JPS5592400A - Purification of stevioside - Google Patents
Purification of steviosideInfo
- Publication number
- JPS5592400A JPS5592400A JP16306778A JP16306778A JPS5592400A JP S5592400 A JPS5592400 A JP S5592400A JP 16306778 A JP16306778 A JP 16306778A JP 16306778 A JP16306778 A JP 16306778A JP S5592400 A JPS5592400 A JP S5592400A
- Authority
- JP
- Japan
- Prior art keywords
- stevioside
- solvent
- phase
- octafluoro
- pentanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 title abstract 5
- 229940013618 stevioside Drugs 0.000 title abstract 5
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 title abstract 5
- 235000019202 steviosides Nutrition 0.000 title abstract 5
- 238000000746 purification Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 abstract 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- JUGSKHLZINSXPQ-UHFFFAOYSA-N 2,2,3,3,4,4,5,5-octafluoropentan-1-ol Chemical compound OCC(F)(F)C(F)(F)C(F)(F)C(F)F JUGSKHLZINSXPQ-UHFFFAOYSA-N 0.000 abstract 2
- 239000008346 aqueous phase Substances 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 239000013078 crystal Substances 0.000 abstract 2
- 239000012071 phase Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- AQYSYJUIMQTRMV-UHFFFAOYSA-N hypofluorous acid Chemical compound FO AQYSYJUIMQTRMV-UHFFFAOYSA-N 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Landscapes
- Saccharide Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16306778A JPS5592400A (en) | 1978-12-29 | 1978-12-29 | Purification of stevioside |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16306778A JPS5592400A (en) | 1978-12-29 | 1978-12-29 | Purification of stevioside |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5592400A true JPS5592400A (en) | 1980-07-12 |
Family
ID=15766544
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP16306778A Pending JPS5592400A (en) | 1978-12-29 | 1978-12-29 | Purification of stevioside |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5592400A (ja) |
Cited By (53)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
| US8257948B1 (en) | 2011-02-17 | 2012-09-04 | Purecircle Usa | Method of preparing alpha-glucosyl Stevia composition |
| US8299224B2 (en) | 2009-10-15 | 2012-10-30 | Purecircle Sdn Bhd | High-purity Rebaudioside D |
| US8318459B2 (en) | 2011-02-17 | 2012-11-27 | Purecircle Usa | Glucosyl stevia composition |
| US8334006B2 (en) | 2005-10-11 | 2012-12-18 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8337927B2 (en) | 2005-10-11 | 2012-12-25 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8414950B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie table top tablet containing the same |
| US8414952B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie diet cookies containing the same |
| US8414949B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie yogurt containing the same |
| US8414951B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie soy sauce containing the same |
| US8414948B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie ice cream containing the same |
| US8420147B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie cake containing the same |
| US8420146B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie bread containing the same |
| US8507022B2 (en) | 2009-10-15 | 2013-08-13 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same |
| US8512790B2 (en) | 2009-10-15 | 2013-08-20 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie chocolate containing the same |
| US8568818B2 (en) | 2009-10-15 | 2013-10-29 | Pure Circle Sdn Bhd | High-purity Rebaudioside D and low-calorie carbonated drink containing the same |
| US8574656B2 (en) | 2009-10-15 | 2013-11-05 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie fruit juice containing the same |
| EP2708548A2 (en) | 2009-10-15 | 2014-03-19 | Purecircle SDN BHD | High-Purity Rebaudioside D and Applications |
| US8790730B2 (en) | 2005-10-11 | 2014-07-29 | Purecircle Usa | Process for manufacturing a sweetener and use thereof |
| US8916138B2 (en) | 2009-10-15 | 2014-12-23 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie tooth paste composition containing the same |
| US8937168B2 (en) | 2007-01-22 | 2015-01-20 | Cargill, Incorporated | Method of producing purified rebaudioside A compositions using solvent/antisolvent crystallization |
| US9029426B2 (en) | 2010-12-13 | 2015-05-12 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
| US9101160B2 (en) | 2005-11-23 | 2015-08-11 | The Coca-Cola Company | Condiments with high-potency sweetener |
| US9131718B2 (en) | 2009-06-16 | 2015-09-15 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US9578895B2 (en) | 2010-08-23 | 2017-02-28 | Epc (Beijing) Natural Products Co., Ltd. | Rebaudioside A and stevioside compositions |
| US9752174B2 (en) | 2013-05-28 | 2017-09-05 | Purecircle Sdn Bhd | High-purity steviol glycosides |
| US9771434B2 (en) | 2011-06-23 | 2017-09-26 | Purecircle Sdn Bhd | Products from stevia rebaudiana |
| US9795156B2 (en) | 2011-03-17 | 2017-10-24 | E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd | Rebaudioside B and derivatives |
| US9877501B2 (en) | 2011-06-03 | 2018-01-30 | Purecircle Sdn Bhd | Stevia composition |
| US9894922B2 (en) | 2011-05-18 | 2018-02-20 | Purecircle Sdn Bhd | Glucosyl rebaudioside C |
| US10004245B2 (en) | 2009-11-12 | 2018-06-26 | Purecircle Sdn Bhd | Granulation of a stevia sweetener |
| US10021899B2 (en) | 2011-05-31 | 2018-07-17 | Purecircle Sdn Bhd | Stevia composition |
| US10264811B2 (en) | 2014-05-19 | 2019-04-23 | Epc Natural Products Co., Ltd. | Stevia sweetener with improved solubility |
