MX2017010418A - Metodo para preparacion continua de cristales de metionina de alta densidad aparente. - Google Patents
Metodo para preparacion continua de cristales de metionina de alta densidad aparente.Info
- Publication number
- MX2017010418A MX2017010418A MX2017010418A MX2017010418A MX2017010418A MX 2017010418 A MX2017010418 A MX 2017010418A MX 2017010418 A MX2017010418 A MX 2017010418A MX 2017010418 A MX2017010418 A MX 2017010418A MX 2017010418 A MX2017010418 A MX 2017010418A
- Authority
- MX
- Mexico
- Prior art keywords
- crystals
- region
- neutralization
- elutriation
- external circulation
- Prior art date
Links
- 239000013078 crystal Substances 0.000 title abstract 9
- 238000000034 method Methods 0.000 title abstract 4
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 title abstract 3
- 229930182817 methionine Natural products 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000000463 material Substances 0.000 abstract 4
- 238000006386 neutralization reaction Methods 0.000 abstract 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- 238000002425 crystallisation Methods 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 2
- SBKRXUMXMKBCLD-UHFFFAOYSA-N 5-(2-methylsulfanylethyl)imidazolidine-2,4-dione Chemical compound CSCCC1NC(=O)NC1=O SBKRXUMXMKBCLD-UHFFFAOYSA-N 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000008021 deposition Effects 0.000 abstract 1
- 229910000027 potassium carbonate Inorganic materials 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
- C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/57—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups
- C07C323/58—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being further substituted by nitrogen atoms, not being part of nitro or nitroso groups with amino groups bound to the carbon skeleton
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0018—Evaporation of components of the mixture to be separated
- B01D9/0027—Evaporation of components of the mixture to be separated by means of conveying fluid, e.g. spray-crystallisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
- B01D9/0054—Use of anti-solvent
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
- C07C319/28—Separation; Purification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente descripción se refiere a un método para preparación continua de cristales de metionina de alta densidad aparente; el procedimiento del método es el siguiente: una solución de hidrolizado, que se obtiene de una reacción de 5- (ß-metilmercaptoetil) hidantoina y una solución de carbonato de potasio, se mezcla con un material de circulación externa de un cristalizador de neutralización de DTB que tiene una sección de neutralización de fase gaseosa; después de enfriarse, la mezcla entra a un distribuidor de líquido de una región de neutralización en la parte superior del cristalizador y se rocía en la forma de gotas o chorro de líquido en gas de dióxido de carbono para reacción de neutralización; y luego cae naturalmente en una región de cristalización en la parte inferior que se va a mezclar con un material en la región; la mezcla obtenida crece en cristales finos en una sistema para formar cristales que tienen diámetros de partículas más grandes, y mientras tanto nuevos núcleos de cristal se forman; en un área de deposición en la parte media de la región de cristalización, los cristales que tienen diámetros de partículas más grandes se depositan en una extremidad de elutriación, mientras los cristales finos circulan con el material de circulación externa, y una parte del material de circulación externa se utiliza para elutriar los cristales en la extremidad de elutriación, mientras otra parte de los mismos se utiliza para mezclarse con la solución de hidrolizado; y los cristales en la extremidad de elutriación se separan, lavan y secan para obtener el producto de metionina de alta densidad aparente.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510078388.1A CN104744326B (zh) | 2015-02-12 | 2015-02-12 | 一种连续制备高堆积密度甲硫氨酸结晶的方法 |
