MA56304B1 - Systèmes et procédés pour le traitement de phosphate - Google Patents

Systèmes et procédés pour le traitement de phosphate

Info

Publication number
MA56304B1
MA56304B1 MA56304A MA56304A MA56304B1 MA 56304 B1 MA56304 B1 MA 56304B1 MA 56304 A MA56304 A MA 56304A MA 56304 A MA56304 A MA 56304A MA 56304 B1 MA56304 B1 MA 56304B1
Authority
MA
Morocco
Prior art keywords
subsystems
phosphoric acid
systems
methods
struvite
Prior art date
Application number
MA56304A
Other languages
English (en)
Other versions
MA56304A1 (fr
Inventor
Ahren Britton
Mikaela Verigin
Bryan Baylor
Ram Prasad Melahalli Sathyanarayana
Ryan Deberry
Steven L Pinney
Original Assignee
Ostara Nutrient Recovery Tech Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ostara Nutrient Recovery Tech Inc filed Critical Ostara Nutrient Recovery Tech Inc
Publication of MA56304A1 publication Critical patent/MA56304A1/fr
Publication of MA56304B1 publication Critical patent/MA56304B1/fr

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025—Reverse osmosis; Hyperfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027—Nanofiltration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/22—Preparation by reacting phosphate-containing material with an acid, e.g. wet process
    • C01B25/222—Preparation by reacting phosphate-containing material with an acid, e.g. wet process with sulfuric acid, a mixture of acids mainly consisting of sulfuric acid or a mixture of compounds forming it in situ, e.g. a mixture of sulfur dioxide, water and oxygen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/18—Phosphoric acid
    • C01B25/234—Purification; Stabilisation; Concentration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/28—Ammonium phosphates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/32—Phosphates of magnesium, calcium, strontium, or barium
    • C01B25/322—Preparation by neutralisation of orthophosphoric acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/46—Preparation involving solvent-solvent extraction
    • C01B25/461—Preparation involving solvent-solvent extraction the phosphoric acid present in the medium obtained after reaction being first extracted from the liquid phase formed or separated then re-extracted as free acid by using water or as a phosphate by using a basic compound
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
    • C02F1/004—Processes for the treatment of water whereby the filtration technique is of importance using large scale industrial sized filters
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/442—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by nanofiltration
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/10—Apparatus for the manufacture of superphosphates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B19/00—Granulation or pelletisation of phosphatic fertilisers, other than slag
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/10—Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12—Granules or flakes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/04—Specific process operations in the feed stream; Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/08—Specific process operations in the concentrate stream
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/263—Chemical reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/26—Further operations combined with membrane separation processes
    • B01D2311/2642—Aggregation, sedimentation, flocculation, precipitation or coagulation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/105—Phosphorus compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/12—Halogens or halogen-containing compounds
    • C02F2101/14—Fluorine or fluorine-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/10—Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00—Technologies for wastewater treatment
    • Y02W10/30—Wastewater or sewage treatment systems using renewable energies
    • Y02W10/37—Wastewater or sewage treatment systems using renewable energies using solar energy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Nanotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Pest Control & Pesticides (AREA)
  • Analytical Chemistry (AREA)
  • Fertilizers (AREA)
  • Treatment Of Sludge (AREA)
  • Removal Of Specific Substances (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)

Abstract

Des modes de réalisation de la présente invention concernent des systèmes et des procédés pour un système de traitement de phosphate avec des sous-systèmes intégrés, tel qu'une installation d'acide phosphorique, un système de précipitation, un système de cristalliseur, un système de rinçage, un système de granulation, un système d'eau de bassin, un système d'élimination de matières organiques et/ou un système de traitement d'échappement. De tels sous-systèmes peuvent être intégrés les uns aux autres en utilisant un ou plusieurs flux de sortie provenant d'un ou de plusieurs sous-systèmes comme un ou plusieurs flux d'entrée pour un ou plusieurs sous-systèmes. Dans certains modes de réalisation, le système de traitement de phosphate peut produire de l'acide phosphorique, de la struvite contenant de l'engrais, de l'engrais à l'aide de struvite recyclée, du magnésium ou du fluorure contenant des compositions à l'aide de magnésium ou de fluorure recyclé, et d'autres composants à l'aide d'acide phosphorique recueilli à partir d'une composition d'acide phosphorique et de gypse ou à l'aide de boues recueillies à partir d'un flux de déchets, par exemple.
MA56304A 2019-10-17 2020-10-16 Systèmes et procédés pour le traitement de phosphate MA56304B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201962916584P 2019-10-17 2019-10-17
PCT/CA2020/051395 WO2021072551A1 (fr) 2019-10-17 2020-10-16 Systèmes et procédés pour le traitement de phosphate

Publications (2)

Publication Number Publication Date
MA56304A1 MA56304A1 (fr) 2022-10-31
MA56304B1 true MA56304B1 (fr) 2023-02-28

Family

ID=75537445

Family Applications (1)

Application Number Title Priority Date Filing Date
MA56304A MA56304B1 (fr) 2019-10-17 2020-10-16 Systèmes et procédés pour le traitement de phosphate

Country Status (9)

