LU86005A1 - Procede pour l'obtention d'une base organique azotee insoluble dans l'eau,au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base,et procede de fabrication de bicarbonate de sodium - Google Patents

Procede pour l'obtention d'une base organique azotee insoluble dans l'eau,au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base,et procede de fabrication de bicarbonate de sodium Download PDF

Info

Publication number: LU86005A1
Authority: LU; Luxembourg
Prior art keywords: organic; aqueous solution; amine; hydrochloride; solution
Prior art date: 1984-07-17

Application number

LU86005A

Other languages

English (en)

French (fr)

Inventor

Ninane Leon

Breton Claude

Original Assignee

Solvay

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-07-17

Filing date

1985-07-15

Publication date

1986-02-12

1985-07-15 Application filed by Solvay filed Critical Solvay

1986-02-12 Publication of LU86005A1 publication Critical patent/LU86005A1/fr

Links

239000007864 aqueous solution Substances 0.000 title claims description 50
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 title claims description 49
238000000034 method Methods 0.000 title claims description 37
239000002585 base Substances 0.000 title claims description 27
235000017557 sodium bicarbonate Nutrition 0.000 title claims description 24
229910000030 sodium bicarbonate Inorganic materials 0.000 title claims description 24
229910052783 alkali metal Inorganic materials 0.000 title claims description 16
238000004519 manufacturing process Methods 0.000 title claims description 12
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 title description 5
150000001340 alkali metals Chemical class 0.000 title description 4
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title 2
XLYOFNOQVPJJNP-PWCQTSIFSA-N Tritiated water Chemical compound [3H]O[3H] XLYOFNOQVPJJNP-PWCQTSIFSA-N 0.000 title 1
229910052757 nitrogen Inorganic materials 0.000 title 1
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 43
-1 nitrogenous organic base Chemical class 0.000 claims description 43
239000000243 solution Substances 0.000 claims description 43
150000001412 amines Chemical class 0.000 claims description 37
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 26
235000002639 sodium chloride Nutrition 0.000 claims description 23
239000011780 sodium chloride Substances 0.000 claims description 23
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
239000003795 chemical substances by application Substances 0.000 claims description 20
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 19
239000000203 mixture Substances 0.000 claims description 19
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims description 19
238000010908 decantation Methods 0.000 claims description 15
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
239000008346 aqueous phase Substances 0.000 claims description 14
239000001569 carbon dioxide Substances 0.000 claims description 10
229910002092 carbon dioxide Inorganic materials 0.000 claims description 10
239000012452 mother liquor Substances 0.000 claims description 9
239000007900 aqueous suspension Substances 0.000 claims description 7
239000007788 liquid Substances 0.000 claims description 7
239000002904 solvent Substances 0.000 claims description 6
239000013589 supplement Substances 0.000 claims description 6
125000004432 carbon atom Chemical group C* 0.000 claims description 5
239000011541 reaction mixture Substances 0.000 claims description 5
150000003973 alkyl amines Chemical class 0.000 claims description 4
239000007787 solid Substances 0.000 claims description 4
UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 3
239000012074 organic phase Substances 0.000 claims description 3
150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
238000006243 chemical reaction Methods 0.000 description 10
239000007789 gas Substances 0.000 description 10
239000003960 organic solvent Substances 0.000 description 10
229920006395 saturated elastomer Polymers 0.000 description 8
238000002425 crystallisation Methods 0.000 description 6
230000008025 crystallization Effects 0.000 description 6
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
150000003141 primary amines Chemical class 0.000 description 5
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 4
150000007529 inorganic bases Chemical class 0.000 description 4
125000001477 organic nitrogen group Chemical group 0.000 description 4
229910052708 sodium Inorganic materials 0.000 description 4
239000011734 sodium Substances 0.000 description 4
AAIUWVOMXTVLRG-UHFFFAOYSA-N 8,8-dimethylnonan-1-amine Chemical compound CC(C)(C)CCCCCCCN AAIUWVOMXTVLRG-UHFFFAOYSA-N 0.000 description 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
229910001514 alkali metal chloride Inorganic materials 0.000 description 3
229910052799 carbon Inorganic materials 0.000 description 3
238000005868 electrolysis reaction Methods 0.000 description 3
230000005484 gravity Effects 0.000 description 3
235000015497 potassium bicarbonate Nutrition 0.000 description 3
229910000028 potassium bicarbonate Inorganic materials 0.000 description 3
239000011736 potassium bicarbonate Substances 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 2
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
235000011941 Tilia x europaea Nutrition 0.000 description 2
239000003513 alkali Substances 0.000 description 2
229910052784 alkaline earth metal Inorganic materials 0.000 description 2
150000001491 aromatic compounds Chemical class 0.000 description 2
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
239000000920 calcium hydroxide Substances 0.000 description 2
229910001861 calcium hydroxide Inorganic materials 0.000 description 2
230000001143 conditioned effect Effects 0.000 description 2
239000013078 crystal Substances 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
229910000041 hydrogen chloride Inorganic materials 0.000 description 2
238000009434 installation Methods 0.000 description 2
239000004571 lime Substances 0.000 description 2
239000012071 phase Substances 0.000 description 2
238000003756 stirring Methods 0.000 description 2
239000008096 xylene Substances 0.000 description 2
HYFLWBNQFMXCPA-UHFFFAOYSA-N 1-ethyl-2-methylbenzene Chemical class CCC1=CC=CC=C1C HYFLWBNQFMXCPA-UHFFFAOYSA-N 0.000 description 1
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
150000007824 aliphatic compounds Chemical class 0.000 description 1
229910001617 alkaline earth metal chloride Inorganic materials 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
239000002152 aqueous-organic solution Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
OCKPCBLVNKHBMX-UHFFFAOYSA-N butylbenzene Chemical class CCCCC1=CC=CC=C1 OCKPCBLVNKHBMX-UHFFFAOYSA-N 0.000 description 1
238000001354 calcination Methods 0.000 description 1
239000001110 calcium chloride Substances 0.000 description 1
229910001628 calcium chloride Inorganic materials 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000010586 diagram Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000000265 homogenisation Methods 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
150000003840 hydrochlorides Chemical class 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
150000002466 imines Chemical class 0.000 description 1
239000000463 material Substances 0.000 description 1
239000012528 membrane Substances 0.000 description 1
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
229910052753 mercury Inorganic materials 0.000 description 1
238000005065 mining Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
150000007530 organic bases Chemical class 0.000 description 1
230000035699 permeability Effects 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
239000011591 potassium Substances 0.000 description 1
239000001103 potassium chloride Substances 0.000 description 1
WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
235000011164 potassium chloride Nutrition 0.000 description 1
150000003242 quaternary ammonium salts Chemical class 0.000 description 1
230000001172 regenerating effect Effects 0.000 description 1
238000012827 research and development Methods 0.000 description 1
150000003335 secondary amines Chemical class 0.000 description 1
238000000926 separation method Methods 0.000 description 1
KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
229910001948 sodium oxide Inorganic materials 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/16—Preparation from compounds of sodium or potassium with amines and carbon dioxide

