JPS63262805A - 鉄ベース永久磁石の製造方法 - Google Patents
鉄ベース永久磁石の製造方法Info
- Publication number
- JPS63262805A JPS63262805A JP63083968A JP8396888A JPS63262805A JP S63262805 A JPS63262805 A JP S63262805A JP 63083968 A JP63083968 A JP 63083968A JP 8396888 A JP8396888 A JP 8396888A JP S63262805 A JPS63262805 A JP S63262805A
- Authority
- JP
- Japan
- Prior art keywords
- rare earth
- powder
- phase
- sintering
- magnetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims description 40
- 229910052742 iron Inorganic materials 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 230000005291 magnetic effect Effects 0.000 claims description 42
- 229910052751 metal Inorganic materials 0.000 claims description 42
- 239000002184 metal Substances 0.000 claims description 42
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 36
- 239000000843 powder Substances 0.000 claims description 26
- 150000002910 rare earth metals Chemical class 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 25
- 150000002739 metals Chemical class 0.000 claims description 22
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 21
- 238000005245 sintering Methods 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 16
- 229910052684 Cerium Inorganic materials 0.000 claims description 15
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 13
- 229910052782 aluminium Inorganic materials 0.000 claims description 12
- 229910052796 boron Inorganic materials 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 10
- 229910045601 alloy Inorganic materials 0.000 claims description 9
- 239000000956 alloy Substances 0.000 claims description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 9
- 229910052746 lanthanum Inorganic materials 0.000 claims description 9
- 229910052760 oxygen Inorganic materials 0.000 claims description 9
- 239000001301 oxygen Substances 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 8
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 7
- 229910052786 argon Inorganic materials 0.000 claims description 7
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000003607 modifier Substances 0.000 claims description 7
- -1 rare earth chloride Chemical class 0.000 claims description 7
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 5
- 239000000155 melt Substances 0.000 claims description 5
- 230000000704 physical effect Effects 0.000 claims description 5
- 238000006467 substitution reaction Methods 0.000 claims description 5
- 238000000137 annealing Methods 0.000 claims description 4
- 238000010791 quenching Methods 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000005868 electrolysis reaction Methods 0.000 claims description 3
- 230000005389 magnetism Effects 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 230000000171 quenching effect Effects 0.000 claims description 3
- IKNAJTLCCWPIQD-UHFFFAOYSA-K cerium(3+);lanthanum(3+);neodymium(3+);oxygen(2-);phosphate Chemical compound [O-2].[La+3].[Ce+3].[Nd+3].[O-]P([O-])([O-])=O IKNAJTLCCWPIQD-UHFFFAOYSA-K 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- 239000013078 crystal Substances 0.000 claims description 2
- 239000003814 drug Substances 0.000 claims description 2
- 229940079593 drug Drugs 0.000 claims description 2
- 229910000765 intermetallic Inorganic materials 0.000 claims description 2
- 229910052590 monazite Inorganic materials 0.000 claims description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims 2
- 239000003963 antioxidant agent Substances 0.000 claims 1
- 230000003078 antioxidant effect Effects 0.000 claims 1
- 230000001680 brushing effect Effects 0.000 claims 1
- 238000000465 moulding Methods 0.000 claims 1
- 239000011780 sodium chloride Substances 0.000 claims 1
- 229910017052 cobalt Inorganic materials 0.000 description 12
- 239000010941 cobalt Substances 0.000 description 12
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 9
- 229910052779 Neodymium Inorganic materials 0.000 description 8
- 229910000722 Didymium Inorganic materials 0.000 description 7
- 241000224487 Didymium Species 0.000 description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
- 238000012545 processing Methods 0.000 description 6
- 230000014759 maintenance of location Effects 0.000 description 5
- 229910052777 Praseodymium Inorganic materials 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000011159 matrix material Substances 0.000 description 4
- 229910052692 Dysprosium Inorganic materials 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000005415 magnetization Effects 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229910000859 α-Fe Inorganic materials 0.000 description 3
- 229910000828 alnico Inorganic materials 0.000 description 2
- 238000012993 chemical processing Methods 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 239000000696 magnetic material Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000018185 Betula X alpestris Nutrition 0.000 description 1
- 235000018212 Betula X uliginosa Nutrition 0.000 description 1
- 241001174990 Boros Species 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical class [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 1
- 244000299906 Cucumis sativus var. sativus Species 0.000 description 1
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 241000282326 Felis catus Species 0.000 description 1
- 229910001047 Hard ferrite Inorganic materials 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 230000018199 S phase Effects 0.000 description 1