Country Link
US (1) US20240116830A1 (fr)
CN (1) CN114728792B (fr)
AU (1) AU2020366291A1 (fr)
BR (1) BR112022007352A2 (fr)
FI (1) FI131441B1 (fr)
IL (1) IL292196B2 (fr)
MA (1) MA56304B1 (fr)
MX (1) MX2022004649A (fr)
WO (1) WO2021072551A1 (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12302926B2 (en) 2021-01-28 2025-05-20 Digested Organics Llc Method to produce high protein residuals
US12312266B1 (en) 2021-07-06 2025-05-27 Brown And Caldwell System and method for wastewater treatment
CA3153419A1 (fr) * 2022-03-25 2023-09-25 Saudi Arabian Mining Company (Ma'aden) Procede integre de valorisation de phosphate calcaire maigre presentant de faibles emissions de co2 et peu de dechets de phosphogypse
PL443060A1 (pl) * 2022-12-06 2024-06-10 Politechnika Wrocławska Sposób wytwarzania nawozu fosforowego na bazie struwitu

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB954423A (en) * 1959-06-24 1964-04-08 Fisons Ltd Fertilizers
GB1092055A (en) * 1964-03-06 1967-11-22 Roman Chelminski Process for the production of phosphoric acid
US4154593A (en) * 1976-08-27 1979-05-15 Mississippi Chemical Corporation Process for granulating ammonium phosphate containing fertilizers
US4393032A (en) * 1982-01-12 1983-07-12 Pennzoil Company Production of phosphoric acid and additional products from phosphate ore
US4485077A (en) * 1983-08-12 1984-11-27 The Badger Company, Inc. Method for conducting wet grinding of phosphate rock in a phosphoric acid production plant
US4613494A (en) * 1985-01-08 1986-09-23 James C. Barber And Associates, Inc. Recovery of fluorine from waste gases
NL8700913A (nl) * 1987-04-16 1988-11-16 Nl Stikstof Werkwijze voor het vervaardigen van kunstmestgranules.
US5180569A (en) * 1990-12-31 1993-01-19 Phosphate Engineering And Construction Company Process for the production of phosphoric acid and hydrogen fluoride from phosphate rock and fluosilicic acid
US20030110821A1 (en) * 2001-10-11 2003-06-19 Peacock Lawrence Alan Process for manufacturing fertilizer
BR112014006571B1 (pt) * 2011-09-21 2020-09-29 Ostara Nutrient Recovery Technologies Inc Método para o tratamento de águas residuais contendo fosfato
PL235904B1 (pl) * 2013-03-06 2020-11-16 Grupa Azoty Zakl Azotowe Pulawy Spolka Akcyjna Sposób ciągłego wytwarzania granulowanego nawozu azotowo- fosforowego typu USP
AU2014225473A1 (en) * 2013-03-08 2015-10-01 The Mosaic Company Production of phosphoric acid by a two-stage crystallization process
SE537780C3 (fr) * 2013-05-02 2015-12-08
LT3008034T (lt) * 2013-06-14 2020-06-25 Ostara Nutrient Recovery Technologies Inc. Lėto ir greito atpalaidavimo trąšų kompozicija ir jos gamybos būdas
EP2904892A1 (fr) * 2014-02-11 2015-08-12 Morten Toft Procédé et système pour extraire au moins une partie de la teneur en phosphore et/ou azote de boue et utilisation d'un système de distribution de suspension épaisse mobile sous la forme d'un récipient de cristallisation
CN104401951B (zh) * 2014-11-27 2017-11-03 贵州开磷集团矿肥有限责任公司 一种用高镁磷矿石生产的氮磷镁复合肥及其生产方法
RU2626947C1 (ru) * 2016-03-03 2017-08-02 Акционерное общество "Минерально-химическая компания "ЕвроХим" Фосфоркалийазотсодержащее npk-удобрение и способ получения гранулированного фосфоркалийазотсодержащего npk-удобрения
RU2634936C2 (ru) * 2016-04-04 2017-11-08 Акционерное общество "Минерально-химическая компания "ЕвроХим" Способ получения комплексных минеральных удобрений из фосфатной руды и установка для его реализации
CN106564926B (zh) * 2016-10-24 2018-12-04 湖北三宁化工股份有限公司 一种盐酸分解磷尾矿制备硫酸钙和高镁复合肥的方法
CN109052353B (zh) * 2018-08-30 2020-09-01 中国科学院过程工程研究所 一种由磷矿制备磷酸和硅钙钾镁肥的系统及方法

Also Published As

Publication number Publication date
WO2021072551A1 (fr) 2021-04-22
FI131441B1 (en) 2025-04-22
FI20225389A1 (en) 2022-05-05
IL292196A (en) 2022-06-01
IL292196B2 (en) 2026-02-01
CN114728792B (zh) 2025-09-12
MA56304A1 (fr) 2022-10-31
AU2020366291A1 (en) 2022-06-02
MX2022004649A (es) 2022-10-03
IL292196B1 (en) 2025-10-01
CN114728792A (zh) 2022-07-08
BR112022007352A2 (pt) 2022-07-05
US20240116830A1 (en) 2024-04-11

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