JPS6136850B2 - - Google Patents

Info

Publication number: JPS6136850B2
Authority: JP; Japan
Prior art keywords: epoxy resin; weight; parts; anhydride; poise
Prior art date: 1981-05-19
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP7618781A

Other languages

English (en)

Japanese (ja)

Other versions

JPS57190018A (en

Inventor

Takeshi Nakahara

Hiroshi Myajima

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Resonac Corp

Original Assignee

Hitachi Chemical Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-05-19

Filing date

1981-05-19

Publication date

1986-08-20

1981-05-19 Application filed by Hitachi Chemical Co Ltd filed Critical Hitachi Chemical Co Ltd

1981-05-19 Priority to JP7618781A priority Critical patent/JPS57190018A/ja

1982-11-22 Publication of JPS57190018A publication Critical patent/JPS57190018A/ja

1986-08-20 Publication of JPS6136850B2 publication Critical patent/JPS6136850B2/ja

Status Granted legal-status Critical Current

Links

239000000203 mixture Substances 0.000 claims description 40
239000003822 epoxy resin Substances 0.000 claims description 31
229920000647 polyepoxide Polymers 0.000 claims description 31
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 claims description 21
OBETXYAYXDNJHR-UHFFFAOYSA-N 2-Ethylhexanoic acid Chemical compound CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 claims description 14
SHZIWNPUGXLXDT-UHFFFAOYSA-N caproic acid ethyl ester Natural products CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 14
150000008064 anhydrides Chemical class 0.000 claims description 6
239000000047 product Substances 0.000 description 15
238000010438 heat treatment Methods 0.000 description 10
150000008065 acid anhydrides Chemical class 0.000 description 8
ULKLGIFJWFIQFF-UHFFFAOYSA-N 5K8XI641G3 Chemical compound CCC1=NC=C(C)N1 ULKLGIFJWFIQFF-UHFFFAOYSA-N 0.000 description 7
239000010409 thin film Substances 0.000 description 6
PQAMFDRRWURCFQ-UHFFFAOYSA-N 2-ethyl-1h-imidazole Chemical compound CCC1=NC=CN1 PQAMFDRRWURCFQ-UHFFFAOYSA-N 0.000 description 5
MWSKJDNQKGCKPA-UHFFFAOYSA-N 6-methyl-3a,4,5,7a-tetrahydro-2-benzofuran-1,3-dione Chemical compound C1CC(C)=CC2C(=O)OC(=O)C12 MWSKJDNQKGCKPA-UHFFFAOYSA-N 0.000 description 5
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 5
238000001035 drying Methods 0.000 description 5
239000007788 liquid Substances 0.000 description 4
BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 4
LXBGSDVWAMZHDD-UHFFFAOYSA-N 2-methyl-1h-imidazole Chemical compound CC1=NC=CN1 LXBGSDVWAMZHDD-UHFFFAOYSA-N 0.000 description 3
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 3
150000002460 imidazoles Chemical class 0.000 description 3
238000005470 impregnation Methods 0.000 description 3
OBETXYAYXDNJHR-SSDOTTSWSA-M (2r)-2-ethylhexanoate Chemical compound CCCC[C@@H](CC)C([O-])=O OBETXYAYXDNJHR-SSDOTTSWSA-M 0.000 description 2
-1 (3,4-epoxycyclohexyl) methyl Chemical group 0.000 description 2
OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 2
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
HYTYOCLNXDJGEK-UHFFFAOYSA-N C(=O)O.C(C)C=1NC=CN1 Chemical compound C(=O)O.C(C)C=1NC=CN1 HYTYOCLNXDJGEK-UHFFFAOYSA-N 0.000 description 2
239000004593 Epoxy Substances 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 2
PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 description 2
238000005266 casting Methods 0.000 description 2
125000003700 epoxy group Chemical group 0.000 description 2
150000002148 esters Chemical class 0.000 description 2
235000019253 formic acid Nutrition 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000008018 melting Effects 0.000 description 2
XLSZMDLNRCVEIJ-UHFFFAOYSA-N methylimidazole Natural products CC1=CNC=N1 XLSZMDLNRCVEIJ-UHFFFAOYSA-N 0.000 description 2
239000002244 precipitate Substances 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
