JPS5825101B2 - フエノ−ル − ホルムアルデヒドジユシハツポウタイ オヨビ ソノセイゾウホウホウ - Google Patents
フエノ−ル − ホルムアルデヒドジユシハツポウタイ オヨビ ソノセイゾウホウホウInfo
- Publication number
- JPS5825101B2 JPS5825101B2 JP754242A JP424275A JPS5825101B2 JP S5825101 B2 JPS5825101 B2 JP S5825101B2 JP 754242 A JP754242 A JP 754242A JP 424275 A JP424275 A JP 424275A JP S5825101 B2 JPS5825101 B2 JP S5825101B2
- Authority
- JP
- Japan
- Prior art keywords
- resin
- resol
- catalyst
- phenol
- viscosity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920001568 phenolic resin Polymers 0.000 title claims description 13
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 title description 2
- 229920003987 resole Polymers 0.000 claims description 20
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 18
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 239000005011 phenolic resin Substances 0.000 claims description 9
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 230000000694 effects Effects 0.000 claims description 6
- 239000003377 acid catalyst Substances 0.000 claims description 5
- 229920005989 resin Polymers 0.000 description 25
- 239000011347 resin Substances 0.000 description 25
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 21
- 238000000034 method Methods 0.000 description 20
- 239000003054 catalyst Substances 0.000 description 17
- 239000006260 foam Substances 0.000 description 17
- 239000000203 mixture Substances 0.000 description 13
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 8
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000004094 surface-active agent Substances 0.000 description 6
- 239000002585 base Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 230000008961 swelling Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000001879 gelation Methods 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 239000012632 extractable Substances 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 238000006386 neutralization reaction Methods 0.000 description 3
- 229920001296 polysiloxane Polymers 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- -1 sulfuric acid ester Chemical class 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- 239000004809 Teflon Substances 0.000 description 2
- 229920006362 Teflon® Polymers 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000008389 polyethoxylated castor oil Substances 0.000 description 2
- WZFUQSJFWNHZHM-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)CC(=O)N1CC2=C(CC1)NN=N2 WZFUQSJFWNHZHM-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 208000037656 Respiratory Sounds Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000012432 intermediate storage Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000009972 noncorrosive effect Effects 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 239000002952 polymeric resin Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
- C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
- C08J2361/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
- C08J2361/08—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols with monohydric phenols
- C08J2361/10—Phenol-formaldehyde condensates
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7346997A FR2256193B1 (fr) | 1973-12-28 | 1973-12-28 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5098560A JPS5098560A (fr) | 1975-08-05 |
| JPS5825101B2 true JPS5825101B2 (ja) | 1983-05-25 |
Family
ID=9129953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP754242A Expired JPS5825101B2 (ja) | 1973-12-28 | 1974-12-28 | フエノ−ル − ホルムアルデヒドジユシハツポウタイ オヨビ ソノセイゾウホウホウ |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS5825101B2 (fr) |
| BE (1) | BE824524A (fr) |
| BR (1) | BR7410805D0 (fr) |
| CA (1) | CA1051149A (fr) |
| DE (1) | DE2461661C2 (fr) |
| DK (1) | DK673474A (fr) |
| ES (1) | ES433403A1 (fr) |
| FI (1) | FI61198C (fr) |
| FR (1) | FR2256193B1 (fr) |
| GB (1) | GB1491730A (fr) |
| IT (1) | IT1026201B (fr) |
| NL (1) | NL7416898A (fr) |
| NO (1) | NO141900C (fr) |
| SE (1) | SE415188B (fr) |
| ZA (1) | ZA748258B (fr) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4202945A (en) * | 1979-04-03 | 1980-05-13 | Leinhardt Franklyn J | Phenolic foam materials and method of making same |
| DE3037683A1 (de) * | 1980-10-04 | 1982-05-19 | Basf Ag, 6700 Ludwigshafen | Elastische duroplast-schaumstoffe |
| CN111103420B (zh) * | 2019-11-20 | 2022-05-10 | 华东理工大学 | 一种原料不确定下的酚醛树脂产品质量预测方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1236183B (de) * | 1964-12-17 | 1967-03-09 | Dynamit Nobel Ag | Verfahren zur Herstellung von Phenolharzschaumstoffen |
| JPS5941441B2 (ja) * | 1977-11-14 | 1984-10-06 | 杏林製薬株式会社 | ハイドロキシエチルデンプンの製造方法 |
| JPS642045A (en) | 1987-06-25 | 1989-01-06 | Konica Corp | Silver halide color photographic sensitive material containing novel cyan coupler |
-
1973
- 1973-12-28 FR FR7346997A patent/FR2256193B1/fr not_active Expired
-
1974
- 1974-12-20 DK DK673474A patent/DK673474A/da not_active Application Discontinuation
- 1974-12-20 SE SE7416153A patent/SE415188B/xx unknown
- 1974-12-26 BR BR10805/74A patent/BR7410805D0/pt unknown
- 1974-12-27 DE DE2461661A patent/DE2461661C2/de not_active Expired
- 1974-12-27 FI FI3753/74A patent/FI61198C/fi active
- 1974-12-27 ES ES433403A patent/ES433403A1/es not_active Expired
- 1974-12-27 GB GB55969/74A patent/GB1491730A/en not_active Expired
- 1974-12-27 NL NL7416898A patent/NL7416898A/xx not_active Application Discontinuation
- 1974-12-27 NO NO744681A patent/NO141900C/no unknown
- 1974-12-28 JP JP754242A patent/JPS5825101B2/ja not_active Expired
- 1974-12-30 ZA ZA00748258A patent/ZA748258B/xx unknown
- 1974-12-30 IT IT54817/74A patent/IT1026201B/it active
- 1974-12-30 CA CA217,137A patent/CA1051149A/fr not_active Expired
-
1975
- 1975-01-20 BE BE2054094A patent/BE824524A/fr not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DK673474A (fr) | 1975-09-08 |
| ES433403A1 (es) | 1976-11-16 |
| CA1051149A (fr) | 1979-03-20 |
| NO141900C (no) | 1980-05-28 |
| NL7416898A (nl) | 1975-07-01 |
| AU7704874A (en) | 1976-07-01 |
| FI375374A7 (fr) | 1975-06-29 |
| JPS5098560A (fr) | 1975-08-05 |
| BE824524A (fr) | 1975-05-15 |
| FI61198C (fi) | 1982-06-10 |
| FR2256193A1 (fr) | 1975-07-25 |
| BR7410805D0 (pt) | 1975-09-02 |
| ZA748258B (en) | 1976-02-25 |
| SE7416153L (fr) | 1975-06-30 |
| FR2256193B1 (fr) | 1978-11-10 |
| DE2461661C2 (de) | 1985-01-31 |
| FI61198B (fi) | 1982-02-26 |
| GB1491730A (en) | 1977-11-16 |
| NO141900B (no) | 1980-02-18 |
| SE415188B (sv) | 1980-09-15 |
| DE2461661A1 (de) | 1975-07-10 |
| IT1026201B (it) | 1978-09-20 |
| NO744681L (fr) | 1975-07-28 |
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