JPS60246338A - アルキリデンビス（ジブロモフエノ−ル）の製造方法 - Google Patents

アルキリデンビス（ジブロモフエノ−ル）の製造方法

Info

Publication number: JPS60246338A
Authority: JP; Japan
Prior art keywords: methanol; water; bromine; tetrabromobisphenol; alkylidene
Prior art date: 1984-05-18
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP10036784A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0475221B2 (fr

Inventor

チヤールズ・テイー・バウンズ

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Dow Chemical Co

Original Assignee

Dow Chemical Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-05-18

Filing date

1984-05-18

Publication date

1985-12-06

1984-05-18 Application filed by Dow Chemical Co filed Critical Dow Chemical Co

1984-05-18 Priority to JP10036784A priority Critical patent/JPS60246338A/ja

1985-12-06 Publication of JPS60246338A publication Critical patent/JPS60246338A/ja

1992-11-30 Publication of JPH0475221B2 publication Critical patent/JPH0475221B2/ja

Status Granted legal-status Critical Current

Links

FNAKEOXYWBWIRT-UHFFFAOYSA-N 2,3-dibromophenol Chemical compound OC1=CC=CC(Br)=C1Br FNAKEOXYWBWIRT-UHFFFAOYSA-N 0.000 title claims description 10
238000004519 manufacturing process Methods 0.000 title claims description 10
125000001118 alkylidene group Chemical group 0.000 title claims description 8
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 162
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
238000000034 method Methods 0.000 claims description 26
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 24
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 24
229910052794 bromium Inorganic materials 0.000 claims description 24
-1 alkylidene diphenol Chemical compound 0.000 claims description 6
XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 claims description 3
GZUXJHMPEANEGY-UHFFFAOYSA-N bromomethane Chemical compound BrC GZUXJHMPEANEGY-UHFFFAOYSA-N 0.000 description 39
239000000047 product Substances 0.000 description 31
CMQUQOHNANGDOR-UHFFFAOYSA-N 2,3-dibromo-4-(2,4-dibromo-5-hydroxyphenyl)phenol Chemical compound BrC1=C(Br)C(O)=CC=C1C1=CC(O)=C(Br)C=C1Br CMQUQOHNANGDOR-UHFFFAOYSA-N 0.000 description 26
238000006243 chemical reaction Methods 0.000 description 23
238000002474 experimental method Methods 0.000 description 21
230000000052 comparative effect Effects 0.000 description 19
229940102396 methyl bromide Drugs 0.000 description 19
238000010438 heat treatment Methods 0.000 description 17
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 14
229930185605 Bisphenol Natural products 0.000 description 13
238000010992 reflux Methods 0.000 description 9
CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 8
238000002844 melting Methods 0.000 description 6
230000008018 melting Effects 0.000 description 6
239000002904 solvent Substances 0.000 description 6
VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical class C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 description 5
239000012535 impurity Substances 0.000 description 5
VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 4
238000001816 cooling Methods 0.000 description 4
239000003822 epoxy resin Substances 0.000 description 4
229910000042 hydrogen bromide Inorganic materials 0.000 description 4
229920000647 polyepoxide Polymers 0.000 description 4
238000001556 precipitation Methods 0.000 description 4
238000003756 stirring Methods 0.000 description 4
230000031709 bromination Effects 0.000 description 3
238000005893 bromination reaction Methods 0.000 description 3
239000013078 crystal Substances 0.000 description 3
LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 3
229920003023 plastic Polymers 0.000 description 3
238000007614 solvation Methods 0.000 description 3
241000894007 species Species 0.000 description 3
239000000126 substance Substances 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
241001550224 Apha Species 0.000 description 2
238000001704 evaporation Methods 0.000 description 2
239000007788 liquid Substances 0.000 description 2
238000002156 mixing Methods 0.000 description 2
239000003960 organic solvent Substances 0.000 description 2
239000004033 plastic Substances 0.000 description 2
239000004417 polycarbonate Substances 0.000 description 2
229920000515 polycarbonate Polymers 0.000 description 2
229920001343 polytetrafluoroethylene Polymers 0.000 description 2
239000004810 polytetrafluoroethylene Substances 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
238000005406 washing Methods 0.000 description 2
MQXNNWDXHFBFEB-UHFFFAOYSA-N 2,2-bis(2-hydroxyphenyl)propane Chemical compound C=1C=CC=C(O)C=1C(C)(C)C1=CC=CC=C1O MQXNNWDXHFBFEB-UHFFFAOYSA-N 0.000 description 1
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
241000238557 Decapoda Species 0.000 description 1
YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
CLBRCZAHAHECKY-UHFFFAOYSA-N [Co].[Pt] Chemical compound [Co].[Pt] CLBRCZAHAHECKY-UHFFFAOYSA-N 0.000 description 1
238000013019 agitation Methods 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical group C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
235000011089 carbon dioxide Nutrition 0.000 description 1
239000007810 chemical reaction solvent Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
XENVCRGQTABGKY-ZHACJKMWSA-N chlorohydrin Chemical compound CC#CC#CC#CC#C\C=C\C(Cl)CO XENVCRGQTABGKY-ZHACJKMWSA-N 0.000 description 1
238000002485 combustion reaction Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
230000037213 diet Effects 0.000 description 1
235000005911 diet Nutrition 0.000 description 1
ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
238000003958 fumigation Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000000203 mixture Substances 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000002243 precursor Substances 0.000 description 1
230000002028 premature Effects 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000005070 sampling Methods 0.000 description 1
238000005507 spraying Methods 0.000 description 1
238000013517 stratification Methods 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP10036784A 1984-05-18 1984-05-18 アルキリデンビス（ジブロモフエノ−ル）の製造方法 Granted JPS60246338A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP10036784A JPS60246338A (ja)	1984-05-18	1984-05-18	アルキリデンビス（ジブロモフエノ−ル）の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP10036784A JPS60246338A (ja)	1984-05-18	1984-05-18	アルキリデンビス（ジブロモフエノ−ル）の製造方法