| PCT/CN2015/098368 WO2016127707A1 (zh) | 2015-02-12 | 2015-12-23 | 一种连续制备高堆积密度甲硫氨酸结晶的方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2017010418A true MX2017010418A (es) | 2018-06-07 |
| MX372561B MX372561B (es) | 2020-03-23 |
Family
ID=53584679
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2017010418A MX372561B (es) | 2015-02-12 | 2015-12-23 | Metodo para preparacion continua de cristales de metionina de alta densidad aparente. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US10293273B2 (es) |
| EP (1) | EP3246310B1 (es) |
| JP (1) | JP6423109B2 (es) |
| KR (1) | KR101975189B1 (es) |
| CN (1) | CN104744326B (es) |
| AU (1) | AU2015382630B2 (es) |
| BR (1) | BR112017017246B1 (es) |
| CA (1) | CA2974447A1 (es) |
| MX (1) | MX372561B (es) |
| MY (1) | MY183295A (es) |
| RU (1) | RU2678585C2 (es) |
| SG (1) | SG11201705530VA (es) |
| WO (1) | WO2016127707A1 (es) |
| ZA (1) | ZA201705902B (es) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104744326B (zh) * | 2015-02-12 | 2016-08-10 | 山东新和成氨基酸有限公司 | 一种连续制备高堆积密度甲硫氨酸结晶的方法 |
| CN106008297B (zh) * | 2016-06-03 | 2018-11-30 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸新晶型ⅱ及其制备方法 |
| CN106083675B (zh) * | 2016-06-03 | 2018-07-27 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸新晶型i及其制备方法 |
| KR20180078621A (ko) * | 2016-12-30 | 2018-07-10 | 씨제이제일제당 (주) | 결정화 기술을 이용한 l-메티오닌 결정의 제조방법 |
| CN108794363A (zh) * | 2017-05-02 | 2018-11-13 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸结晶方法 |
| WO2018212149A1 (ja) * | 2017-05-16 | 2018-11-22 | 住友化学株式会社 | メチオニンの気流搬送方法 |
| CN109384696A (zh) * | 2017-08-03 | 2019-02-26 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种获得高纯度高堆积密度蛋氨酸的方法 |
| JP6983256B2 (ja) * | 2017-12-27 | 2021-12-17 | 住友化学株式会社 | 精製メチオニンの製造方法 |
| CN108939603B (zh) * | 2018-09-06 | 2021-06-18 | 四川金象赛瑞化工股份有限公司 | 一种分离硫酸钠和硫酸铵过程中直接冷却结晶的方法 |
| CN109173329B (zh) * | 2018-10-31 | 2023-08-29 | 浙江新和成股份有限公司 | 用于蒸发结晶的装置 |
| US12195422B2 (en) * | 2019-06-18 | 2025-01-14 | Evonik Operations Gmbh | Process for the preparation of D,L-methionine |
| JP7490500B2 (ja) * | 2019-09-12 | 2024-05-27 | 住友化学株式会社 | ポリビニルアルコール除去装置及び偏光子の製造方法 |
| CN111389044A (zh) * | 2020-04-16 | 2020-07-10 | 天津天大清能环境工程有限公司 | 一种防结垢蒸发结晶系统及方法 |
| CN116348446A (zh) * | 2020-10-13 | 2023-06-27 | 赢创运营有限公司 | 具有优化粒径分布的d,l-甲硫氨酸 |
| CN114426298B (zh) * | 2020-10-29 | 2023-08-01 | 中国石油化工股份有限公司 | 碳化法制备氢氧化铝的系统及其碳化反应器 |
| CN113289372A (zh) * | 2021-06-23 | 2021-08-24 | 江苏派克斯特纤维素有限公司 | 非食用盐加工用蒸发结晶装置 |
| CN113663355B (zh) * | 2021-08-16 | 2025-08-12 | 华电水务科技股份有限公司 | 一种应用晶体增大装置的结晶系统 |
| CN115043763B (zh) * | 2022-06-14 | 2024-04-05 | 天津大学 | 一种dl-蛋氨酸的气液连续结晶方法 |
| CN115715890A (zh) * | 2022-11-07 | 2023-02-28 | 福州法莫优科机械科技有限公司 | 一种植物精油结晶脱色的控温设备 |
| CN116199593A (zh) * | 2023-01-05 | 2023-06-02 | 浙江天瑞化学有限公司 | 一种dl-丙氨酸的结晶方法 |
| FR3162219B1 (fr) | 2024-05-17 | 2026-04-17 | Adisseo France Sas | Procédé d’obtention d’un acide aminé sous forme cristallisée à partir d’un sel dudit acide aminé en solution aqueuse |
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| CA866570A (en) | 1968-07-19 | 1971-03-23 | Werner Hans-Helmut | Recovery of minerals from saturated solutions by crystallization |
| JPS5818122B2 (ja) * | 1975-05-23 | 1983-04-11 | 日石三菱株式会社 | シヨウセキハンノウソウチ |
| SU1428406A1 (ru) * | 1986-10-08 | 1988-10-07 | Предприятие П/Я Р-6273 | Способ регулировани процесса кристаллизации в циркул ционном кристаллизаторе |
| JP2921097B2 (ja) * | 1990-10-30 | 1999-07-19 | 住友化学工業株式会社 | メチオニンの製造方法 |
| FR2708267B1 (fr) | 1993-07-28 | 1995-09-01 | Rhone Poulenc Nutrition Animal | Méthode de cristallisation de la méthionine. |