MUTGBJKUEZFXGO-OLQVQODUSA-N (3as,7ar)-3a,4,5,6,7,7a-hexahydro-2-benzofuran-1,3-dione Chemical compound C1CCC[C@@H]2C(=O)OC(=O)[C@@H]21 MUTGBJKUEZFXGO-OLQVQODUSA-N 0.000 description 1
KMOUUZVZFBCRAM-OLQVQODUSA-N (3as,7ar)-3a,4,7,7a-tetrahydro-2-benzofuran-1,3-dione Chemical compound C1C=CC[C@@H]2C(=O)OC(=O)[C@@H]21 KMOUUZVZFBCRAM-OLQVQODUSA-N 0.000 description 1
FBHPRUXJQNWTEW-UHFFFAOYSA-N 1-benzyl-2-methylimidazole Chemical compound CC1=NC=CN1CC1=CC=CC=C1 FBHPRUXJQNWTEW-UHFFFAOYSA-N 0.000 description 1
OAKAPFPXXUWHMV-UHFFFAOYSA-N 2-methoxycarbonylcyclohex-3-ene-1-carboxylic acid Chemical compound COC(=O)C1C=CCCC1C(O)=O OAKAPFPXXUWHMV-UHFFFAOYSA-N 0.000 description 1
OVEUFHOBGCSKSH-UHFFFAOYSA-N 2-methyl-n,n-bis(oxiran-2-ylmethyl)aniline Chemical compound CC1=CC=CC=C1N(CC1OC1)CC1OC1 OVEUFHOBGCSKSH-UHFFFAOYSA-N 0.000 description 1
XYXBMCIMPXOBLB-UHFFFAOYSA-N 3,4,5-tris(dimethylamino)-2-methylphenol Chemical compound CN(C)C1=CC(O)=C(C)C(N(C)C)=C1N(C)C XYXBMCIMPXOBLB-UHFFFAOYSA-N 0.000 description 1
WVRNUXJQQFPNMN-VAWYXSNFSA-N 3-[(e)-dodec-1-enyl]oxolane-2,5-dione Chemical compound CCCCCCCCCC\C=C\C1CC(=O)OC1=O WVRNUXJQQFPNMN-VAWYXSNFSA-N 0.000 description 1
OXQXGKNECHBVMO-UHFFFAOYSA-N 7-oxabicyclo[4.1.0]heptane-4-carboxylic acid Chemical compound C1C(C(=O)O)CCC2OC21 OXQXGKNECHBVMO-UHFFFAOYSA-N 0.000 description 1
BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 description 1
LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 description 1
230000005856 abnormality Effects 0.000 description 1
238000000862 absorption spectrum Methods 0.000 description 1
239000002253 acid Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
150000001334 alicyclic compounds Chemical class 0.000 description 1
OCBHHZMJRVXXQK-UHFFFAOYSA-M benzyl-dimethyl-tetradecylazanium;chloride Chemical compound [Cl-].CCCCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 OCBHHZMJRVXXQK-UHFFFAOYSA-M 0.000 description 1
XFUOBHWPTSIEOV-UHFFFAOYSA-N bis(oxiran-2-ylmethyl) cyclohexane-1,2-dicarboxylate Chemical compound C1CCCC(C(=O)OCC2OC2)C1C(=O)OCC1CO1 XFUOBHWPTSIEOV-UHFFFAOYSA-N 0.000 description 1
JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
230000008094 contradictory effect Effects 0.000 description 1
IFDVQVHZEKPUSC-UHFFFAOYSA-N cyclohex-3-ene-1,2-dicarboxylic acid Chemical compound OC(=O)C1CCC=CC1C(O)=O IFDVQVHZEKPUSC-UHFFFAOYSA-N 0.000 description 1
150000001991 dicarboxylic acids Chemical class 0.000 description 1
238000007598 dipping method Methods 0.000 description 1
LDLDYFCCDKENPD-UHFFFAOYSA-N ethenylcyclohexane Chemical compound C=CC1CCCCC1 LDLDYFCCDKENPD-UHFFFAOYSA-N 0.000 description 1
150000002170 ethers Chemical class 0.000 description 1
WNBZZZXHGXBKSD-UHFFFAOYSA-N ethyl 4-ethylhexanoate Chemical compound CCOC(=O)CCC(CC)CC WNBZZZXHGXBKSD-UHFFFAOYSA-N 0.000 description 1
150000004675 formic acid derivatives Chemical class 0.000 description 1
ANSXAPJVJOKRDJ-UHFFFAOYSA-N furo[3,4-f][2]benzofuran-1,3,5,7-tetrone Chemical compound C1=C2C(=O)OC(=O)C2=CC2=C1C(=O)OC2=O ANSXAPJVJOKRDJ-UHFFFAOYSA-N 0.000 description 1
238000001879 gelation Methods 0.000 description 1
125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
239000011810 insulating material Substances 0.000 description 1
238000009413 insulation Methods 0.000 description 1
150000003893 lactate salts Chemical class 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
238000000034 method Methods 0.000 description 1
VYKXQOYUCMREIS-UHFFFAOYSA-N methylhexahydrophthalic anhydride Chemical compound C1CCCC2C(=O)OC(=O)C21C VYKXQOYUCMREIS-UHFFFAOYSA-N 0.000 description 1
238000002156 mixing Methods 0.000 description 1
150000004965 peroxy acids Chemical class 0.000 description 1
150000002989 phenols Chemical class 0.000 description 1
239000011342 resin composition Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
UFDHBDMSHIXOKF-UHFFFAOYSA-N tetrahydrophthalic acid Natural products OC(=O)C1=C(C(O)=O)CCCC1 UFDHBDMSHIXOKF-UHFFFAOYSA-N 0.000 description 1
SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Landscapes

