JPS61127612A - 導電性黒鉛材料の製造方法 - Google Patents

導電性黒鉛材料の製造方法

Info

Publication number: JPS61127612A
Authority: JP; Japan
Prior art keywords: graphite; liquid; powder; graphite powder; thin plate
Prior art date: 1984-11-26
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP59249934A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6313929B2 (fr

Inventor

Masakazu Adachi

足立　正和

Rokuro Fujii

藤井　禄郎

Shoji Hori

昭二堀

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

National Institute of Advanced Industrial Science and Technology AIST

Original Assignee

Agency of Industrial Science and Technology

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-11-26

Filing date

1984-11-26

Publication date

1986-06-14

1984-11-26 Application filed by Agency of Industrial Science and Technology filed Critical Agency of Industrial Science and Technology

1984-11-26 Priority to JP59249934A priority Critical patent/JPS61127612A/ja

1986-06-14 Publication of JPS61127612A publication Critical patent/JPS61127612A/ja

1988-03-28 Publication of JPS6313929B2 publication Critical patent/JPS6313929B2/ja

Status Granted legal-status Critical Current

Links

239000007770 graphite material Substances 0.000 title claims abstract description 5
238000004519 manufacturing process Methods 0.000 title claims description 8
238000000034 method Methods 0.000 title description 11
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 93
229910002804 graphite Inorganic materials 0.000 claims abstract description 50
239000010439 graphite Substances 0.000 claims abstract description 50
239000007788 liquid Substances 0.000 claims abstract description 30
239000000126 substance Substances 0.000 claims abstract description 8
239000000843 powder Substances 0.000 claims description 12
238000010298 pulverizing process Methods 0.000 claims description 6
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 abstract description 10
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract description 9
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract description 6
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 6
229910052760 oxygen Inorganic materials 0.000 abstract description 6
239000001301 oxygen Substances 0.000 abstract description 6
230000001590 oxidative effect Effects 0.000 abstract description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 3
239000011261 inert gas Substances 0.000 abstract description 3
239000000203 mixture Substances 0.000 abstract description 3
238000001816 cooling Methods 0.000 abstract description 2
239000002904 solvent Substances 0.000 abstract description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 22
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 21
229920003023 plastic Polymers 0.000 description 14
239000004033 plastic Substances 0.000 description 14
235000019441 ethanol Nutrition 0.000 description 12
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 9
239000003973 paint Substances 0.000 description 9
239000000463 material Substances 0.000 description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
239000002253 acid Substances 0.000 description 6
150000001875 compounds Chemical class 0.000 description 6
229920006395 saturated elastomer Polymers 0.000 description 6
239000007864 aqueous solution Substances 0.000 description 5
239000011148 porous material Substances 0.000 description 5
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
238000010438 heat treatment Methods 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
238000003917 TEM image Methods 0.000 description 3
229910052799 carbon Inorganic materials 0.000 description 3
239000006185 dispersion Substances 0.000 description 3
238000005516 engineering process Methods 0.000 description 3
239000000945 filler Substances 0.000 description 3
238000011049 filling Methods 0.000 description 3
-1 hegyusen Chemical compound 0.000 description 3
239000004570 mortar (masonry) Substances 0.000 description 3
239000002245 particle Substances 0.000 description 3
238000001179 sorption measurement Methods 0.000 description 3
229910052717 sulfur Chemical group 0.000 description 3
239000011593 sulfur Chemical group 0.000 description 3
239000010409 thin film Substances 0.000 description 3
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
JKTORXLUQLQJCM-UHFFFAOYSA-N 4-phosphonobutylphosphonic acid Chemical compound OP(O)(=O)CCCCP(O)(O)=O JKTORXLUQLQJCM-UHFFFAOYSA-N 0.000 description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
239000000654 additive Substances 0.000 description 2
230000000996 additive effect Effects 0.000 description 2
229910000147 aluminium phosphate Inorganic materials 0.000 description 2
235000015278 beef Nutrition 0.000 description 2
HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
230000005540 biological transmission Effects 0.000 description 2
238000000576 coating method Methods 0.000 description 2
239000013078 crystal Substances 0.000 description 2
238000001035 drying Methods 0.000 description 2
239000003792 electrolyte Substances 0.000 description 2
238000000635 electron micrograph Methods 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
239000010408 film Substances 0.000 description 2
238000007710 freezing Methods 0.000 description 2
230000008014 freezing Effects 0.000 description 2
239000011521 glass Substances 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
ZGEGCLOFRBLKSE-UHFFFAOYSA-N methylene hexane Natural products CCCCCC=C ZGEGCLOFRBLKSE-UHFFFAOYSA-N 0.000 description 2
230000003647 oxidation Effects 0.000 description 2
238000007254 oxidation reaction Methods 0.000 description 2
FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 2
238000011160 research Methods 0.000 description 2
239000011347 resin Substances 0.000 description 2
229920005989 resin Polymers 0.000 description 2
238000004381 surface treatment Methods 0.000 description 2
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
229920002554 vinyl polymer Polymers 0.000 description 2
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000001335 aliphatic alkanes Chemical class 0.000 description 1
150000001336 alkenes Chemical class 0.000 description 1
150000001491 aromatic compounds Chemical class 0.000 description 1
229910021383 artificial graphite Inorganic materials 0.000 description 1
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
239000000920 calcium hydroxide Substances 0.000 description 1
229910001861 calcium hydroxide Inorganic materials 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000004040 coloring Methods 0.000 description 1
239000004020 conductor Substances 0.000 description 1
238000007872 degassing Methods 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
AXZAYXJCENRGIM-UHFFFAOYSA-J dipotassium;tetrabromoplatinum(2-) Chemical compound [K+].[K+].[Br-].[Br-].[Br-].[Br-].[Pt+2] AXZAYXJCENRGIM-UHFFFAOYSA-J 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
239000010931 gold Substances 0.000 description 1
229910052737 gold Inorganic materials 0.000 description 1
238000000227 grinding Methods 0.000 description 1
238000002347 injection Methods 0.000 description 1
239000007924 injection Substances 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
229910001960 metal nitrate Inorganic materials 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
KWKAKUADMBZCLK-UHFFFAOYSA-N methyl heptene Natural products CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 description 1
238000001000 micrograph Methods 0.000 description 1
150000007522 mineralic acids Chemical class 0.000 description 1
238000002156 mixing Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
235000005985 organic acids Nutrition 0.000 description 1
239000005416 organic matter Substances 0.000 description 1
235000006408 oxalic acid Nutrition 0.000 description 1
QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
XNLICIUVMPYHGG-UHFFFAOYSA-N pentan-2-one Chemical compound CCCC(C)=O XNLICIUVMPYHGG-UHFFFAOYSA-N 0.000 description 1
YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical compound CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 1
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
230000000379 polymerizing effect Effects 0.000 description 1
229910001487 potassium perchlorate Inorganic materials 0.000 description 1
238000001878 scanning electron micrograph Methods 0.000 description 1
238000004062 sedimentation Methods 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
239000000243 solution Substances 0.000 description 1
150000003440 styrenes Chemical class 0.000 description 1
125000005504 styryl group Chemical group 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
238000005406 washing Methods 0.000 description 1
230000004580 weight loss Effects 0.000 description 1
239000013585 weight reducing agent Substances 0.000 description 1

Landscapes

Carbon And Carbon Compounds (AREA)

JP59249934A 1984-11-26 1984-11-26 導電性黒鉛材料の製造方法 Granted JPS61127612A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP59249934A JPS61127612A (ja)	1984-11-26	1984-11-26	導電性黒鉛材料の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP59249934A JPS61127612A (ja)	1984-11-26	1984-11-26	導電性黒鉛材料の製造方法

Publications (2)

Publication Number	Publication Date
JPS61127612A true JPS61127612A (ja)	1986-06-14
JPS6313929B2 JPS6313929B2 (fr)	1988-03-28

Family

ID=17200345

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP59249934A Granted JPS61127612A (ja)	1984-11-26	1984-11-26	導電性黒鉛材料の製造方法

Country Status (1)

