CA1051149A - Mousses formo-phenoliques et leur methode de preparation - Google Patents

Mousses formo-phenoliques et leur methode de preparation

Info

Publication number: CA1051149A
Authority: CA; Canada
Prior art keywords: process according; acid; temperature; resol; catalyst
Prior art date: 1973-12-28
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

CA217,137A

Other languages

English (en)

Other versions

CA217137S (en

Inventor

Paul Mottez

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Orkem SA

Original Assignee

Chimique des Charbonnages SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-12-28

Filing date

1974-12-30

Publication date

1979-03-20

1974-12-30 Application filed by Chimique des Charbonnages SA filed Critical Chimique des Charbonnages SA

1979-03-20 Application granted granted Critical

1979-03-20 Publication of CA1051149A publication Critical patent/CA1051149A/fr

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title claims abstract description 21
239000006260 foam Substances 0.000 title description 13
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 24
239000002253 acid Substances 0.000 claims abstract description 18
239000003054 catalyst Substances 0.000 claims abstract description 17
239000000203 mixture Substances 0.000 claims abstract description 16
229920003987 resole Polymers 0.000 claims abstract description 16
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 12
239000004604 Blowing Agent Substances 0.000 claims abstract description 11
239000003513 alkali Substances 0.000 claims abstract description 10
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims abstract description 9
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 8
238000004519 manufacturing process Methods 0.000 claims abstract description 8
ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims abstract description 7
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims abstract description 6
229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 6
230000000694 effects Effects 0.000 claims abstract description 6
KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 5
239000003377 acid catalyst Substances 0.000 claims abstract description 4
230000003472 neutralizing effect Effects 0.000 claims abstract description 3
235000006408 oxalic acid Nutrition 0.000 claims abstract description 3
229910021653 sulphate ion Inorganic materials 0.000 claims abstract description 3
229920005989 resin Polymers 0.000 claims description 21
239000011347 resin Substances 0.000 claims description 21
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 18
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical group CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 17
238000009835 boiling Methods 0.000 claims description 6
239000004094 surface-active agent Substances 0.000 claims description 6
238000002156 mixing Methods 0.000 claims description 5
238000005342 ion exchange Methods 0.000 claims description 2
239000004014 plasticizer Substances 0.000 claims description 2
150000001875 compounds Chemical class 0.000 claims 1
239000000047 product Substances 0.000 description 13
229920001568 phenolic resin Polymers 0.000 description 8
229960004279 formaldehyde Drugs 0.000 description 6
235000019256 formaldehyde Nutrition 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 4
SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
150000002500 ions Chemical class 0.000 description 3
239000001117 sulphuric acid Substances 0.000 description 3
235000011149 sulphuric acid Nutrition 0.000 description 3
239000004215 Carbon black (E152) Substances 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
238000007664 blowing Methods 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002430 hydrocarbons Chemical class 0.000 description 2
229920001296 polysiloxane Polymers 0.000 description 2
239000012429 reaction media Substances 0.000 description 2
101100328884 Caenorhabditis elegans sqt-3 gene Proteins 0.000 description 1
229910000831 Steel Inorganic materials 0.000 description 1
239000004809 Teflon Substances 0.000 description 1
229920006362 Teflon® Polymers 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
239000004359 castor oil Substances 0.000 description 1
229960001777 castor oil Drugs 0.000 description 1
235000019438 castor oil Nutrition 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
239000007859 condensation product Substances 0.000 description 1
230000002844 continuous effect Effects 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000005336 cracking Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
238000012432 intermediate storage Methods 0.000 description 1
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
229910052753 mercury Inorganic materials 0.000 description 1
238000000465 moulding Methods 0.000 description 1
RCHKEJKUUXXBSM-UHFFFAOYSA-N n-benzyl-2-(3-formylindol-1-yl)acetamide Chemical compound C12=CC=CC=C2C(C=O)=CN1CC(=O)NCC1=CC=CC=C1 RCHKEJKUUXXBSM-UHFFFAOYSA-N 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
230000009972 noncorrosive effect Effects 0.000 description 1
239000008389 polyethoxylated castor oil Substances 0.000 description 1
235000013824 polyphenols Nutrition 0.000 description 1
238000003825 pressing Methods 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
239000007858 starting material Substances 0.000 description 1
239000010959 steel Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
239000010409 thin film Substances 0.000 description 1
239000003039 volatile agent Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
- C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
- C08J2361/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
- C08J2361/08—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols with monohydric phenols
- C08J2361/10—Phenol-formaldehyde condensates

