JPH02153992A - 炭化水素系原料の水素化分解方法 - Google Patents
炭化水素系原料の水素化分解方法Info
- Publication number
- JPH02153992A JPH02153992A JP20492289A JP20492289A JPH02153992A JP H02153992 A JPH02153992 A JP H02153992A JP 20492289 A JP20492289 A JP 20492289A JP 20492289 A JP20492289 A JP 20492289A JP H02153992 A JPH02153992 A JP H02153992A
- Authority
- JP
- Japan
- Prior art keywords
- effluent
- pressure
- hydrogen
- reaction stage
- hydrocracking
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004517 catalytic hydrocracking Methods 0.000 title claims abstract description 42
- 229930195733 hydrocarbon Natural products 0.000 title claims abstract description 13
- 150000002430 hydrocarbons Chemical class 0.000 title claims abstract description 13
- 239000004215 Carbon black (E152) Substances 0.000 title claims abstract description 11
- 238000000034 method Methods 0.000 title claims description 23
- 239000002994 raw material Substances 0.000 title abstract description 16
- 239000003054 catalyst Substances 0.000 claims abstract description 55
- 238000006243 chemical reaction Methods 0.000 claims abstract description 51
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 30
- 238000000926 separation method Methods 0.000 claims abstract description 30
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000007789 gas Substances 0.000 claims abstract description 28
- 239000001257 hydrogen Substances 0.000 claims abstract description 28
- 229910052751 metal Inorganic materials 0.000 claims abstract description 18
- 239000002184 metal Substances 0.000 claims abstract description 18
- 239000007791 liquid phase Substances 0.000 claims abstract description 17
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000012071 phase Substances 0.000 claims abstract description 14
- 239000010457 zeolite Substances 0.000 claims abstract description 13
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 12
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000001875 compounds Chemical class 0.000 claims abstract description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 14
- 229910021529 ammonia Inorganic materials 0.000 claims description 11
- 238000005194 fractionation Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 238000004064 recycling Methods 0.000 claims description 2
- 238000004508 fractional distillation Methods 0.000 claims 1
- 239000000047 product Substances 0.000 description 21
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 239000003921 oil Substances 0.000 description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 7
- 229910052759 nickel Inorganic materials 0.000 description 7
- 229910000510 noble metal Inorganic materials 0.000 description 7
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 229910052750 molybdenum Inorganic materials 0.000 description 6
- 239000011733 molybdenum Substances 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 5
- 150000002739 metals Chemical class 0.000 description 5
- 229910017464 nitrogen compound Inorganic materials 0.000 description 5
- 150000002830 nitrogen compounds Chemical class 0.000 description 5
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- 229910052721 tungsten Inorganic materials 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000010779 crude oil Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000007792 gaseous phase Substances 0.000 description 3
- 239000012263 liquid product Substances 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 3
- 239000010937 tungsten Substances 0.000 description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- 239000000395 magnesium oxide Substances 0.000 description 2