Country	Link
JP (1)	JPS61127612A (fr)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH02248312A (ja) *	1989-03-20	1990-10-04	Kansai Coke & Chem Co Ltd	キッシュグラファイト精製方法
FR2682370A1 (fr) *	1991-10-15	1993-04-16	Centre Nat Rech Scient	Graphite micronique plat, procede pour sa preparation et ses applications.
WO1998006679A1 (fr) *	1996-08-08	1998-02-19	Hitachi Chemical Company, Ltd.	Particules de graphite et element secondaire au lithium les utilisant en tant que materiau de cathode
US6824924B1 (en)	1998-07-06	2004-11-30	Tdk Corporation	Electrode for nonaqueous electrolyte battery
KR20050064539A (ko) *	2003-12-24	2005-06-29	재단법인 포항산업과학연구원	표면처리 흑연으로부터의 팽창흑연 제조방법
JP2011148701A (ja) *	2011-05-09	2011-08-04	Mitsubishi Gas Chemical Co Inc	炭素からなる骨格を持つ薄膜状粒子の合成方法
CN104310382A (zh) *	2014-09-29	2015-01-28	东华大学	一种石墨烯纳米筛的制备方法
CN114162815A (zh) *	2020-09-10	2022-03-11	中国石油化工股份有限公司	可膨胀石墨材料及其制备方法和应用

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE10322358B4 (de)	2003-05-09	2014-12-31	Behr Thermot-Tronik Gmbh	Thermostatisches Arbeitselement

1984
- 1984-11-26 JP JP59249934A patent/JPS61127612A/ja active Granted

Cited By (23)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH02248312A (ja) *	1989-03-20	1990-10-04	Kansai Coke & Chem Co Ltd	キッシュグラファイト精製方法
FR2682370A1 (fr) *	1991-10-15	1993-04-16	Centre Nat Rech Scient	Graphite micronique plat, procede pour sa preparation et ses applications.
US7288342B2 (en)	1996-08-08	2007-10-30	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7335447B2 (en)	1996-08-08	2008-02-26	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US6447956B2 (en)	1996-08-08	2002-09-10	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
WO1998006679A1 (fr) *	1996-08-08	1998-02-19	Hitachi Chemical Company, Ltd.	Particules de graphite et element secondaire au lithium les utilisant en tant que materiau de cathode
US9508980B2 (en)	1996-08-08	2016-11-29	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative
US6953640B2 (en)	1996-08-08	2005-10-11	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US8580437B2 (en)	1996-08-08	2013-11-12	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US6444365B2 (en)	1996-08-08	2002-09-03	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7378191B2 (en)	1996-08-08	2008-05-27	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7399553B2 (en)	1996-08-08	2008-07-15	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7410727B2 (en)	1996-08-08	2008-08-12	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7700239B2 (en)	1996-08-08	2010-04-20	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US7947395B2 (en)	1996-08-08	2011-05-24	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US8802297B2 (en)	1996-08-08	2014-08-12	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US8129051B2 (en)	1996-08-08	2012-03-06	Hitachi Chemical Company, Ltd.	Graphite particles and lithium secondary battery using the same as negative electrode
US6824924B1 (en)	1998-07-06	2004-11-30	Tdk Corporation	Electrode for nonaqueous electrolyte battery
KR20050064539A (ko) *	2003-12-24	2005-06-29	재단법인 포항산업과학연구원	표면처리 흑연으로부터의 팽창흑연 제조방법
JP2011148701A (ja) *	2011-05-09	2011-08-04	Mitsubishi Gas Chemical Co Inc	炭素からなる骨格を持つ薄膜状粒子の合成方法
CN104310382A (zh) *	2014-09-29	2015-01-28	东华大学	一种石墨烯纳米筛的制备方法
CN114162815A (zh) *	2020-09-10	2022-03-11	中国石油化工股份有限公司	可膨胀石墨材料及其制备方法和应用
CN114162815B (zh) *	2020-09-10	2023-03-10	中国石油化工股份有限公司	可膨胀石墨材料及其制备方法和应用

Also Published As

Publication number	Publication date
JPS6313929B2 (fr)	1988-03-28

Legal Events

Date	Code	Title	Description
2004-11-26	EXPY	Cancellation because of completion of term

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