JPH0566958B2 - - Google Patents

Info

Publication number: JPH0566958B2
Authority: JP; Japan
Prior art keywords: phosphoric acid; reaction; alcohol; acid ester; monoester
Prior art date: 1985-08-07
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

JP17393485A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6233190A (ja

Inventor

Masatoshi Takahashi

Shunsuke Ikemori

Koichi Fukuda

Yukiro Kamata

Mitsunobu Takada

Seijiro Myakoshi

Koji Onoda

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Myoshi Oil and Fat Co Ltd

Original Assignee

Myoshi Oil and Fat Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-08-07

Filing date

1985-08-07

Publication date

1993-09-22

1985-08-07 Application filed by Myoshi Oil and Fat Co Ltd filed Critical Myoshi Oil and Fat Co Ltd

1985-08-07 Priority to JP17393485A priority Critical patent/JPS6233190A/ja

1987-02-13 Publication of JPS6233190A publication Critical patent/JPS6233190A/ja

1993-09-22 Publication of JPH0566958B2 publication Critical patent/JPH0566958B2/ja

Status Granted legal-status Critical Current

Links

NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 69
DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 claims description 40
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 35
150000003014 phosphoric acid esters Chemical class 0.000 claims description 30
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 26
238000006243 chemical reaction Methods 0.000 claims description 25
-1 aliphatic alcohols Chemical class 0.000 claims description 23
238000004519 manufacturing process Methods 0.000 claims description 13
238000005886 esterification reaction Methods 0.000 claims description 11
238000000034 method Methods 0.000 claims description 10
DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 8
238000007664 blowing Methods 0.000 claims description 8
235000011007 phosphoric acid Nutrition 0.000 description 38
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
238000006386 neutralization reaction Methods 0.000 description 9
150000005690 diesters Chemical class 0.000 description 8
239000011541 reaction mixture Substances 0.000 description 8
239000003599 detergent Substances 0.000 description 7
150000002148 esters Chemical class 0.000 description 7
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
150000001298 alcohols Chemical class 0.000 description 6
239000012670 alkaline solution Substances 0.000 description 6
125000004432 carbon atom Chemical group C* 0.000 description 6
239000003795 chemical substances by application Substances 0.000 description 6
TVACALAUIQMRDF-UHFFFAOYSA-N dodecyl dihydrogen phosphate Chemical group CCCCCCCCCCCCOP(O)(O)=O TVACALAUIQMRDF-UHFFFAOYSA-N 0.000 description 6
150000002440 hydroxy compounds Chemical class 0.000 description 6
230000007423 decrease Effects 0.000 description 5
LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 5
238000004448 titration Methods 0.000 description 5
125000000217 alkyl group Chemical group 0.000 description 4
230000000052 comparative effect Effects 0.000 description 4
230000035484 reaction time Effects 0.000 description 4
229920006395 saturated elastomer Polymers 0.000 description 4
239000002453 shampoo Substances 0.000 description 4
238000010793 Steam injection (oil industry) Methods 0.000 description 3
239000000654 additive Substances 0.000 description 3
125000002947 alkylene group Chemical group 0.000 description 3
239000002216 antistatic agent Substances 0.000 description 3
239000007864 aqueous solution Substances 0.000 description 3
239000003995 emulsifying agent Substances 0.000 description 3
239000000835 fiber Substances 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
GOQYKNQRPGWPLP-UHFFFAOYSA-N heptadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 3
JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
239000010687 lubricating oil Substances 0.000 description 3
230000000865 phosphorylative effect Effects 0.000 description 3
230000003449 preventive effect Effects 0.000 description 3
KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 2
230000000694 effects Effects 0.000 description 2
235000021323 fish oil Nutrition 0.000 description 2
238000005187 foaming Methods 0.000 description 2
230000007062 hydrolysis Effects 0.000 description 2
238000006460 hydrolysis reaction Methods 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
XGFDHKJUZCCPKQ-UHFFFAOYSA-N nonadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCO XGFDHKJUZCCPKQ-UHFFFAOYSA-N 0.000 description 2
ZWRUINPWMLAQRD-UHFFFAOYSA-N nonan-1-ol Chemical compound CCCCCCCCCO ZWRUINPWMLAQRD-UHFFFAOYSA-N 0.000 description 2
GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
REIUXOLGHVXAEO-UHFFFAOYSA-N pentadecan-1-ol Chemical compound CCCCCCCCCCCCCCCO REIUXOLGHVXAEO-UHFFFAOYSA-N 0.000 description 2
229910052698 phosphorus Inorganic materials 0.000 description 2
239000011574 phosphorus Substances 0.000 description 2
239000002994 raw material Substances 0.000 description 2
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
239000000243 solution Substances 0.000 description 2
239000000126 substance Substances 0.000 description 2
HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 description 2
KJIOQYGWTQBHNH-UHFFFAOYSA-N undecanol Chemical compound CCCCCCCCCCCO KJIOQYGWTQBHNH-UHFFFAOYSA-N 0.000 description 2
ALSTYHKOOCGGFT-KTKRTIGZSA-N (9Z)-octadecen-1-ol Chemical compound CCCCCCCC\C=C/CCCCCCCCO ALSTYHKOOCGGFT-KTKRTIGZSA-N 0.000 description 1
XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 description 1
BWDBEAQIHAEVLV-UHFFFAOYSA-N 6-methylheptan-1-ol Chemical compound CC(C)CCCCCO BWDBEAQIHAEVLV-UHFFFAOYSA-N 0.000 description 1
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
235000019484 Rapeseed oil Nutrition 0.000 description 1
229960000541 cetyl alcohol Drugs 0.000 description 1
235000019864 coconut oil Nutrition 0.000 description 1
239000003240 coconut oil Substances 0.000 description 1
238000004040 coloring Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000001877 deodorizing effect Effects 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
239000003814 drug Substances 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
229930195729 fatty acid Natural products 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
229940043348 myristyl alcohol Drugs 0.000 description 1
239000003921 oil Substances 0.000 description 1
235000019198 oils Nutrition 0.000 description 1
229940055577 oleyl alcohol Drugs 0.000 description 1
XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
SMYREFDDLSTNKQ-UHFFFAOYSA-N oxocan-2-ol Chemical compound OC1CCCCCCO1 SMYREFDDLSTNKQ-UHFFFAOYSA-N 0.000 description 1
239000010452 phosphate Substances 0.000 description 1
150000003016 phosphoric acids Chemical class 0.000 description 1
229910001961 silver nitrate Inorganic materials 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
239000003760 tallow Substances 0.000 description 1
229940087291 tridecyl alcohol Drugs 0.000 description 1
150000005691 triesters Chemical class 0.000 description 1
229940057402 undecyl alcohol Drugs 0.000 description 1
239000004711 α-olefin Substances 0.000 description 1

