JPS6470423A - Production of 1-halogeno-2-alkalols having optical activity - Google Patents
Production of 1-halogeno-2-alkalols having optical activityInfo
- Publication number
- JPS6470423A JPS6470423A JP22292787A JP22292787A JPS6470423A JP S6470423 A JPS6470423 A JP S6470423A JP 22292787 A JP22292787 A JP 22292787A JP 22292787 A JP22292787 A JP 22292787A JP S6470423 A JPS6470423 A JP S6470423A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- organic solvent
- optical activity
- alkalols
- halogeno
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE:To simply obtain the titled substance useful as an intermediate for medicine, agricultural chemical, ferroelectric liquid crystal, etc., by reacting 1,2-epoxyalkanes with a halogen compound containing Li and Cu or Ni. CONSTITUTION:1,2-Epoxyalkanes [e.g. (+)-1,2-epoxyhexane] having optical activity is reacted with a compound expressed by formula I (M is Cu or Ni; X is halogen) at -10-30 deg.C for 3-48hr to provide the compound expressed by formula II. The reaction is preferably carried out in an organic solvent such as THF by dropping an organic solvent solution of compound expressed by formula I into a solution obtained by dissolving 1,2-epoxyalkane in an organic solvent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP22292787A JPS6470423A (en) | 1987-06-19 | 1987-09-08 | Production of 1-halogeno-2-alkalols having optical activity |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15127087 | 1987-06-19 | ||
| JP22292787A JPS6470423A (en) | 1987-06-19 | 1987-09-08 | Production of 1-halogeno-2-alkalols having optical activity |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6470423A true JPS6470423A (en) | 1989-03-15 |
| JPH0420416B2 JPH0420416B2 (en) | 1992-04-02 |
Family
ID=26480571
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP22292787A Granted JPS6470423A (en) | 1987-06-19 | 1987-09-08 | Production of 1-halogeno-2-alkalols having optical activity |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6470423A (en) |
-
1987
- 1987-09-08 JP JP22292787A patent/JPS6470423A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0420416B2 (en) | 1992-04-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Pedersen | Synthetic multidentate macrocyclic compounds | |
| Miller Jr et al. | Perfluoroalkylsilver compounds | |
| McCollum et al. | Bimetallic reactivity. General synthesis of binucleating macrocyclic ligands containing 6-and 4-coordinate sites | |
| JPS6470423A (en) | Production of 1-halogeno-2-alkalols having optical activity | |
| US3027371A (en) | Molybdenum-containing derivatives of 1-hydroxy-2-pyridinethiones and method of preparing same | |
| JPS6475468A (en) | Production of 2,3,5-trichloropyridine | |
| JPS63258462A (en) | 2-phenoxypyrimidine derivatives and herbicides | |
| JPS5692281A (en) | Preparation of 5-amino-1,2,3-thiadiazole | |
| US3493557A (en) | Trialkyl stannyloxy derivatives of fructose,cyclic mercaptols as pesticides | |
| JPS6471850A (en) | Sulfoxide derivative and production thereof | |
| JPS6422846A (en) | Bischloroformate of 2,2-bis(4-hydroxycyclohexyl)propane and production thereof | |
| JPS56120667A (en) | Preparation of chloro-beta-trifluoromethylpyridine | |
| DE3375480D1 (en) | Process for the preparation of 13-cis-retinoic acid | |
| JPS5747304A (en) | Novel tris bipyridyl ruthenium high polymeric complex and its preparation | |
| JPS6442467A (en) | Production of alpha-halogenopyridine derivative | |
| JPS6483042A (en) | Production of alkoxybenzaldehyde | |
| JPS6468380A (en) | Bis(1,2,5)thiadiazolo(3,4-b:3',4'-e)pyrazine | |
| JPS5592343A (en) | Preparation of optically active substituted isovaleric acid | |
| McAlees et al. | Esterification of isocyanide carboxylic acids and hydrolysis of their esters | |
| JPS6438058A (en) | Production of mercaptized ether compound | |
| Okajima et al. | Hydrolytic activation/decomposition pathways of herbicidally active ethyl 5‐[N‐(5, 7‐dimethoxy‐2H‐1, 2, 4‐thiadiazolo [2, 3‐a] pyrimidin‐2‐ylidene) sulfamoyl]‐1, 3‐dimethylpyrazole‐4‐carboxylate | |
| JPS6422845A (en) | Bischloroformate of tricyclo(5.2.1.02,6)decane-dimethanol and production thereof | |
| JPS6416765A (en) | Substituted pyridine compound and production thereof | |
| JPS54157566A (en) | Preparation of nucleoside | |
| Bolger et al. | 1-Amino-2-nitro-4, 5-bis (p-toluenesulfonamido) benzene |