JPS5921528A - 二硫化鉄の製造方法 - Google Patents

二硫化鉄の製造方法

Info

Publication number: JPS5921528A
Authority: JP; Japan
Prior art keywords: disulfide; crystals; ferrous; alkali; aqueous soln
Prior art date: 1982-07-27
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP57131660A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0216249B2 (2

Inventor

Noriyuki Mikasa

三笠　宣幸

Akira Umehara

梅原　晟

Goro Kawakami

河上　悟朗

Tamito Mukoda

民人向田

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Sankyo Kasei Co Ltd

Original Assignee

Sankyo Kasei Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-07-27

Filing date

1982-07-27

Publication date

1984-02-03

1982-07-27 Application filed by Sankyo Kasei Co Ltd filed Critical Sankyo Kasei Co Ltd

1982-07-27 Priority to JP57131660A priority Critical patent/JPS5921528A/ja

1984-02-03 Publication of JPS5921528A publication Critical patent/JPS5921528A/ja

1990-04-16 Publication of JPH0216249B2 publication Critical patent/JPH0216249B2/ja

Status Granted legal-status Critical Current

Links

238000004519 manufacturing process Methods 0.000 title claims abstract description 8
NFMAZVUSKIJEIH-UHFFFAOYSA-N bis(sulfanylidene)iron Chemical compound S=[Fe]=S NFMAZVUSKIJEIH-UHFFFAOYSA-N 0.000 title abstract description 5
229910000339 iron disulfide Inorganic materials 0.000 title abstract description 5
BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 claims abstract description 10
238000006243 chemical reaction Methods 0.000 claims abstract description 9
BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 9
239000000203 mixture Substances 0.000 claims abstract description 6
239000003513 alkali Substances 0.000 claims abstract description 5
238000010438 heat treatment Methods 0.000 claims abstract description 5
239000011149 active material Substances 0.000 claims abstract description 4
238000002156 mixing Methods 0.000 claims abstract description 3
-1 ammonium disulfide Chemical compound 0.000 claims abstract 2
239000007864 aqueous solution Substances 0.000 claims description 11
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 14
239000013078 crystal Substances 0.000 abstract description 13
230000000694 effects Effects 0.000 abstract description 5
239000002904 solvent Substances 0.000 abstract description 5
CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract description 4
235000003891 ferrous sulphate Nutrition 0.000 abstract description 3
239000011790 ferrous sulphate Substances 0.000 abstract description 3
229910000359 iron(II) sulfate Inorganic materials 0.000 abstract description 3
229910002651 NO3 Inorganic materials 0.000 abstract description 2
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract description 2
239000008367 deionised water Substances 0.000 abstract description 2
229910021641 deionized water Inorganic materials 0.000 abstract description 2
LTJSXGVQCAVSJW-UHFFFAOYSA-N [K+].[K+].[S-][S-] Chemical compound [K+].[K+].[S-][S-] LTJSXGVQCAVSJW-UHFFFAOYSA-N 0.000 abstract 1
229960002089 ferrous chloride Drugs 0.000 abstract 1
238000001914 filtration Methods 0.000 abstract 1
NMCUIPGRVMDVDB-UHFFFAOYSA-L iron dichloride Chemical compound Cl[Fe]Cl NMCUIPGRVMDVDB-UHFFFAOYSA-L 0.000 abstract 1
150000001455 metallic ions Chemical class 0.000 abstract 1
239000002245 particle Substances 0.000 abstract 1
SRRKNRDXURUMPP-UHFFFAOYSA-N sodium disulfide Chemical compound [Na+].[Na+].[S-][S-] SRRKNRDXURUMPP-UHFFFAOYSA-N 0.000 abstract 1
238000000034 method Methods 0.000 description 12
MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 5
229910052979 sodium sulfide Inorganic materials 0.000 description 5
GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 5
239000000047 product Substances 0.000 description 4
NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 4
238000005987 sulfurization reaction Methods 0.000 description 4
238000001816 cooling Methods 0.000 description 3
229910052683 pyrite Inorganic materials 0.000 description 3
239000011028 pyrite Substances 0.000 description 3
239000000243 solution Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
229910052717 sulfur Inorganic materials 0.000 description 3
238000005406 washing Methods 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
238000002441 X-ray diffraction Methods 0.000 description 2
239000003125 aqueous solvent Substances 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
238000001035 drying Methods 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
239000007788 liquid Substances 0.000 description 2
NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
230000002269 spontaneous effect Effects 0.000 description 2
239000011593 sulfur Substances 0.000 description 2
238000001308 synthesis method Methods 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
244000061456 Solanum tuberosum Species 0.000 description 1
235000002595 Solanum tuberosum Nutrition 0.000 description 1
240000006394 Sorghum bicolor Species 0.000 description 1
235000011684 Sorghum saccharatum Nutrition 0.000 description 1
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
235000009430 Thespesia populnea Nutrition 0.000 description 1
241000209140 Triticum Species 0.000 description 1
235000021307 Triticum Nutrition 0.000 description 1
230000004913 activation Effects 0.000 description 1
230000002411 adverse Effects 0.000 description 1
239000006183 anode active material Substances 0.000 description 1
KPMQAAGZEHZCQN-UHFFFAOYSA-N azete-2-carbonitrile Chemical compound N#CC1=NC=C1 KPMQAAGZEHZCQN-UHFFFAOYSA-N 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
230000008859 change Effects 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
238000007872 degassing Methods 0.000 description 1
238000010586 diagram Methods 0.000 description 1
239000003792 electrolyte Substances 0.000 description 1
230000007717 exclusion Effects 0.000 description 1
210000000744 eyelid Anatomy 0.000 description 1
230000005484 gravity Effects 0.000 description 1
238000011005 laboratory method Methods 0.000 description 1
229910052960 marcasite Inorganic materials 0.000 description 1
239000000463 material Substances 0.000 description 1
229930014626 natural product Natural products 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
229910052573 porcelain Inorganic materials 0.000 description 1
235000012015 potatoes Nutrition 0.000 description 1
230000008569 process Effects 0.000 description 1
239000002994 raw material Substances 0.000 description 1
230000009257 reactivity Effects 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000002002 slurry Substances 0.000 description 1
239000011734 sodium Substances 0.000 description 1
238000004611 spectroscopical analysis Methods 0.000 description 1
238000006467 substitution reaction Methods 0.000 description 1