| US10357052B2 (en) | 2014-06-16 | 2019-07-23 | Sweet Green Fields USA LLC | Rebaudioside A and stevioside with improved solubilities |
| US10362797B2 (en) | 2011-02-10 | 2019-07-30 | Purecircle Sdn Bhd | Stevia composition |
| US10480019B2 (en) | 2011-08-10 | 2019-11-19 | Purecircle Sdn Bhd | Process for producing high-purity rubusoside |
| US10485257B2 (en) | 2012-05-22 | 2019-11-26 | Purecircle Sdn Bhd | Method of making steviol glycosides |
| US10485256B2 (en) | 2014-06-20 | 2019-11-26 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility with a cyclodextrin |
| US10602762B2 (en) | 2011-02-17 | 2020-03-31 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US10780170B2 (en) | 2013-06-07 | 2020-09-22 | Purecircle Sdn Bhd | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US10952458B2 (en) | 2013-06-07 | 2021-03-23 | Purecircle Usa Inc | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US11202461B2 (en) | 2014-09-02 | 2021-12-21 | Purecircle Sdn Bhd | Stevia extracts |
| US11464246B2 (en) | 2011-09-07 | 2022-10-11 | Purecircle Sdn Bhd | Highly soluble Stevia sweetener |
| US11647771B2 (en) | 2015-10-26 | 2023-05-16 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11653686B2 (en) | 2015-12-15 | 2023-05-23 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11678685B2 (en) | 2011-02-17 | 2023-06-20 | Purecircle Sdn Bhd | Glucosyl stevia composition |
| US11690391B2 (en) | 2011-02-17 | 2023-07-04 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US11871771B2 (en) | 2011-02-17 | 2024-01-16 | Purecircle Sdn Bhd | Glucosyl Stevia composition |
| US12016355B2 (en) | 2011-02-10 | 2024-06-25 | Purecircle Sdn Bhd | Stevia composition |
| US12441753B2 (en) | 2011-12-19 | 2025-10-14 | Purecircle Sdn. Bhd. | Methods for purifying steviol glycosides and uses of the same |
| US12479877B2 (en) | 2010-03-12 | 2025-11-25 | The Coca-Cola Company | Methods for purifying steviol glycosides and uses of the same |
| US12514274B2 (en) | 2009-11-12 | 2026-01-06 | Purecircle Sdn. Bhd. | Granulation of a stevia sweetener |
-
1978
- 1978-12-29 JP JP16306778A patent/JPS5592400A/ja active Pending
Cited By (86)
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|---|---|---|---|---|
| US8790730B2 (en) | 2005-10-11 | 2014-07-29 | Purecircle Usa | Process for manufacturing a sweetener and use thereof |
| US10531683B2 (en) | 2005-10-11 | 2020-01-14 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8334006B2 (en) | 2005-10-11 | 2012-12-18 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8337927B2 (en) | 2005-10-11 | 2012-12-25 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US9101160B2 (en) | 2005-11-23 | 2015-08-11 | The Coca-Cola Company | Condiments with high-potency sweetener |
| US8017168B2 (en) | 2006-11-02 | 2011-09-13 | The Coca-Cola Company | High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith |
| US8937168B2 (en) | 2007-01-22 | 2015-01-20 | Cargill, Incorporated | Method of producing purified rebaudioside A compositions using solvent/antisolvent crystallization |
| US9131718B2 (en) | 2009-06-16 | 2015-09-15 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US9635878B2 (en) | 2009-06-16 | 2017-05-02 | Epc (Beijing) Natural Products Co., Ltd. | Process for rebaudioside D |
| US8414950B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie table top tablet containing the same |
| US8574656B2 (en) | 2009-10-15 | 2013-11-05 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie fruit juice containing the same |
| US8420147B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie cake containing the same |
| US8420146B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie bread containing the same |
| US8507022B2 (en) | 2009-10-15 | 2013-08-13 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same |
| US8512790B2 (en) | 2009-10-15 | 2013-08-20 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie chocolate containing the same |
| US8568818B2 (en) | 2009-10-15 | 2013-10-29 | Pure Circle Sdn Bhd | High-purity Rebaudioside D and low-calorie carbonated drink containing the same |
| US8414948B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie ice cream containing the same |
| EP2708548A2 (en) | 2009-10-15 | 2014-03-19 | Purecircle SDN BHD | High-Purity Rebaudioside D and Applications |
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| US12479877B2 (en) | 2010-03-12 | 2025-11-25 | The Coca-Cola Company | Methods for purifying steviol glycosides and uses of the same |
| US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
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| US11155570B2 (en) | 2010-03-12 | 2021-10-26 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US10285425B2 (en) | 2010-08-23 | 2019-05-14 | Epc Natural Products Co. Ltd | Rebaudioside A and stevioside compositions |
| US9578895B2 (en) | 2010-08-23 | 2017-02-28 | Epc (Beijing) Natural Products Co., Ltd. | Rebaudioside A and stevioside compositions |
| US11202462B2 (en) | 2010-08-23 | 2021-12-21 | Sweet Green Fields International Co., Limited | Rebaudioside A and stevioside compositions |
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| US10485256B2 (en) | 2014-06-20 | 2019-11-26 | Sweet Green Fields International Co., Limited | Stevia sweetener with improved solubility with a cyclodextrin |
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| US11647771B2 (en) | 2015-10-26 | 2023-05-16 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11653686B2 (en) | 2015-12-15 | 2023-05-23 | Purecircle Usa Inc. | Steviol glycoside compositions |
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