JPS6172229A - スプラッシュ調製したハロゲン化銀乳剤の製法 - Google Patents

スプラッシュ調製したハロゲン化銀乳剤の製法

Info

Publication number: JPS6172229A
Authority: JP; Japan
Prior art keywords: prepared; splash; silver; silver halide; emulsion
Prior art date: 1984-09-06
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP19500185A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0443569B2 (2

Inventor

ダグラス・リー・ウイルハイト

ダニエル・ジエイムズ・ミツケウイツチ

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

EIDP Inc

Original Assignee

EI Du Pont de Nemours and Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-09-06

Filing date

1985-09-05

Publication date

1986-04-14

1985-09-05 Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co

1986-04-14 Publication of JPS6172229A publication Critical patent/JPS6172229A/ja

1992-07-17 Publication of JPH0443569B2 publication Critical patent/JPH0443569B2/ja

Status Granted legal-status Critical Current

Links

239000000839 emulsion Substances 0.000 title claims description 67
229910052709 silver Inorganic materials 0.000 title claims description 40
239000004332 silver Substances 0.000 title claims description 37
-1 silver halide Chemical class 0.000 title claims description 27
238000000034 method Methods 0.000 claims description 54
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims description 36
239000013078 crystal Substances 0.000 claims description 25
229910001961 silver nitrate Inorganic materials 0.000 claims description 12
238000009826 distribution Methods 0.000 claims description 11
238000002156 mixing Methods 0.000 claims description 10
238000004519 manufacturing process Methods 0.000 claims description 6
150000004820 halides Chemical class 0.000 claims description 5
230000001681 protective effect Effects 0.000 claims description 5
239000000084 colloidal system Substances 0.000 claims description 4
239000003513 alkali Substances 0.000 claims description 3
229910001508 alkali metal halide Inorganic materials 0.000 claims description 3
150000008045 alkali metal halides Chemical class 0.000 claims description 2
239000007864 aqueous solution Substances 0.000 claims 1
239000000243 solution Substances 0.000 description 30
235000013339 cereals Nutrition 0.000 description 29
230000000052 comparative effect Effects 0.000 description 28
108010010803 Gelatin Proteins 0.000 description 16
239000008273 gelatin Substances 0.000 description 16
229920000159 gelatin Polymers 0.000 description 16
235000019322 gelatine Nutrition 0.000 description 16
235000011852 gelatine desserts Nutrition 0.000 description 16
239000002245 particle Substances 0.000 description 15
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 11
238000001556 precipitation Methods 0.000 description 10
239000000203 mixture Substances 0.000 description 8
239000011248 coating agent Substances 0.000 description 7
238000000576 coating method Methods 0.000 description 7
206010070834 Sensitisation Diseases 0.000 description 6
230000032683 aging Effects 0.000 description 6
210000003127 knee Anatomy 0.000 description 6
230000008313 sensitization Effects 0.000 description 6
238000002360 preparation method Methods 0.000 description 5
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
230000007547 defect Effects 0.000 description 4
239000008367 deionised water Substances 0.000 description 4
229910021641 deionized water Inorganic materials 0.000 description 4
238000000635 electron micrograph Methods 0.000 description 4
NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Substances [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 4
229910052703 rhodium Inorganic materials 0.000 description 4
239000010948 rhodium Substances 0.000 description 4
MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 4
230000005070 ripening Effects 0.000 description 4
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 4
239000004094 surface-active agent Substances 0.000 description 4
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
239000011230 binding agent Substances 0.000 description 3
239000003795 chemical substances by application Substances 0.000 description 3
230000018109 developmental process Effects 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
239000010931 gold Substances 0.000 description 3
150000003839 salts Chemical class 0.000 description 3
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 3
238000003756 stirring Methods 0.000 description 3
239000011593 sulfur Substances 0.000 description 3
229910052717 sulfur Inorganic materials 0.000 description 3
238000005406 washing Methods 0.000 description 3
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 2
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
229910021612 Silver iodide Inorganic materials 0.000 description 2
238000005299 abrasion Methods 0.000 description 2
229960000583 acetic acid Drugs 0.000 description 2
238000001493 electron microscopy Methods 0.000 description 2
239000012362 glacial acetic acid Substances 0.000 description 2
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
229910052737 gold Inorganic materials 0.000 description 2
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 2
CBEQRNSPHCCXSH-UHFFFAOYSA-N iodine monobromide Chemical compound IBr CBEQRNSPHCCXSH-UHFFFAOYSA-N 0.000 description 2
239000007788 liquid Substances 0.000 description 2
239000000463 material Substances 0.000 description 2
229920000139 polyethylene terephthalate Polymers 0.000 description 2
239000005020 polyethylene terephthalate Substances 0.000 description 2
239000011148 porous material Substances 0.000 description 2
229940045105 silver iodide Drugs 0.000 description 2
239000003381 stabilizer Substances 0.000 description 2
239000000758 substrate Substances 0.000 description 2
238000009827 uniform distribution Methods 0.000 description 2
101710134784 Agnoprotein Proteins 0.000 description 1
229920000742 Cotton Polymers 0.000 description 1
241000218691 Cupressaceae Species 0.000 description 1
229910017974 NH40H Inorganic materials 0.000 description 1
229910004879 Na2S2O5 Inorganic materials 0.000 description 1
241001666145 Noia Species 0.000 description 1
240000007594 Oryza sativa Species 0.000 description 1
235000007164 Oryza sativa Nutrition 0.000 description 1
239000004372 Polyvinyl alcohol Substances 0.000 description 1
229910021607 Silver chloride Inorganic materials 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000002519 antifouling agent Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
210000000988 bone and bone Anatomy 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000000701 coagulant Substances 0.000 description 1
230000015271 coagulation Effects 0.000 description 1
238000005345 coagulation Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000005520 cutting process Methods 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
238000007598 dipping method Methods 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000000855 fungicidal effect Effects 0.000 description 1
239000000417 fungicide Substances 0.000 description 1
239000000499 gel Substances 0.000 description 1
238000011065 in-situ storage Methods 0.000 description 1
BVJUXXYBIMHHDW-UHFFFAOYSA-N iodane Chemical compound I.I BVJUXXYBIMHHDW-UHFFFAOYSA-N 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
238000001000 micrograph Methods 0.000 description 1
238000003921 particle size analysis Methods 0.000 description 1
CMCWWLVWPDLCRM-UHFFFAOYSA-N phenidone Chemical compound N1C(=O)CCN1C1=CC=CC=C1 CMCWWLVWPDLCRM-UHFFFAOYSA-N 0.000 description 1
239000004848 polyfunctional curative Substances 0.000 description 1
229920002689 polyvinyl acetate Polymers 0.000 description 1
239000011118 polyvinyl acetate Substances 0.000 description 1
229920002451 polyvinyl alcohol Polymers 0.000 description 1
229920001289 polyvinyl ether Polymers 0.000 description 1
SONJTKJMTWTJCT-UHFFFAOYSA-K rhodium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[Rh+3] SONJTKJMTWTJCT-UHFFFAOYSA-K 0.000 description 1
235000009566 rice Nutrition 0.000 description 1
230000035945 sensitivity Effects 0.000 description 1
230000001235 sensitizing effect Effects 0.000 description 1
238000004904 shortening Methods 0.000 description 1
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
235000010262 sodium metabisulphite Nutrition 0.000 description 1
239000007787 solid Substances 0.000 description 1
230000007928 solubilization Effects 0.000 description 1
238000005063 solubilization Methods 0.000 description 1
241000894007 species Species 0.000 description 1
230000003595 spectral effect Effects 0.000 description 1
239000000126 substance Substances 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
229910052721 tungsten Inorganic materials 0.000 description 1
239000010937 tungsten Substances 0.000 description 1
239000000052 vinegar Substances 0.000 description 1
235000021419 vinegar Nutrition 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1