Publications (2)

Publication Number	Publication Date
JPS60246338A true JPS60246338A (ja)	1985-12-06
JPH0475221B2 JPH0475221B2 (fr)	1992-11-30

Family

ID=14272086

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP10036784A Granted JPS60246338A (ja)	1984-05-18	1984-05-18	アルキリデンビス（ジブロモフエノ−ル）の製造方法

Country Status (1)

Country	Link
JP (1)	JPS60246338A (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6263537A (ja) *	1985-09-09	1987-03-20	ザ　ダウ　ケミカル　カンパニ−	臭素化ヒドロキシ芳香族化合物

1984
- 1984-05-18 JP JP10036784A patent/JPS60246338A/ja active Granted

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6263537A (ja) *	1985-09-09	1987-03-20	ザ　ダウ　ケミカル　カンパニ−	臭素化ヒドロキシ芳香族化合物

Also Published As

Publication number	Publication date
JPH0475221B2 (fr)	1992-11-30

Publication	Publication Date	Title
US4451675A (en)	1984-05-29	Preparation of alkylidenebis(dibromophenol)
EP0112615B1 (fr)	1988-11-30	Procédé de préparation de 2,2-bis(4-hydroxyphényl)propane
US2959622A (en)	1960-11-08	Purification of crude jj-p-bis-
US4162270A (en)	1979-07-24	Process for producing 4,4'-dihydroxydiphenylsulfone of high purity
US4546207A (en)	1985-10-08	Process for preparing anhydrous salts of dihydroxyaromatic compounds
US4461915A (en)	1984-07-24	Purification of bisphenol-A
EP0220004B1 (fr)	1990-04-11	Procédé de synthèse de 4,4'-dihydroxydiphénylsulfone
US4408087A (en)	1983-10-04	Purification of bisphenol-A
US4529823A (en)	1985-07-16	Purification of bisphenol-A
US4507509A (en)	1985-03-26	Purification of bisphenol-A
US4588532A (en)	1986-05-13	Preparation of para-acyloxybenzene sulfonates
US3627846A (en)	1971-12-14	Process for obtaining particularly pure 2,2-bis-(phenylol)-propane
US4294993A (en)	1981-10-13	Purification of bisphenol-A
US4192955A (en)	1980-03-11	Process for the recovery of 2,2-bis(4-hydroxyphenyl) propane
JPS5928539B2 (ja)	1984-07-13	ビスフエノ−ルビスクロロ炭酸エステルの製造法
JPS60246338A (ja)	1985-12-06	アルキリデンビス（ジブロモフエノ−ル）の製造方法
US6049014A (en)	2000-04-11	Process for the manufacture of tetrabromobisphenol-A with co-production of n-propyl bromide
US4300000A (en)	1981-11-10	Process for the recovery of 2,2-bis(4-hydroxyphenyl)propane
EP0117459B1 (fr)	1989-09-06	Procédé de préparation de sels anhydres de composés aromatiques dihydroxylés
US5041677A (en)	1991-08-20	Process for synthesizing 4,4'-dihydroxydiphenyl sulfone
DE3417027A1 (de)	1985-11-14	Verfahren zur herstellung von alkylidenbis(dibromphenol)
US6972344B2 (en)	2005-12-06	Method of producing pure 1,1-bis-(4-hydroxyphenyl)-3,3,5-trimethylcyclohexane
JP4836062B2 (ja)	2011-12-14	ビスフェノールジアルキルエーテル類の製造方法
JPS5949217B2 (ja)	1984-12-01	置換ジフェニルエ−テルの製造方法
NL8401687A (nl)	1985-12-16	Werkwijze ter bereiding van alkylideenbis(dibroomfenol).

JPS60246338A - アルキリデンビス（ジブロモフエノ−ル）の製造方法 - Google Patents

Info

Links

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (2)

Family

ID=14272086

Family Applications (1)

Country Status (1)

Cited By (1)

Cited By (1)

Also Published As

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