastische Polymere |
| DE10321297B4 (de) * | 2003-05-13 | 2005-11-10 | Clariant Gmbh | Flammwidrige duroplastische Massen, ein Verfahren zu ihrer Herstellung und ihre Verwendung |
| DE10323116A1 (de) * | 2003-05-22 | 2004-12-16 | Clariant Gmbh | Titanhaltige Phosphinat-Flammschutzmittel |
| DE10331888B4 (de) | 2003-07-14 | 2005-11-10 | Clariant Gmbh | Elastisches Belagmaterial mit verbesserten Flammschutzeigenschaften sowie ein Verfahren zu dessen Herstellung |
| DE10331887A1 (de) | 2003-07-14 | 2005-02-17 | Clariant Gmbh | Flammschutzmittel-Zubereitung |
| JP5068919B2 (ja) * | 2003-09-25 | 2012-11-07 | スリーエム イノベイティブ プロパティズ カンパニー | 発泡シート形成性組成物、熱伝導性発泡シート及びその製造方法 |
| US7294661B2 (en) | 2003-10-03 | 2007-11-13 | E.I. Du Pont De Nemours And Company | Flame resistant aromatic polyamide resin composition and articles therefrom |
| US7211639B2 (en) * | 2003-10-03 | 2007-05-01 | General Electric Company | Composition comprising functionalized poly(arylene ether) and ethylene-alkyl (meth)acrylate copolymer, method for the preparation thereof, and articles prepared therefrom |
| US8188172B2 (en) | 2003-12-17 | 2012-05-29 | Sabic Innovative Plastics Ip B.V. | Polyester compositions, method of manufacture, and uses thereof |
| US8034870B2 (en) | 2003-12-17 | 2011-10-11 | Sabic Innovative Plastics Ip B.V. | Flame-retardant polyester composition |
| US7812077B2 (en) | 2003-12-17 | 2010-10-12 | Sabic Innovative Plastics Ip B.V. | Polyester compositions, method of manufacture, and uses thereof |
| WO2005061606A1 (fr) * | 2003-12-19 | 2005-07-07 | Rhodia Engineering Plastics S.R.L. | Composition ignifugee a base de matrice thermoplastique |
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| DE102004009455A1 (de) * | 2004-02-27 | 2005-09-15 | Clariant Gmbh | Flammschutzmittel-Kombination für thermoplastische Polymere |
| DE102004035517A1 (de) * | 2004-07-22 | 2006-02-16 | Clariant Gmbh | Nanoteiliges Phosphor-haltiges Flammschutzmittel |
| DE102004035508A1 (de) * | 2004-07-22 | 2006-02-16 | Clariant Gmbh | Flammgeschützte Polymerformmassen |
| DE102004039758A1 (de) * | 2004-08-17 | 2006-03-02 | Clariant Gmbh | Brandschutzbeschichtung |
| EP1777257B1 (fr) * | 2005-10-20 | 2018-08-22 | Arkema France | Composition méthacrylique ignifugée |
| FR2892422B1 (fr) * | 2005-10-20 | 2011-08-05 | Arkema | Composition methacrylique ignifugee |
| EP1948735B1 (en) * | 2005-11-16 | 2011-01-26 | Basf Se | Flame retardant prepregs and laminates for printed circuit boards |
| US8680167B2 (en) * | 2006-01-27 | 2014-03-25 | Sabic Innovative Plastics Ip B.V. | Molding compositions containing fillers and modified polybutylene terephthalate (PBT) random copolymers derived from polyethylene terephthalate (PET) |
| US7758964B2 (en) | 2006-02-10 | 2010-07-20 | 3M Innovative Properties Company | Flame resistant covercoat for flexible circuit |
| WO2007105781A1 (en) * | 2006-03-09 | 2007-09-20 | Showa Denko K.K. | Thermosetting resin composition and uses thereof |
| DE102007001862A1 (de) | 2007-01-12 | 2008-07-17 | Clariant International Ltd. | Flammwidrige Harzformulierung und ihre Verwendung |
