JPS606664A - １，３−プロパンジイル−（２，２′−ピリジン）の製造法 - Google Patents

１，３−プロパンジイル−（２，２′−ピリジン）の製造法

Info

Publication number: JPS606664A
Authority: JP; Japan
Prior art keywords: pyridine; basic catalyst; propanediyl; picoline; reacting
Prior art date: 1983-06-27
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP11544183A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0458466B2 (de

Inventor

Yoshikazu Murao

村尾　嘉一

Masao Miyake

正男三宅

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Mitsubishi Chemical Corp

Original Assignee

Mitsubishi Chemical Industries Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-06-27

Filing date

1983-06-27

Publication date

1985-01-14

1983-06-27 Application filed by Mitsubishi Chemical Industries Ltd filed Critical Mitsubishi Chemical Industries Ltd

1983-06-27 Priority to JP11544183A priority Critical patent/JPS606664A/ja

1985-01-14 Publication of JPS606664A publication Critical patent/JPS606664A/ja

1992-09-17 Publication of JPH0458466B2 publication Critical patent/JPH0458466B2/ja

Status Granted legal-status Critical Current

Links

JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 title claims abstract description 29
238000004519 manufacturing process Methods 0.000 title claims description 4
239000003054 catalyst Substances 0.000 claims abstract description 30
150000001875 compounds Chemical class 0.000 claims abstract description 14
238000004821 distillation Methods 0.000 claims abstract description 9
238000009835 boiling Methods 0.000 claims abstract description 6
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
229910052698 phosphorus Inorganic materials 0.000 claims 1
239000011574 phosphorus Substances 0.000 claims 1
238000006243 chemical reaction Methods 0.000 abstract description 25
BSKHPKMHTQYZBB-UHFFFAOYSA-N 2-methylpyridine Chemical compound CC1=CC=CC=N1 BSKHPKMHTQYZBB-UHFFFAOYSA-N 0.000 abstract description 14
238000000034 method Methods 0.000 abstract description 11
KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 abstract description 10
239000011541 reaction mixture Substances 0.000 abstract description 8
239000002994 raw material Substances 0.000 abstract description 7
239000006227 byproduct Substances 0.000 abstract description 4
239000002904 solvent Substances 0.000 abstract description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
239000012044 organic layer Substances 0.000 description 8
229910052708 sodium Inorganic materials 0.000 description 8
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
239000011734 sodium Substances 0.000 description 7
239000000203 mixture Substances 0.000 description 6
230000007423 decrease Effects 0.000 description 5
239000010410 layer Substances 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
238000001816 cooling Methods 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
229910052751 metal Inorganic materials 0.000 description 3
239000002184 metal Substances 0.000 description 3
239000000047 product Substances 0.000 description 3
238000007086 side reaction Methods 0.000 description 3
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
229910052783 alkali metal Inorganic materials 0.000 description 2
150000001340 alkali metals Chemical class 0.000 description 2
HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 2
125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 2
KFDVPJUYSDEJTH-UHFFFAOYSA-N 4-ethenylpyridine Chemical compound C=CC1=CC=NC=C1 KFDVPJUYSDEJTH-UHFFFAOYSA-N 0.000 description 1
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
241000755266 Kathetostoma giganteum Species 0.000 description 1
241000283986 Lepus Species 0.000 description 1
BAWFJGJZGIEFAR-NNYOXOHSSA-N NAD zwitterion Chemical compound NC(=O)C1=CC=C[N+]([C@H]2[C@@H]([C@H](O)[C@@H](COP([O-])(=O)OP(O)(=O)OC[C@@H]3[C@H]([C@@H](O)[C@@H](O3)N3C4=NC=NC(N)=C4N=C3)O)O2)O)=C1 BAWFJGJZGIEFAR-NNYOXOHSSA-N 0.000 description 1
KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
229910052802 copper Inorganic materials 0.000 description 1
239000010949 copper Substances 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
229910021645 metal ion Inorganic materials 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000001294 propane Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1

Landscapes

Pyridine Compounds (AREA)

JP11544183A 1983-06-27 1983-06-27 １，３−プロパンジイル−（２，２′−ピリジン）の製造法 Granted JPS606664A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP11544183A JPS606664A (ja)	1983-06-27	1983-06-27	１，３−プロパンジイル−（２，２′−ピリジン）の製造法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP11544183A JPS606664A (ja)	1983-06-27	1983-06-27	１，３−プロパンジイル−（２，２′−ピリジン）の製造法

Publications (2)

Publication Number	Publication Date
JPS606664A true JPS606664A (ja)	1985-01-14
JPH0458466B2 JPH0458466B2 (de)	1992-09-17

Family

ID=14662632

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP11544183A Granted JPS606664A (ja)	1983-06-27	1983-06-27	１，３−プロパンジイル−（２，２′−ピリジン）の製造法

Country Status (1)

Country	Link
JP (1)	JPS606664A (de)

1983
- 1983-06-27 JP JP11544183A patent/JPS606664A/ja active Granted

Also Published As

Publication number	Publication date
JPH0458466B2 (de)	1992-09-17

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