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Phenolic Resins Or Amino Resins (AREA)

CA217,137A 1973-12-28 1974-12-30 Mousses formo-phenoliques et leur methode de preparation Expired CA1051149A (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR7346997A FR2256193B1 (fr)	1973-12-28	1973-12-28

Publications (1)

Publication Number	Publication Date
CA1051149A true CA1051149A (fr)	1979-03-20

Family

ID=9129953

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA217,137A Expired CA1051149A (fr)	1973-12-28	1974-12-30	Mousses formo-phenoliques et leur methode de preparation

Country Status (15)

Country	Link
JP (1)	JPS5825101B2 (fr)
BE (1)	BE824524A (fr)
BR (1)	BR7410805D0 (fr)
CA (1)	CA1051149A (fr)
DE (1)	DE2461661C2 (fr)
DK (1)	DK673474A (fr)
ES (1)	ES433403A1 (fr)
FI (1)	FI61198C (fr)
FR (1)	FR2256193B1 (fr)
GB (1)	GB1491730A (fr)
IT (1)	IT1026201B (fr)
NL (1)	NL7416898A (fr)
NO (1)	NO141900C (fr)
SE (1)	SE415188B (fr)
ZA (1)	ZA748258B (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4202945A (en) *	1979-04-03	1980-05-13	Leinhardt Franklyn J	Phenolic foam materials and method of making same
DE3037683A1 (de) *	1980-10-04	1982-05-19	Basf Ag, 6700 Ludwigshafen	Elastische duroplast-schaumstoffe
CN111103420B (zh) *	2019-11-20	2022-05-10	华东理工大学	一种原料不确定下的酚醛树脂产品质量预测方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1236183B (de) *	1964-12-17	1967-03-09	Dynamit Nobel Ag	Verfahren zur Herstellung von Phenolharzschaumstoffen
JPS5941441B2 (ja) *	1977-11-14	1984-10-06	杏林製薬株式会社	ハイドロキシエチルデンプンの製造方法
JPS642045A (en)	1987-06-25	1989-01-06	Konica Corp	Silver halide color photographic sensitive material containing novel cyan coupler

1973
- 1973-12-28 FR FR7346997A patent/FR2256193B1/fr not_active Expired
1974
- 1974-12-20 SE SE7416153A patent/SE415188B/xx unknown
- 1974-12-20 DK DK673474A patent/DK673474A/da not_active Application Discontinuation
- 1974-12-26 BR BR10805/74A patent/BR7410805D0/pt unknown
- 1974-12-27 GB GB55969/74A patent/GB1491730A/en not_active Expired
- 1974-12-27 FI FI3753/74A patent/FI61198C/fi active
- 1974-12-27 DE DE2461661A patent/DE2461661C2/de not_active Expired
- 1974-12-27 NL NL7416898A patent/NL7416898A/xx not_active Application Discontinuation
- 1974-12-27 NO NO744681A patent/NO141900C/no unknown
- 1974-12-27 ES ES433403A patent/ES433403A1/es not_active Expired
- 1974-12-28 JP JP754242A patent/JPS5825101B2/ja not_active Expired
- 1974-12-30 CA CA217,137A patent/CA1051149A/fr not_active Expired
- 1974-12-30 IT IT54817/74A patent/IT1026201B/it active
- 1974-12-30 ZA ZA00748258A patent/ZA748258B/xx unknown
1975
- 1975-01-20 BE BE2054094A patent/BE824524A/fr not_active IP Right Cessation