JP17393485A 1985-08-07 1985-08-07 リン酸エステルの製造方法 Granted JPS6233190A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP17393485A JPS6233190A (ja)	1985-08-07	1985-08-07	リン酸エステルの製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP17393485A JPS6233190A (ja)	1985-08-07	1985-08-07	リン酸エステルの製造方法

Publications (2)

Publication Number	Publication Date
JPS6233190A JPS6233190A (ja)	1987-02-13
JPH0566958B2 true JPH0566958B2 (th)	1993-09-22

Family

ID=15969776

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP17393485A Granted JPS6233190A (ja)	1985-08-07	1985-08-07	リン酸エステルの製造方法

Country Status (1)

Country	Link
JP (1)	JPS6233190A (th)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP3115489B2 (ja) *	1994-09-20	2000-12-04	花王株式会社	リン酸モノエステルの製造方法
EP0796264B1 (en) *	1994-12-09	2003-12-10	Kao Corporation	Process for the preparation of phosophoric monoester
CN109879906B (zh) *	2019-04-02	2021-05-07	上海多纶化工有限公司	磷酸酯的制备方法

1985
- 1985-08-07 JP JP17393485A patent/JPS6233190A/ja active Granted

Also Published As

Publication number	Publication date
JPS6233190A (ja)	1987-02-13

Legal Events

Date	Code	Title	Description
2004-09-22	LAPS	Cancellation because of no payment of annual fees

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