- 229910052763 palladium Inorganic materials 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 125000000101 thioether group Chemical group 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229910020515 Co—W Inorganic materials 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- 229910003296 Ni-Mo Inorganic materials 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000011959 amorphous silica alumina Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000004523 catalytic cracking Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229910052570 clay Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- -1 doria Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 238000007327 hydrogenolysis reaction Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- DDTIGTPWGISMKL-UHFFFAOYSA-N molybdenum nickel Chemical compound [Ni].[Mo] DDTIGTPWGISMKL-UHFFFAOYSA-N 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- 150000002897 organic nitrogen compounds Chemical class 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 102200025801 rs179363883 Human genes 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000003079 shale oil Substances 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- YBRBMKDOPFTVDT-UHFFFAOYSA-N tert-butylamine Chemical compound CC(C)(C)N YBRBMKDOPFTVDT-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G65/00—Treatment of hydrocarbon oils by two or more hydrotreatment processes only
- C10G65/02—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only
- C10G65/10—Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural serial stages only including only cracking steps
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB888819122A GB8819122D0 (en) | 1988-08-11 | 1988-08-11 | Process for hydrocracking of hydrocarbonaceous feedstock |
| GB8819122.6 | 1988-08-11 | ||
| CA000604067A CA1320925C (fr) | 1989-06-27 | 1989-06-27 | Procede d'hydrocraquage d'une charge d'alimentation hydrocarbonee |
| CA604067 | 1989-06-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH02153992A true JPH02153992A (ja) | 1990-06-13 |
Family
ID=25672845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP20492289A Pending JPH02153992A (ja) | 1988-08-11 | 1989-08-09 | 炭化水素系原料の水素化分解方法 |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0354623B1 (fr) |
| JP (1) | JPH02153992A (fr) |
| AU (1) | AU615565B2 (fr) |
| DE (1) | DE68901696T2 (fr) |
| ES (1) | ES2032103T3 (fr) |
| SG (1) | SG45293G (fr) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009179795A (ja) * | 2001-06-28 | 2009-08-13 | Chevron Usa Inc | 原油脱硫 |
| JP2019534348A (ja) * | 2016-09-30 | 2019-11-28 | ヒンドゥスタン ペトロリアム コーポレーション リミテッド | 重質炭化水素の等級改善プロセス |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1482023B1 (fr) * | 2000-11-11 | 2008-04-09 | Haldor Topsoe A/S | Procédé permettant d'adapter des réacteurs d'hydrocraquage existants |
| US7354560B2 (en) | 2006-01-31 | 2008-04-08 | Haldor Topsoe A/S | Process for the production of hydrogen |
| CN104650974B (zh) * | 2013-11-20 | 2016-08-17 | 中国石油化工股份有限公司 | 降低轻馏分产品硫含量的加氢裂化工艺方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3365388A (en) * | 1965-06-08 | 1968-01-23 | Chevron Res | Multistage residuum hydroconversion process |
| DE1770267A1 (de) * | 1967-04-25 | 1971-12-23 | Atlantic Richfield Co | Verfahren zur Entschwefelung von Erdoelprodukten |
| US3554898A (en) * | 1968-08-29 | 1971-01-12 | Union Oil Co | Recycle hydrocracking process for converting heavy oils to middle distillates |
| NL7605356A (nl) * | 1975-05-21 | 1976-11-23 | Inst Francais Du Petrole | Werkwijze voor het hydrokraken van koolwater- stofolien. |
-
1989
- 1989-08-08 EP EP19890202059 patent/EP0354623B1/fr not_active Expired
- 1989-08-08 ES ES89202059T patent/ES2032103T3/es not_active Expired - Lifetime
- 1989-08-08 DE DE1989601696 patent/DE68901696T2/de not_active Expired - Lifetime
- 1989-08-09 AU AU39454/89A patent/AU615565B2/en not_active Ceased
- 1989-08-09 JP JP20492289A patent/JPH02153992A/ja active Pending
-
1993
- 1993-04-14 SG SG45293A patent/SG45293G/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009179795A (ja) * | 2001-06-28 | 2009-08-13 | Chevron Usa Inc | 原油脱硫 |
| JP2019534348A (ja) * | 2016-09-30 | 2019-11-28 | ヒンドゥスタン ペトロリアム コーポレーション リミテッド | 重質炭化水素の等級改善プロセス |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2032103T3 (es) | 1993-01-01 |
| EP0354623B1 (fr) | 1992-06-03 |
| DE68901696D1 (de) | 1992-07-09 |
| AU615565B2 (en) | 1991-10-03 |
| AU3945489A (en) | 1990-02-15 |
| EP0354623A1 (fr) | 1990-02-14 |
| SG45293G (en) | 1993-06-25 |
| DE68901696T2 (de) | 1992-12-17 |
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