Epoxy Resins (AREA)

JP7618781A 1981-05-19 1981-05-19 Epoxy resin composition Granted JPS57190018A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP7618781A JPS57190018A (en)	1981-05-19	1981-05-19	Epoxy resin composition

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP7618781A JPS57190018A (en)	1981-05-19	1981-05-19	Epoxy resin composition

Publications (2)

Publication Number	Publication Date
JPS57190018A JPS57190018A (en)	1982-11-22
JPS6136850B2 true JPS6136850B2 (2)	1986-08-20

Family

ID=13598116

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP7618781A Granted JPS57190018A (en)	1981-05-19	1981-05-19	Epoxy resin composition

Country Status (1)

Country	Link
JP (1)	JPS57190018A (2)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP1646054A4 (en)	2003-07-11	2010-05-19	Ube Industries	ACIDS-BASE MIXTURE AND ION CONDUCTOR COMPOSED FROM SUCH A MIXTURE
CN109563240A (zh) *	2016-08-15	2019-04-02	赢创德固赛有限公司	用于环氧树脂体系的具有咪唑盐添加剂的酸酐环氧固化剂
KR102439519B1 (ko) *	2016-12-12	2022-09-05	에보니크 오퍼레이션즈 게엠베하	신규한 저온 무수물 에폭시 경화된 시스템

1981
- 1981-05-19 JP JP7618781A patent/JPS57190018A/ja active Granted

Also Published As

Publication number	Publication date
JPS57190018A (en)	1982-11-22

Publication	Publication Date	Title
US4026862A (en)	1977-05-31	Carboxylic acid storage stabilizers for latent catalyst cured epoxy resins
JP3201262B2 (ja)	2001-08-20	熱硬化性樹脂組成物，電機絶縁線輪，回転電機及びその製造方法
US4564651A (en)	1986-01-14	Method for the manufacture of reaction resin molding materials
EP0009645B1 (en)	1982-12-15	5-(2,5-diketotetrahydrofuryl)-3-methyl-3-cyclohexene-1,2-dicarboxylicanhydride, its use as curing agent for epoxy resins and as raw material for the production of polyimides, epoxy resins containing it, and their use in the preparation of various articles, and powder coating compositions
JP2019524967A (ja)	2019-09-05	エポキシ樹脂系用のイミダゾール塩添加剤を含有する酸無水物エポキシ硬化剤
EP0117113A2 (en)	1984-08-29	Curing agents for epoxy resins
EP0318088B1 (en)	1993-07-21	Thermosetting liquid composition containing a polyepoxide
US4020017A (en)	1977-04-26	Epoxides containing organo-tin compounds and electrical members insulated therewith
US3637572A (en)	1972-01-25	Epoxy resins with organoboron cure promotors
JPS5817534B2 (ja)	1983-04-07	可撓性エポキシ樹脂組成物
JPS6136850B2 (2)	1986-08-20
JP3399095B2 (ja)	2003-04-21	液状エポキシ樹脂組成物
JPH06233486A (ja)	1994-08-19	絶縁電気線輪、回転電機及びその製造方法
JPH06192396A (ja)	1994-07-12	一液型エポキシ樹脂組成物
JPH05279451A (ja)	1993-10-26	エポキシ樹脂組成物及びその硬化物
JP2763388B2 (ja)	1998-06-11	結晶化防止方法
JP2789002B2 (ja)	1998-08-20	エポキシ樹脂組成物
JPH043407B2 (2)	1992-01-23
JPH07224153A (ja)	1995-08-22	エポキシ樹脂硬化促進剤
JP2511691B2 (ja)	1996-07-03	エポキシ樹脂硬化剤組成物並びにエポキシ樹脂組成物
JPS61293216A (ja)	1986-12-24	エポキシ樹脂硬化剤
JPS61293217A (ja)	1986-12-24	エポキシ樹脂硬化剤
JPS6119664B2 (2)	1986-05-19
CN111164126A (zh)	2020-05-15	浸渍树脂混合物
US4307213A (en)	1981-12-22	Curable epoxy resin compositions