| DE19547236A1 (de) * | 1995-12-18 | 1997-07-03 | Degussa | Verfahren zur Herstellung von D,L-Methionin oder dessen Salz |
| EP0839804B1 (en) * | 1996-10-31 | 2002-01-09 | Sumitomo Chemical Company, Limited | Process for producing methionine |
| JP4482973B2 (ja) * | 1998-09-11 | 2010-06-16 | 住友化学株式会社 | メチオニンの製造方法 |
| CN1178909C (zh) * | 1999-05-21 | 2004-12-08 | 住友化学工业株式会社 | 蛋氨酸的制备方法 |
| JP4338524B2 (ja) * | 2001-11-29 | 2009-10-07 | 日本曹達株式会社 | メチオニンの製造方法 |
| DE10160358A1 (de) | 2001-12-08 | 2003-06-18 | Degussa | Verfahren zur Herstellung von Methionin |
| AU2004320909B2 (en) * | 2004-08-24 | 2010-09-09 | Asahi Glass Company, Limited | Method for producing alkali metal hydrogencarbonate |
| JP2008297251A (ja) * | 2007-05-31 | 2008-12-11 | Mitsui Chemicals Inc | ビスフェノール類の晶析方法 |
| JP2009292795A (ja) * | 2008-06-09 | 2009-12-17 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
| JP2009292796A (ja) * | 2008-06-09 | 2009-12-17 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
| DE102008029050A1 (de) * | 2008-06-18 | 2009-12-24 | Gea Messo Gmbh | Verfahren und Vorrichtung zur kontinuierlichen Herstellung eines Kristallisats mit konstanter Korngrößenverteilung |
| JP2010111640A (ja) * | 2008-11-07 | 2010-05-20 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
| KR101543199B1 (ko) * | 2010-12-29 | 2015-08-10 | 씨제이제일제당 (주) | Ｌ-메티오닌 및 관련 산물의 생산방법 |
| EP2641898A1 (de) | 2012-03-20 | 2013-09-25 | Evonik Industries AG | Verfahren zur Herstellung von Methionin |
| CN102897795B (zh) * | 2012-11-12 | 2015-02-25 | 中国石油化工股份有限公司 | 一种大颗粒硫酸铵晶体的生产方法 |
| CN202983275U (zh) | 2012-11-22 | 2013-06-12 | 中节能六合天融环保科技有限公司 | 一种具有dtb特性的真空结晶器 |
| CN104174181A (zh) | 2014-05-14 | 2014-12-03 | 重庆紫光化工股份有限公司 | 一种有机合成料液的分离纯化系统及分离纯化方法 |
| CN104744326B (zh) * | 2015-02-12 | 2016-08-10 | 山东新和成氨基酸有限公司 | 一种连续制备高堆积密度甲硫氨酸结晶的方法 |
-
2015
- 2015-02-12 CN CN201510078388.1A patent/CN104744326B/zh active Active
- 2015-12-23 AU AU2015382630A patent/AU2015382630B2/en active Active
- 2015-12-23 BR BR112017017246-1A patent/BR112017017246B1/pt active IP Right Grant
- 2015-12-23 MX MX2017010418A patent/MX372561B/es active IP Right Grant
- 2015-12-23 EP EP15881855.9A patent/EP3246310B1/en not_active Not-in-force
- 2015-12-23 CA CA2974447A patent/CA2974447A1/en not_active Abandoned
- 2015-12-23 KR KR1020177022736A patent/KR101975189B1/ko active Active
- 2015-12-23 JP JP2017552207A patent/JP6423109B2/ja active Active
- 2015-12-23 WO PCT/CN2015/098368 patent/WO2016127707A1/zh not_active Ceased
- 2015-12-23 MY MYPI2017001156A patent/MY183295A/en unknown
- 2015-12-23 US US15/549,833 patent/US10293273B2/en active Active
- 2015-12-23 RU RU2017121649A patent/RU2678585C2/ru active
- 2015-12-23 SG SG11201705530VA patent/SG11201705530VA/en unknown
-
2017
- 2017-08-30 ZA ZA2017/05902A patent/ZA201705902B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| MY183295A (en) | 2021-02-18 |
| AU2015382630B2 (en) | 2018-05-17 |
| US20180043281A1 (en) | 2018-02-15 |
| BR112017017246A2 (pt) | 2018-04-17 |
| US10293273B2 (en) | 2019-05-21 |
| KR20170106400A (ko) | 2017-09-20 |
| CN104744326A (zh) | 2015-07-01 |
| RU2017121649A3 (es) | 2018-12-21 |
| KR101975189B1 (ko) | 2019-05-07 |
| ZA201705902B (en) | 2018-12-19 |
| JP6423109B2 (ja) | 2018-11-14 |
| EP3246310A1 (en) | 2017-11-22 |
| AU2015382630A1 (en) | 2017-08-24 |
| CN104744326B (zh) | 2016-08-10 |
| JP2018504453A (ja) | 2018-02-15 |
| EP3246310A4 (en) | 2018-01-10 |
| EP3246310B1 (en) | 2019-08-07 |
| WO2016127707A1 (zh) | 2016-08-18 |
| BR112017017246B1 (pt) | 2021-06-01 |
| CA2974447A1 (en) | 2016-08-18 |
| RU2017121649A (ru) | 2018-12-21 |
| RU2678585C2 (ru) | 2019-01-30 |
| MX372561B (es) | 2020-03-23 |
| SG11201705530VA (en) | 2017-08-30 |
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