JPS55735A - Preparation of diphenylamine acetone condensate - Google Patents
Preparation of diphenylamine acetone condensateInfo
- Publication number
- JPS55735A JPS55735A JP7399678A JP7399678A JPS55735A JP S55735 A JPS55735 A JP S55735A JP 7399678 A JP7399678 A JP 7399678A JP 7399678 A JP7399678 A JP 7399678A JP S55735 A JPS55735 A JP S55735A
- Authority
- JP
- Japan
- Prior art keywords
- water
- diphenylamine
- condensate
- solvent
- acetone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Phenolic Resins Or Amino Resins (AREA)
Abstract
PURPOSE: To prepare a diphenylamine.acetone condensate under atmospheric pressure, having comparable anti-oxidant activity to the condensate prepared under high pressure, by condensing diphenylamine with acetone in the presence of a solvent which is slightly soluble to water and forms an azeotripic mixture with water, while removing the produced water from the system.
CONSTITUTION: Diphenylamine is condensed with acetone in the presence of a solvent which is slightly soluble to water and forms an azeotropic mixture with water, pref. an aromatic hydrocarbon having a boiling point of 50W200°C , esp. 100W170°C, pref. at a reaction temperature of 100W300°C, esp, 150W280°C, under atmospheric pressure, while distilling off the produced water as an azeotropic mixture with the solvent, to afford a condensate having a viscosity of 100W20,000 cps at 25°C. The high reaction temperature results in the formation of resinous materials.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7399678A JPS55735A (en) | 1978-06-19 | 1978-06-19 | Preparation of diphenylamine acetone condensate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7399678A JPS55735A (en) | 1978-06-19 | 1978-06-19 | Preparation of diphenylamine acetone condensate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS55735A true JPS55735A (en) | 1980-01-07 |
Family
ID=13534238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7399678A Pending JPS55735A (en) | 1978-06-19 | 1978-06-19 | Preparation of diphenylamine acetone condensate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS55735A (en) |
-
1978
- 1978-06-19 JP JP7399678A patent/JPS55735A/en active Pending
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