Classifications

- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries

Landscapes

Battery Electrode And Active Subsutance (AREA)
Inorganic Compounds Of Heavy Metals (AREA)

JP57131660A 1982-07-27 1982-07-27 二硫化鉄の製造方法 Granted JPS5921528A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP57131660A JPS5921528A (ja)	1982-07-27	1982-07-27	二硫化鉄の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP57131660A JPS5921528A (ja)	1982-07-27	1982-07-27	二硫化鉄の製造方法

Publications (2)

Publication Number	Publication Date
JPS5921528A true JPS5921528A (ja)	1984-02-03
JPH0216249B2 JPH0216249B2 (2)	1990-04-16

Family

ID=15063243

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP57131660A Granted JPS5921528A (ja)	1982-07-27	1982-07-27	二硫化鉄の製造方法

Country Status (1)

Country	Link
JP (1)	JPS5921528A (2)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH0768219B2 (ja) *	1985-12-09	1995-07-26	キノインギオギスゼルエスベギエスゼチテルメケクギヤラア−ル．テイ−．	キノリンカルボン酸の製造法
CN1089278C (zh) *	1995-05-25	2002-08-21	旭化成株式会社	硫化铁及其制造方法
CN101311122B (zh)	2007-05-25	2010-09-22	北京有色金属研究总院	一种FeS的制备方法
CN114477305A (zh) *	2021-12-27	2022-05-13	上海交通大学	一种镁锂双离子电池二硫化亚铁正极材料制备方法及应用

1982
- 1982-07-27 JP JP57131660A patent/JPS5921528A/ja active Granted

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH0768219B2 (ja) *	1985-12-09	1995-07-26	キノインギオギスゼルエスベギエスゼチテルメケクギヤラア−ル．テイ−．	キノリンカルボン酸の製造法
CN1089278C (zh) *	1995-05-25	2002-08-21	旭化成株式会社	硫化铁及其制造方法
CN101311122B (zh)	2007-05-25	2010-09-22	北京有色金属研究总院	一种FeS的制备方法
CN114477305A (zh) *	2021-12-27	2022-05-13	上海交通大学	一种镁锂双离子电池二硫化亚铁正极材料制备方法及应用

Also Published As

Publication number	Publication date
JPH0216249B2 (2)	1990-04-16

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Packer et al.	1921	CLIV.—Cupritartrates

JPS5921528A - 二硫化鉄の製造方法 - Google Patents

Info

Links

Classifications

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (2)

Family

ID=15063243

Family Applications (1)

Country Status (1)

Cited By (4)

Cited By (4)

Also Published As

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