| ES2365987T3 (es) * | 2007-07-13 | 2011-10-14 | Italmatch Chemicals S.P.A. | Aditivo retardador de la llama libre de halógeno. |
| JP5311088B2 (ja) * | 2007-09-06 | 2013-10-09 | Ｄｉｃ株式会社 | 防水用トップコート材組成物、それを用いた土木建築構造体及びそれを用いた施工方法 |
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| EP2343335A1 (de) * | 2009-12-21 | 2011-07-13 | LANXESS Deutschland GmbH | Flammgeschützte Polymerzusammensetzungen |
| US8686072B2 (en) | 2010-06-29 | 2014-04-01 | Sabic Innovative Plastics Ip B.V. | Flame resistant polyester compositions, method of manufacture, and articles therof |
| US8716378B2 (en) | 2010-06-29 | 2014-05-06 | Sabic Innovative Plastics Ip B.V. | Flame resistant polyester compositions, method of manufacture, and articles thereof |
| JP5616163B2 (ja) * | 2010-08-19 | 2014-10-29 | 帝人株式会社 | 光学レンズ用ポリカーボネート共重合体およびそれを用いた光学レンズ |
| US8604105B2 (en) | 2010-09-03 | 2013-12-10 | Eastman Chemical Company | Flame retardant copolyester compositions |
| US9327873B2 (en) | 2010-11-09 | 2016-05-03 | Orbis Corporation | Rigid urethane self-skinning foam top frame, pallet support board, and pallet and integrally formed grommets |
| US9522760B2 (en) | 2010-11-09 | 2016-12-20 | Orbis Corporation | Rigid urethane self-skinning foam top frame, pallet support board, and pallet |
| US9145488B2 (en) | 2011-05-19 | 2015-09-29 | Chemtura Corporation | Aluminum phosphorus acid salts as epoxy resin cure inhibitors |
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| CN104610704A (zh) * | 2015-01-28 | 2015-05-13 | 清远市普塞呋磷化学有限公司 | 一种无卤阻燃酸酐固化环氧树脂组合物 |
| CN104861206B (zh) * | 2015-06-18 | 2017-12-29 | 广州金凯新材料有限公司 | 一种包覆型阻燃剂及其制备方法与应用和由其组成的高聚物组合物 |
| CN104877177B (zh) * | 2015-06-18 | 2017-12-29 | 广州金凯新材料有限公司 | 一种包覆型阻燃剂及其制备方法与应用和由其组成的模塑组合物 |
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| DE19619095A1 (de) * | 1996-05-06 | 1997-11-13 | Schill & Seilacher | Flammfeste Epoxidharze und Flammschutzmittel für Epoxidharze |
| DE19629432A1 (de) | 1996-07-22 | 1998-01-29 | Hoechst Ag | Aluminiumsalze von Phosphinsäuren |
| US5852085A (en) * | 1996-12-31 | 1998-12-22 | General Electric Company | Transparent blends of polyetherimide resins |
| DE19708726A1 (de) | 1997-03-04 | 1998-09-10 | Hoechst Ag | Flammgeschützte Polymerformmassen |
| DE19734437A1 (de) * | 1997-08-08 | 1999-02-11 | Clariant Gmbh | Synergistische Flammschutzmittel-Kombination für Polymere |
| DE19851768C2 (de) * | 1997-11-28 | 2000-03-23 | Clariant Gmbh | Verfahren zur Herstellung von Dialkylphosphinsäuresalzen |
| DE19933901A1 (de) * | 1999-07-22 | 2001-02-01 | Clariant Gmbh | Flammschutzmittel-Kombination |
-
1999
- 1999-01-30 DE DE19903707A patent/DE19903707C2/de not_active Expired - Fee Related
- 1999-12-24 EP EP99125891A patent/EP1024168B1/de not_active Expired - Lifetime
- 1999-12-24 DE DE59905175T patent/DE59905175D1/de not_active Expired - Lifetime
- 1999-12-24 AT AT99125891T patent/ATE238385T1/de not_active IP Right Cessation
- 1999-12-24 ES ES99125891T patent/ES2195503T3/es not_active Expired - Lifetime
-
2000
- 2000-01-25 US US09/491,321 patent/US6420459B1/en not_active Expired - Lifetime
- 2000-01-28 JP JP2000020188A patent/JP4871440B2/ja not_active Expired - Lifetime
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