Classifications

- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/035—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein characterised by the crystal form or composition, e.g. mixed grain
- G03C2001/0357—Monodisperse emulsion

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Physics & Mathematics (AREA)
General Physics & Mathematics (AREA)
Silver Salt Photography Or Processing Solution Therefor (AREA)
Colloid Chemistry (AREA)

JP19500185A 1984-09-06 1985-09-05 スプラッシュ調製したハロゲン化銀乳剤の製法 Granted JPS6172229A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US64780884A	1984-09-06	1984-09-06
US647808		1984-09-06

Publications (2)

Publication Number	Publication Date
JPS6172229A true JPS6172229A (ja)	1986-04-14
JPH0443569B2 JPH0443569B2 (2)	1992-07-17

Family

ID=24598347

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP19500185A Granted JPS6172229A (ja)	1984-09-06	1985-09-05	スプラッシュ調製したハロゲン化銀乳剤の製法

Country Status (3)

Country	Link
EP (1)	EP0174018B1 (2)
JP (1)	JPS6172229A (2)
DE (1)	DE3582633D1 (2)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6332537A (ja) *	1986-06-18	1988-02-12	Konica Corp	ハロゲン化銀写真感光乳剤及びその製造方法及び該乳剤を用いたハロゲン化銀写真感光材料

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4794070A (en) *	1987-06-09	1988-12-27	Minnesota Mining And Manufacturing Company	Automatically processible photographic element comprising a non-silver halide layer containing bromide
EP0632321B1 (en) *	1993-07-02	1999-12-08	Minnesota Mining And Manufacturing Company	Process for preparing monodispersed silver halide emulsions

Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5542739A (en) *	1978-09-20	1980-03-26	Nippon Telegr & Teleph Corp <Ntt>	Cylinder cutting method and device with multi blade
JPS581408A (ja) *	1981-06-25	1983-01-06	小堀　しづ	ヘヤ−ブラシ及びクシ

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1162689B (de) *	1962-11-15	1964-02-06	Perutz Photowerke G M B H	Verfahren zur Herstellung von lichtempfindlichen photographischen Emulsionen
GB1170648A (en) *	1966-11-12	1969-11-12	Fuji Photo Film Co Ltd	Process for the Preparation of Photographic Light-Sensitive Emulsions
US4339532A (en) *	1981-01-08	1982-07-13	Polaroid Corporation	Novel photosensitive silver halide emulsion and method of preparing same

1985
- 1985-09-04 DE DE8585111158T patent/DE3582633D1/de not_active Expired - Lifetime
- 1985-09-04 EP EP19850111158 patent/EP0174018B1/en not_active Expired
- 1985-09-05 JP JP19500185A patent/JPS6172229A/ja active Granted

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5542739A (en) *	1978-09-20	1980-03-26	Nippon Telegr & Teleph Corp <Ntt>	Cylinder cutting method and device with multi blade
JPS581408A (ja) *	1981-06-25	1983-01-06	小堀　しづ	ヘヤ−ブラシ及びクシ

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS6332537A (ja) *	1986-06-18	1988-02-12	Konica Corp	ハロゲン化銀写真感光乳剤及びその製造方法及び該乳剤を用いたハロゲン化銀写真感光材料

Also Published As

Publication number	Publication date
DE3582633D1 (de)	1991-05-29
EP0174018A3 (en)	1988-02-17
EP0174018A2 (en)	1986-03-12
EP0174018B1 (en)	1991-04-24
JPH0443569B2 (2)	1992-07-17

Publication	Publication Date	Title
US4184877A (en)	1980-01-22	Process for the manufacture of photographic silver halide emulsions containing silver halide crystals of the twinned type
US4184878A (en)	1980-01-22	Process for the manufacture of photographic silver halide emulsions containing silver halide crystals of the twinned type
JP2670847B2 (ja)	1997-10-29	ハロゲン化銀写真乳剤およびその製造方法
GB1570581A (en)	1980-07-02	Preparation of silver halide emulsions
JPS63107813A (ja)	1988-05-12	せまい粒度分布を有する平板状粒子を含有する写真乳剤の製造法
US5017469A (en)	1991-05-21	Twinned emulsions made from silver iodide seed crystals having an aspect ratio of at least 2:1
JPS6158027B2 (2)	1986-12-09
JP3025585B2 (ja)	2000-03-27	ハロゲン化銀乳剤
JPS5824772B2 (ja)	1983-05-23	新規なハロゲン化銀結晶の製造法
JPH0833598B2 (ja)	1996-03-29	臭化物シエルを用いる修正された晶癖をもつ高塩化物結晶の安定化方法
JPS6172229A (ja)	1986-04-14	スプラッシュ調製したハロゲン化銀乳剤の製法
JP3383397B2 (ja)	2003-03-04	ハロゲン化銀乳剤
EP0569971B1 (en)	1999-03-24	Silver halide emulsion
EP0645670A1 (en)	1995-03-29	Silver halide emulsion
US5009991A (en)	1991-04-23	Silver halide emulsions containing twinned silver halide crystals
JPS62218959A (ja)	1987-09-26	ハロゲン化銀写真乳剤の製造方法
US4678744A (en)	1987-07-07	Splash-prepared silver halide emulsions with a uniform particle size distribution
JPH0711679B2 (ja)	1995-02-08	ハロゲン化銀乳剤の製造方法
JPS59111144A (ja)	1984-06-27	ハロゲン化銀写真乳剤の製造方法
JP2840897B2 (ja)	1998-12-24	ハロゲン化銀乳剤およびその製造方法
JP3388914B2 (ja)	2003-03-24	ハロゲン化銀乳剤
JPS6046415B2 (ja)	1985-10-16	ハロゲン化銀写真乳剤
JP3325954B2 (ja)	2002-09-17	ハロゲン化銀乳剤
JPH11249248A (ja)	1999-09-17	ハロゲン化銀乳剤
JPH07209784A (ja)	1995-08-11	ハロゲン化銀写真乳剤及びそれを用いたハロゲン化銀写真感光材料

JPS6172229A - スプラッシュ調製したハロゲン化銀乳剤の製法 - Google Patents

Info

Links

Classifications

Landscapes

Applications Claiming Priority (2)

Publications (2)

Family

ID=24598347

Family Applications (1)

Country Status (3)

Cited By (1)

Families Citing this family (2)

Citations (2)

Family Cites Families (3)

Patent Citations (2)

Cited By (1)

Also Published As

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