JPS5770879A - Preparation of mercaptothiazoline compound - Google Patents

Preparation of mercaptothiazoline compound

Info

Publication number
JPS5770879A
JPS5770879A JP14628280A JP14628280A JPS5770879A JP S5770879 A JPS5770879 A JP S5770879A JP 14628280 A JP14628280 A JP 14628280A JP 14628280 A JP14628280 A JP 14628280A JP S5770879 A JPS5770879 A JP S5770879A
Authority
JP
Japan
Prior art keywords
carbon disulfide
alkaline hydroxide
aminoalkyl sulfuric
ester
sulfuric ester
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP14628280A
Other languages
Japanese (ja)
Other versions
JPS639509B2 (en
Inventor
Kozo Iwasaki
Eiichi Noda
Yoshiaki Noguchi
Isamu Yamamoto
Hiromi Inagaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Priority to JP14628280A priority Critical patent/JPS5770879A/en
Publication of JPS5770879A publication Critical patent/JPS5770879A/en
Publication of JPS639509B2 publication Critical patent/JPS639509B2/ja
Granted legal-status Critical Current

Links

Landscapes

  • Thiazole And Isothizaole Compounds (AREA)

Abstract

PURPOSE: To obtain the titled substance in high yield without side reactions, by reacting an aminoalkyl sulfuric easter with carbon disulfide in the presence of an alkaline hydroxide at a ratio of the alkaline hydroxide and carbon disulfide to the ester in a given range.
CONSTITUTION: An aminoalkyl sulfuric ester is reacted with carbon disulfide in the presence of an alkaline hydroxide. In the process, the carbon disulfide and alkaline hydroxide are used in an amount in the range of equimolar to 2mol% excess based on the aminoalkyl sulfuric ester, and the reaction is carried out in an aqueous solvent at 45W70°C to give the aimed compound in high yield. 2-Aminoethyl sulfate, 2-amino-1-propyl sulfate, etc. may be cited as the aminoalkyl sulfuric ester.
COPYRIGHT: (C)1982,JPO&Japio
JP14628280A 1980-10-21 1980-10-21 Preparation of mercaptothiazoline compound Granted JPS5770879A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14628280A JPS5770879A (en) 1980-10-21 1980-10-21 Preparation of mercaptothiazoline compound

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14628280A JPS5770879A (en) 1980-10-21 1980-10-21 Preparation of mercaptothiazoline compound

Publications (2)

Publication Number Publication Date
JPS5770879A true JPS5770879A (en) 1982-05-01
JPS639509B2 JPS639509B2 (en) 1988-02-29

Family

ID=15404184

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14628280A Granted JPS5770879A (en) 1980-10-21 1980-10-21 Preparation of mercaptothiazoline compound

Country Status (1)

Country Link
JP (1) JPS5770879A (en)

Also Published As

Publication number Publication date
JPS639509B2 (en) 1988-02-29

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