JPH0717657B2 - 再循環を伴なうメタノール−けい素反応によるトリメトキシシランの製造 - Google Patents

再循環を伴なうメタノール−けい素反応によるトリメトキシシランの製造

Info

Publication number
JPH0717657B2
JPH0717657B2 JP3058023A JP5802391A JPH0717657B2 JP H0717657 B2 JPH0717657 B2 JP H0717657B2 JP 3058023 A JP3058023 A JP 3058023A JP 5802391 A JP5802391 A JP 5802391A JP H0717657 B2 JPH0717657 B2 JP H0717657B2
Authority
JP
Japan
Prior art keywords
methanol
reactor
trimethoxysilane
silicon
azeotrope
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP3058023A
Other languages
English (en)
Japanese (ja)
Other versions
JPH06287195A (ja
Inventor
ローレンス・ギルバート・ムーデイ
トマス・エツジワース・チルドレス
ロバート・ルイス・ピトロロ
ジエイムズ・スチーブン・リツチヤー
ロナルド・ポール・レイチリター
Original Assignee
ユニオン・カーバイド・ケミカルズ・アンド・プラスティックス・カンパニー・インコーポレイテッド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ユニオン・カーバイド・ケミカルズ・アンド・プラスティックス・カンパニー・インコーポレイテッド filed Critical ユニオン・カーバイド・ケミカルズ・アンド・プラスティックス・カンパニー・インコーポレイテッド
Publication of JPH06287195A publication Critical patent/JPH06287195A/ja
Publication of JPH0717657B2 publication Critical patent/JPH0717657B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/20—Purification, separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/025—Silicon compounds without C-silicon linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/04—Esters of silicic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
JP3058023A 1990-06-21 1991-02-28 再循環を伴なうメタノール−けい素反応によるトリメトキシシランの製造 Expired - Lifetime JPH0717657B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US541516 1990-06-21
US07/541,516 US4999446A (en) 1990-06-21 1990-06-21 Trimethoxysilane preparation via the methanol-silicon reaction with recycle

Publications (2)

Publication Number Publication Date
JPH06287195A JPH06287195A (ja) 1994-10-11
JPH0717657B2 true JPH0717657B2 (ja) 1995-03-01

Family

ID=24159909

Family Applications (1)

Application Number Title Priority Date Filing Date
JP3058023A Expired - Lifetime JPH0717657B2 (ja) 1990-06-21 1991-02-28 再循環を伴なうメタノール−けい素反応によるトリメトキシシランの製造

Country Status (10)

Country Link
US (1) US4999446A (2)
EP (1) EP0462359B1 (2)
JP (1) JPH0717657B2 (2)
KR (1) KR950007594B1 (2)
AT (1) ATE121747T1 (2)
BR (1) BR9100827A (2)
CA (1) CA2037347C (2)
DE (1) DE69109187T2 (2)
ES (1) ES2071142T3 (2)
TW (1) TW222635B (2)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08301025A (ja) * 1995-04-28 1996-11-19 Denken:Kk 自動車等のナンバープレート