- 229910052772 Samarium Inorganic materials 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004873 anchoring Methods 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- ZADPBFCGQRWHPN-UHFFFAOYSA-N boronic acid Chemical compound OBO ZADPBFCGQRWHPN-UHFFFAOYSA-N 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000003841 chloride salts Chemical class 0.000 description 1
- KPLQYGBQNPPQGA-UHFFFAOYSA-N cobalt samarium Chemical compound [Co].[Sm] KPLQYGBQNPPQGA-UHFFFAOYSA-N 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 229910052802 copper Chemical class 0.000 description 1
- 239000010949 copper Chemical class 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 230000005294 ferromagnetic effect Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 239000003049 inorganic solvent Substances 0.000 description 1
- 229910001867 inorganic solvent Inorganic materials 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 230000016507 interphase Effects 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- QEFYFXOXNSNQGX-UHFFFAOYSA-N neodymium atom Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910000938 samarium–cobalt magnet Inorganic materials 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/10—Sintering only
- B22F3/1003—Use of special medium during sintering, e.g. sintering aid
- B22F3/1007—Atmosphere
- B22F3/101—Changing atmosphere
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
- H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
- H01F1/047—Alloys characterised by their composition
- H01F1/053—Alloys characterised by their composition containing rare earth metals
- H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
- H01F1/057—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
- H01F1/0571—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
- H01F1/0575—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
- H01F1/0577—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together sintered
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Power Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Hard Magnetic Materials (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US3486287A | 1987-04-06 | 1987-04-06 | |
| US034862 | 1987-04-06 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS63262805A true JPS63262805A (ja) | 1988-10-31 |
Family
ID=21879060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP63083968A Pending JPS63262805A (ja) | 1987-04-06 | 1988-04-05 | 鉄ベース永久磁石の製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0286357A3 (fr) |
| JP (1) | JPS63262805A (fr) |
| KR (1) | KR880013194A (fr) |
| AU (1) | AU608309B2 (fr) |
| BR (1) | BR8801585A (fr) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU609669B2 (en) * | 1986-10-13 | 1991-05-02 | N.V. Philips Gloeilampenfabrieken | Method of manufacturing a permanent magnet |
| FR2652319A1 (fr) * | 1989-09-26 | 1991-03-29 | Eyherabide Michel | Retroviseur automobile pour supprimer l'angle mort. |
| FR2652535A1 (fr) * | 1989-10-03 | 1991-04-05 | Caine Stephane | Procede de fabrication simplifiee de pastilles de composition donnee appartenant au groupe des supraconducteurs, des ferrites et des materiaux a structure granulaire complexe. |
| US6669788B1 (en) | 1999-02-12 | 2003-12-30 | General Electric Company | Permanent magnetic materials of the Fe-B-R tpe, containing Ce and Nd and/or Pr, and process for manufacture |
| EP1072044A1 (fr) * | 1999-02-12 | 2001-01-31 | General Electric Company | Composition riche en praseodyme a base de fer, de bore et de terres rares, aimant permanent produit a partir de celle-ci et procede de production |
| CN1251252C (zh) * | 1999-02-12 | 2006-04-12 | 通用电气公司 | 含有铈、钕和/或镨的铁-硼-稀土型永磁材料及其生产方法 |
| EP1059645B1 (fr) | 1999-06-08 | 2006-06-14 | Shin-Etsu Chemical Co., Ltd. | Ruban mince d'un alliage de terre rare pour aimant permanent |
| US7988795B2 (en) * | 2005-12-02 | 2011-08-02 | Shin-Etsu Chemical Co., Ltd. | R-T-B—C rare earth sintered magnet and making method |
| JP4702542B2 (ja) * | 2005-12-02 | 2011-06-15 | 信越化学工業株式会社 | R−t−b−c型焼結磁石の製造方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61119006A (ja) * | 1984-11-15 | 1986-06-06 | Hitachi Metals Ltd | 焼結磁石の製造方法 |
| JPS61159709A (ja) * | 1985-09-17 | 1986-07-19 | Kaneo Mori | 永久磁石 |
| JPS61208809A (ja) * | 1985-03-13 | 1986-09-17 | Hitachi Metals Ltd | 焼結磁石の製造方法 |
| JPS6223902A (ja) * | 1985-07-23 | 1987-01-31 | Sumitomo Special Metals Co Ltd | 希土類・ボロン・鉄系合金粉末およびその製造方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3379084D1 (en) * | 1982-09-27 | 1989-03-02 | Sumitomo Spec Metals | Permanently magnetizable alloys, magnetic materials and permanent magnets comprising febr or (fe,co)br (r=vave earth) |
| EP0157329A3 (fr) * | 1984-03-30 | 1987-06-16 | Union Oil Company Of California | Aimants contenant PrCo5 |
-
1988
- 1988-04-01 KR KR1019880003727A patent/KR880013194A/ko not_active Withdrawn
- 1988-04-05 EP EP88303018A patent/EP0286357A3/fr not_active Withdrawn
- 1988-04-05 BR BR8801585A patent/BR8801585A/pt unknown
- 1988-04-05 JP JP63083968A patent/JPS63262805A/ja active Pending
- 1988-04-05 AU AU14154/88A patent/AU608309B2/en not_active Ceased
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61119006A (ja) * | 1984-11-15 | 1986-06-06 | Hitachi Metals Ltd | 焼結磁石の製造方法 |
| JPS61208809A (ja) * | 1985-03-13 | 1986-09-17 | Hitachi Metals Ltd | 焼結磁石の製造方法 |
| JPS6223902A (ja) * | 1985-07-23 | 1987-01-31 | Sumitomo Special Metals Co Ltd | 希土類・ボロン・鉄系合金粉末およびその製造方法 |
| JPS61159709A (ja) * | 1985-09-17 | 1986-07-19 | Kaneo Mori | 永久磁石 |
Also Published As
| Publication number | Publication date |
|---|---|
| AU1415488A (en) | 1988-10-06 |
| KR880013194A (ko) | 1988-11-30 |
| EP0286357A3 (fr) | 1990-06-06 |
| AU608309B2 (en) | 1991-03-28 |
| BR8801585A (pt) | 1988-11-08 |
| EP0286357A2 (fr) | 1988-10-12 |
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