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Removal Of Specific Substances (AREA)
Treatment Of Water By Oxidation Or Reduction (AREA)
Fertilizers (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

LU86005A 1984-07-17 1985-07-15 Procede pour l'obtention d'une base organique azotee insoluble dans l'eau,au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base,et procede de fabrication de bicarbonate de sodium LU86005A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FR8411424		1984-07-17
FR8411424A FR2567878B1 (fr)	1984-07-17	1984-07-17	Procede pour l'obtention d'une base organique azotee insoluble dans l'eau, au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base, et procede de fabrication de bicarbonate de sodium

Publications (1)

Publication Number	Publication Date
LU86005A1 true LU86005A1 (fr)	1986-02-12

Family

ID=9306264

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU86005A LU86005A1 (fr)	1984-07-17	1985-07-15	Procede pour l'obtention d'une base organique azotee insoluble dans l'eau,au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base,et procede de fabrication de bicarbonate de sodium

Country Status (19)

Country	Link
US (1)	US4677229A (de)
JP (1)	JPS6156157A (de)
AT (1)	AT383591B (de)
AU (1)	AU4485785A (de)
BE (1)	BE902854A (de)
BR (1)	BR8503385A (de)
DE (1)	DE3525573A1 (de)
ES (1)	ES8607208A1 (de)
FR (1)	FR2567878B1 (de)
GB (1)	GB2162176A (de)
IL (1)	IL75759A0 (de)
IT (1)	IT1187690B (de)
LU (1)	LU86005A1 (de)
MA (1)	MA20489A1 (de)
NL (1)	NL8502060A (de)
NO (1)	NO852837L (de)
PT (1)	PT80814B (de)
SE (1)	SE8503478L (de)
ZA (1)	ZA855161B (de)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3443889A (en) *	1964-08-17	1969-05-13	Kaiser Aluminium Chem Corp	Method of synthesis of alkali metal salts
JPS5734020A (en) *	1980-08-06	1982-02-24	Toyo Soda Mfg Co Ltd	Recovery of ammonia