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5084590A (en) * 1991-06-24 1992-01-28 Union Carbide Chemicals & Plastics Technology Corporation Trimethoxysilane preparation via the methanol-silicon reaction using a continuous process and multiple reactors
US5166384A (en) * 1992-04-07 1992-11-24 Union Carbide Chemicals & Plastics Technology Corporation Method for the removal of siloxane dissolved in the solvent employed in the preparation of trimethoxysilane via methanol-silicon metal reaction
US5362897A (en) * 1993-04-30 1994-11-08 Toagosei Chemical Industry Co., Ltd. Process for producing trialkoxysilanes
DE4438032C2 (de) 1994-10-25 2001-09-27 Degussa Verfahren zur Herstellung von Hydrogenalkoxysilanen
BE1010603A3 (fr) * 1995-09-08 1998-11-03 Kaneka Corp Procede de purification de composes du type silane.
US5783720A (en) 1996-10-10 1998-07-21 Osi Specialties, Inc. Surface-active additives in the direct synthesis of trialkoxysilanes
US6090965A (en) * 1998-04-02 2000-07-18 Osi Specialties, Inc. Removal of dissolved silicates from alcohol-silicon direct synthesis solvents
RU2157375C1 (ru) * 1999-03-31 2000-10-10 Государственный научный центр Российской Федерации Государственный научно-исследовательский институт химии и технологии элементоорганических соединений Способ получения алкоксисиланов
DE19947591A1 (de) 1999-10-04 2001-04-12 Basf Ag Verfahren zur Isolierung von Trimethoxysilan aus einer TMS-Methanol-Mischung
DE10025367A1 (de) * 2000-05-23 2001-12-13 Basf Ag Frisch gefälltes CuO als Katalysator für die Trialkoxysilan-Synthese
US7858818B2 (en) * 2001-01-31 2010-12-28 Momentive Performance Materials Inc. Nanosized copper catalyst precursors for the direct synthesis of trialkoxysilanes
US7339068B2 (en) 2001-01-31 2008-03-04 Momentive Performance Materials Inc. Nanosized copper catalyst precursors for the direct synthesis of trialkoxysilanes
US6580000B1 (en) 2002-06-06 2003-06-17 Ak Research Company Process for the manufacture of alkoxysilanes and alkoxy orthosilicates
US6872845B2 (en) * 2003-03-03 2005-03-29 General Electric Company Process for making haloorganoalkoxysilanes
US7652164B2 (en) * 2005-09-13 2010-01-26 Momentive Performance Materials Inc. Process for the direct synthesis of trialkoxysilane
US7365220B2 (en) * 2005-09-29 2008-04-29 Momentive Performance Materials Inc. Process for the recovery of alkoxysilanes obtained from the direct reaction of silicon with alkanols
US7645894B2 (en) * 2006-04-22 2010-01-12 Bernard Kanner Direct process for making cyclic dimethylsiloxane oligomers
US7429672B2 (en) * 2006-06-09 2008-09-30 Momentive Performance Materials Inc. Process for the direct synthesis of trialkoxysilane
US8153566B2 (en) * 2008-09-30 2012-04-10 Cherron Oronite Company LLC Lubricating oil compositions
US8197782B2 (en) 2010-02-08 2012-06-12 Momentive Performance Materials Method for making high purity metal oxide particles and materials made thereof
US8933001B2 (en) 2010-03-31 2015-01-13 Chevron Oronite Company Llc Method for improving fluorocarbon elastomer seal compatibility
US8901050B2 (en) 2010-03-31 2014-12-02 Chevron Oronite Company Llc Method for improving copper corrosion performance
CN103717531A (zh) 2011-07-29 2014-04-09 莫门蒂夫性能材料股份有限公司 制造高质量金属氧化物颗粒的方法和制造其的材料
JP6538726B2 (ja) * 2014-06-11 2019-07-03 ダウ シリコーンズ コーポレーション 気体及び液体を反応させる膜接触器を使用して有機ケイ素生成物を生成する方法
DE102016206429A1 (de) * 2016-04-15 2017-10-19 Robert Bosch Gmbh Verfahren zur Steuerung einer Fördereinheit eines Hochdruckeinspritzsystems einer Brennkraftmaschine
WO2024220295A1 (en) 2023-04-19 2024-10-24 Momentive Performance Materials Inc. Direct synthesis of alkoxysilanes using copper-aluminum alloy catalysts

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2473260A (en) * 1946-06-26 1949-06-14 Gen Electric Preparation of tetramethyl silicate
US3072700A (en) * 1959-08-07 1963-01-08 Union Carbide Corp Process for producing silanes
BE789535A (fr) * 1971-09-30 1973-01-15 Tokyo Shibaura Electric Co Procede de fabrication d'alkoxysilanes
JPS54163529A (en) * 1978-06-13 1979-12-26 Mitsubishi Chem Ind Production of alkoxysilane
JPS5511538A (en) * 1978-07-11 1980-01-26 Mitsubishi Chem Ind Ltd Production of methoxysilane
US4288604A (en) * 1980-05-19 1981-09-08 Stauffer Chemical Company Method for the production of tetraalkyl silicates
US4447632A (en) * 1983-04-18 1984-05-08 Union Carbide Corporation Process for production of alkyl silicates from silicon metal
US4487949A (en) * 1983-11-22 1984-12-11 Union Carbide Corporation Process for the preparation of alkyl silicates
JPS611694A (ja) * 1984-06-13 1986-01-07 Shin Etsu Chem Co Ltd トリアルコキシシランの製造方法
JPS6327993A (ja) * 1986-07-21 1988-02-05 Omron Tateisi Electronics Co Ｉｃカ−ド読取書込装置
CA1323037C (en) * 1987-02-23 1993-10-12 Yoshiro Ohta Process for the production of trialkoxysilanes
US4727173A (en) * 1987-03-31 1988-02-23 Union Carbide Corporation Process for producing trialkoxysilanes from the reaction of silicon metal and alcohol
US4761492A (en) * 1987-09-28 1988-08-02 Union Carbide Corporation Process for recovering trimethoxysilane from a trimethoxysilane and methanol mixture
US4762939A (en) * 1987-09-30 1988-08-09 Union Carbide Corporation Process for trialkoxysilane/tetraalkoxysilane mixtures from silicon metal and alcohol

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08301025A (ja) * 1995-04-28 1996-11-19 Denken:Kk 自動車等のナンバープレート

Also Published As

Publication number Publication date
US4999446A (en) 1991-03-12
TW222635B (2) 1994-04-21
ES2071142T3 (es) 1995-06-16
CA2037347C (en) 1995-08-01
KR920000771A (ko) 1992-01-29
ATE121747T1 (de) 1995-05-15
DE69109187D1 (de) 1995-06-01
BR9100827A (pt) 1992-04-07
JPH06287195A (ja) 1994-10-11
EP0462359A1 (en) 1991-12-27
CA2037347A1 (en) 1991-12-22
KR950007594B1 (ko) 1995-07-12
EP0462359B1 (en) 1995-04-26
DE69109187T2 (de) 1995-08-31

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