Also Published As

Publication number	Publication date
NO744681L (fr)	1975-07-28
FR2256193A1 (fr)	1975-07-25
BE824524A (fr)	1975-05-15
SE7416153L (fr)	1975-06-30
BR7410805D0 (pt)	1975-09-02
DE2461661A1 (de)	1975-07-10
DE2461661C2 (de)	1985-01-31
JPS5825101B2 (ja)	1983-05-25
JPS5098560A (fr)	1975-08-05
FR2256193B1 (fr)	1978-11-10
GB1491730A (en)	1977-11-16
FI61198C (fi)	1982-06-10
NO141900C (no)	1980-05-28
ES433403A1 (es)	1976-11-16
SE415188B (sv)	1980-09-15
NL7416898A (nl)	1975-07-01
DK673474A (fr)	1975-09-08
ZA748258B (en)	1976-02-25
IT1026201B (it)	1978-09-20
AU7704874A (en)	1976-07-01
NO141900B (no)	1980-02-18
FI375374A7 (fr)	1975-06-29
FI61198B (fi)	1982-02-26

Publication	Publication Date	Title
US4022755A (en)	1977-05-10	Cyanato-group-containing phenol resin
US2653139A (en)	1953-09-22	In-place expanded cellular resinous bodies and processes for producing them from phenol-aldehyde resins with the aid of a peroxide
US2911380A (en)	1959-11-03	Poly-(aromatic ether) compositions and method of making same
US4423163A (en)	1983-12-27	Method of producing phenolic foam using pressure and foam produced by the method
JPS5829814B2 (ja)	1983-06-24	アルキロ−ル基を含有するフエノ−ル系重合体とフエノ−ル類とから成る組成物及びその製造方法
US4720510A (en)	1988-01-19	Process for producing phenolic foams
JPS61246237A (ja)	1986-11-01	フェノ−ル樹脂複合発泡体の製造方法
US2865869A (en)	1958-12-23	Composition comprising an alkyd resin, organic polyisocyanate and a tertiary alcohol-concentrated acid foaming agent and method of preparing cellular resin therefrom
CA1051149A (fr)	1979-03-20	Mousses formo-phenoliques et leur methode de preparation
CN104387541B (zh)	2016-10-05	一种增韧改性酚醛泡沫及其制备方法
US4309527A (en)	1982-01-05	Fire retardant polymer resin
US3429851A (en)	1969-02-25	Silicate resins
US4275170A (en)	1981-06-23	Method of making a fire retardant polymer resin
US4105623A (en)	1978-08-08	Method of making molding compounds and materials made thereby
US4075139A (en)	1978-02-21	Process of making a cured resole foam and product produced therefrom
CN106832248A (zh)	2017-06-13	快速脱模硬泡聚醚多元醇的制备方法
US4471089A (en)	1984-09-11	Fire retardant polymer resin
US4883824A (en)	1989-11-28	Modified phenolic foam catalysts and method
JPH047381B2 (fr)	1992-02-10
US1020593A (en)	1912-03-19	Phenolic condensation product and method of preparing same.
US4945077A (en)	1990-07-31	Modified phenolic foam catalysts and method
CN114736420B (zh)	2022-09-02	一种改性酚醛树脂泡沫及其制备方法
FI101392B (fi)	1998-06-15	Lämmöneristelevyksi työstettävä vaahtoutuva fenoli-formaldehydihartsin ja polystyreenin seos sekä lämmöneristyslevy
SU883103A1 (ru)	1981-11-23	Способ получени мочевино-формальдегидного пенопласта
SU1219604A1 (ru)	1986-03-23	Композици дл пенопласта