JPH11179115A - スラリーからの結晶回収方法および装置 - Google Patents
スラリーからの結晶回収方法および装置Info
- Publication number
- JPH11179115A JPH11179115A JP9355396A JP35539697A JPH11179115A JP H11179115 A JPH11179115 A JP H11179115A JP 9355396 A JP9355396 A JP 9355396A JP 35539697 A JP35539697 A JP 35539697A JP H11179115 A JPH11179115 A JP H11179115A
- Authority
- JP
- Japan
- Prior art keywords
- cake
- filter medium
- slurry
- rotary
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002002 slurry Substances 0.000 title claims abstract description 62
- 239000013078 crystal Substances 0.000 title claims abstract description 53
- 238000000034 method Methods 0.000 title claims abstract description 23
- 238000005406 washing Methods 0.000 claims abstract description 56
- 238000001914 filtration Methods 0.000 claims abstract description 31
- 239000007788 liquid Substances 0.000 claims description 47
- 238000004140 cleaning Methods 0.000 claims description 46
- 239000002699 waste material Substances 0.000 claims description 11
- 230000000694 effects Effects 0.000 abstract description 4
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 28
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
- 239000007789 gas Substances 0.000 description 13
- 239000000706 filtrate Substances 0.000 description 12
- 238000007254 oxidation reaction Methods 0.000 description 12
- 239000007921 spray Substances 0.000 description 11
- 230000003647 oxidation Effects 0.000 description 10
- 238000000926 separation method Methods 0.000 description 7
- 230000002411 adverse Effects 0.000 description 6
- 238000000746 purification Methods 0.000 description 5
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 4
- 239000012535 impurity Substances 0.000 description 3
- 238000002347 injection Methods 0.000 description 3
- 239000007924 injection Substances 0.000 description 3
- 238000003825 pressing Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 229910001882 dioxygen Inorganic materials 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000000967 suction filtration Methods 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- -1 aromatic dicarboxylic acids Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000011085 pressure filtration Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 1
- 229960001755 resorcinol Drugs 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Landscapes
- Processing Of Solid Wastes (AREA)
- Filtration Of Liquid (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9355396A JPH11179115A (ja) | 1997-12-24 | 1997-12-24 | スラリーからの結晶回収方法および装置 |
| IDP981683A ID21868A (id) | 1997-12-24 | 1998-12-23 | Metode dan alat untuk memperoleh kembali kristal-kristal dari bubur |
| CN 98111682 CN1233521A (zh) | 1997-12-24 | 1998-12-24 | 从悬浮液中回收结晶物的方法和装置 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9355396A JPH11179115A (ja) | 1997-12-24 | 1997-12-24 | スラリーからの結晶回収方法および装置 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH11179115A true JPH11179115A (ja) | 1999-07-06 |
Family
ID=18443701
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9355396A Pending JPH11179115A (ja) | 1997-12-24 | 1997-12-24 | スラリーからの結晶回収方法および装置 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JPH11179115A (id) |
| CN (1) | CN1233521A (id) |
| ID (1) | ID21868A (id) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000071226A1 (en) * | 1999-05-24 | 2000-11-30 | Baker Hughes Incorporated | Pressure filtration device and method employing a depressurizing chamber and material transport |
| US6655531B1 (en) | 2000-05-23 | 2003-12-02 | Baker Hughes Incorporated | Pressure filtration device |
| JP2006265124A (ja) * | 2005-03-22 | 2006-10-05 | Mitsui Chemicals Inc | スラリーから結晶を回収する方法 |
| WO2007135738A1 (ja) * | 2006-05-24 | 2007-11-29 | Mitsubishi Kakoki Kaisha, Ltd. | 結晶成分の回収方法及び結晶成分の回収システム |
| JP2008504112A (ja) * | 2004-06-23 | 2008-02-14 | イーストマン ケミカル カンパニー | 加圧濾過を用いたカルボン酸合成における母液からの不純物の除去方法 |
| JP2010528100A (ja) * | 2007-05-31 | 2010-08-19 | ダウ イタリア ソチエタ レスポンサビリタ リミテ | テレフタル酸の回収のための改善された方法 |
| DE102012206590A1 (de) | 2012-04-20 | 2013-10-24 | Coperion Gmbh | Verfahren zum Betrieb einer Zellenradschleuse sowie Zellenradschleuse zur Durchführung des Verfahrens |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3292898A1 (en) * | 2016-09-12 | 2018-03-14 | Sulzer Chemtech AG | Wash column apparatus with a static grid element for the use in a suspension crystallization process |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01299618A (ja) * | 1988-05-27 | 1989-12-04 | Mitsui Petrochem Ind Ltd | スラリーから結晶を回収する方法 |
| JPH0451428U (id) * | 1990-09-05 | 1992-04-30 | ||
| JPH06327915A (ja) * | 1993-05-24 | 1994-11-29 | Mitsui Petrochem Ind Ltd | スラリーから結晶を回収する方法及び装置 |
-
1997
- 1997-12-24 JP JP9355396A patent/JPH11179115A/ja active Pending
-
1998
- 1998-12-23 ID IDP981683A patent/ID21868A/id unknown
- 1998-12-24 CN CN 98111682 patent/CN1233521A/zh active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01299618A (ja) * | 1988-05-27 | 1989-12-04 | Mitsui Petrochem Ind Ltd | スラリーから結晶を回収する方法 |
| JPH0451428U (id) * | 1990-09-05 | 1992-04-30 | ||
| JPH06327915A (ja) * | 1993-05-24 | 1994-11-29 | Mitsui Petrochem Ind Ltd | スラリーから結晶を回収する方法及び装置 |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000071226A1 (en) * | 1999-05-24 | 2000-11-30 | Baker Hughes Incorporated | Pressure filtration device and method employing a depressurizing chamber and material transport |
| US6655531B1 (en) | 2000-05-23 | 2003-12-02 | Baker Hughes Incorporated | Pressure filtration device |
| JP2008504112A (ja) * | 2004-06-23 | 2008-02-14 | イーストマン ケミカル カンパニー | 加圧濾過を用いたカルボン酸合成における母液からの不純物の除去方法 |
| JP2006265124A (ja) * | 2005-03-22 | 2006-10-05 | Mitsui Chemicals Inc | スラリーから結晶を回収する方法 |
| WO2007135738A1 (ja) * | 2006-05-24 | 2007-11-29 | Mitsubishi Kakoki Kaisha, Ltd. | 結晶成分の回収方法及び結晶成分の回収システム |
| JP4850904B2 (ja) * | 2006-05-24 | 2012-01-11 | 三菱化工機株式会社 | 結晶成分の回収方法及び結晶成分の回収システム |
| JP2010528100A (ja) * | 2007-05-31 | 2010-08-19 | ダウ イタリア ソチエタ レスポンサビリタ リミテ | テレフタル酸の回収のための改善された方法 |
| JP2014221791A (ja) * | 2007-05-31 | 2014-11-27 | ダウ イタリア ソチエタ レスポンサビリタ リミテ | テレフタル酸の回収のための改善された方法 |
| DE102012206590A1 (de) | 2012-04-20 | 2013-10-24 | Coperion Gmbh | Verfahren zum Betrieb einer Zellenradschleuse sowie Zellenradschleuse zur Durchführung des Verfahrens |
Also Published As
| Publication number | Publication date |
|---|---|
| ID21868A (id) | 1999-08-05 |
| CN1233521A (zh) | 1999-11-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20050530 |
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| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20050607 |
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| A521 | Written amendment |
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| A02 | Decision of refusal |
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