1984
- 1984-07-17 FR FR8411424A patent/FR2567878B1/fr not_active Expired
1985
- 1985-07-09 ZA ZA855161A patent/ZA855161B/xx unknown
- 1985-07-10 IL IL75759A patent/IL75759A0/xx unknown
- 1985-07-11 BE BE1/011295A patent/BE902854A/fr not_active IP Right Cessation
- 1985-07-12 AU AU44857/85A patent/AU4485785A/en not_active Abandoned
- 1985-07-15 PT PT80814A patent/PT80814B/pt unknown
- 1985-07-15 SE SE8503478A patent/SE8503478L/ not_active Application Discontinuation
- 1985-07-15 LU LU86005A patent/LU86005A1/fr unknown
- 1985-07-15 US US06/754,972 patent/US4677229A/en not_active Expired - Fee Related
- 1985-07-16 GB GB08517879A patent/GB2162176A/en not_active Withdrawn
- 1985-07-16 NO NO852837A patent/NO852837L/no unknown
- 1985-07-16 BR BR8503385A patent/BR8503385A/pt unknown
- 1985-07-16 ES ES545249A patent/ES8607208A1/es not_active Expired
- 1985-07-16 AT AT0210085A patent/AT383591B/de not_active IP Right Cessation
- 1985-07-16 JP JP60156847A patent/JPS6156157A/ja active Pending
- 1985-07-16 MA MA20714A patent/MA20489A1/fr unknown
- 1985-07-17 DE DE19853525573 patent/DE3525573A1/de not_active Withdrawn
- 1985-07-17 IT IT21613/85A patent/IT1187690B/it active
- 1985-07-17 NL NL8502060A patent/NL8502060A/nl not_active Application Discontinuation

Also Published As

Publication number	Publication date
US4677229A (en)	1987-06-30
IL75759A0 (en)	1985-11-29
FR2567878B1 (fr)	1986-12-05
IT1187690B (it)	1987-12-23
GB2162176A (en)	1986-01-29
AU4485785A (en)	1986-01-23
IT8521613A0 (it)	1985-07-17
PT80814B (fr)	1987-03-23
JPS6156157A (ja)	1986-03-20
DE3525573A1 (de)	1986-01-23
PT80814A (fr)	1985-08-01
ES545249A0 (es)	1986-05-16
BR8503385A (pt)	1986-04-08
ES8607208A1 (es)	1986-05-16
ZA855161B (en)	1986-03-26
AT383591B (de)	1987-07-27
BE902854A (fr)	1986-01-13
MA20489A1 (fr)	1986-04-01
NL8502060A (nl)	1986-02-17
GB8517879D0 (en)	1985-08-21
FR2567878A1 (fr)	1986-01-24
ATA210085A (de)	1986-12-15
NO852837L (no)	1986-01-20
SE8503478D0 (sv)	1985-07-15
SE8503478L (sv)	1986-01-18

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FR2593829A1 (fr)	1987-08-07	Procede pour extraire selectivement du zinc d'une saumure aqueuse
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LU86005A1 (fr)	1986-02-12	Procede pour l'obtention d'une base organique azotee insoluble dans l'eau,au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base,et procede de fabrication de bicarbonate de sodium
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CA1217783A (fr)	1987-02-10	Procede et installation pour la production d'une solution organique d'une base organique insoluble dans l'eau
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EP0266830B1 (de)	1992-07-29	Verfahren für die Extraktion einer organischen Flüssigkeit, die eine azotierte organische Base aus einer wässrigen Suspension von mineralischen Teilchen enthält und Verfahren zur Herstellung von Alkalimetall-Bikarbonat
LU85506A1 (fr)	1985-04-24	Procede pour la preparation d'une solution aqueuse de chlorure de sodium et procede de fabrication de bicarbonate de sodium
LU85684A1 (fr)	1985-07-24	Procede pour la production de bicarbonate de metal alcalin et carbonate de sodium obtenu a partir de ce procede
EP0266831B1 (de)	1992-07-29	Verfahren zum Trennen von Alkalimetallbikarbonat-Teilchen von einer an ihrer Oberfläche adsorbierten flüssigen Schicht von Chlorhydrat einer azotierten organischen Base und Verfahren zur Herstellung von Alkalimetallbikarbonat
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FR2590495A1 (fr)	1987-05-29	Procede pour epurer une base organique azotee insoluble dans l'eau, en metal alcalino-terreux dissous et procede pour la production de bicarbonate de metal alcalin
FR2608145A1 (fr)	1988-06-17	Procede de fabrication d'hypochlorite de calcium et produit obtenu par ce procede
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OA20559A (fr)	2022-10-27	Procédé de désextraction de l'uranium contenu dans un solvant.
FR3118063A1 (fr)	2022-06-24	Procédé de désextraction de l’uranium contenu dans un solvant
FR2529232A1 (fr)	1983-12-30	Procede pour la production de chlore et d'une solution aqueuse d'hydroxyde de metal alcalin dans une cellule a membrane a permeabilite selective
CH230066A (fr)	1943-12-15	Procédé de fabrication de l'alumine à partir d'aluminates de chaux bruts.
JPH0623042B2 (ja)	1994-03-30	バナジウムの回収方法