NL194264C - Werkwijze voor het winnen van houdbare kamille-extracten, die rijk zijn aan actieve stof. - Google Patents

Werkwijze voor het winnen van houdbare kamille-extracten, die rijk zijn aan actieve stof. Download PDF

Info

Publication number: NL194264C
Authority: NL; Netherlands
Prior art keywords: chamomile; fresh; content; extract; extraction
Prior art date: 1984-09-19

Application number

NL8502554A

Other languages

English (en)

Dutch (nl)

Other versions

NL8502554A (nl

NL194264B (nl

Original Assignee

Asta Medica Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-09-19

Filing date

1985-09-18

Publication date

2001-11-05

1985-09-18 Application filed by Asta Medica Ag filed Critical Asta Medica Ag

1986-04-16 Publication of NL8502554A publication Critical patent/NL8502554A/nl

2001-07-02 Publication of NL194264B publication Critical patent/NL194264B/xx

2001-11-05 Application granted granted Critical

2001-11-05 Publication of NL194264C publication Critical patent/NL194264C/nl

Links

239000013543 active substance Substances 0.000 title claims description 25
238000000034 method Methods 0.000 title claims description 24
235000020221 chamomile extract Nutrition 0.000 title claims description 11
238000000605 extraction Methods 0.000 claims abstract description 28
238000010438 heat treatment Methods 0.000 claims abstract description 6
235000007232 Matricaria chamomilla Nutrition 0.000 claims description 60
235000007866 Chamaemelum nobile Nutrition 0.000 claims description 59
229940070641 chamomile flowers Drugs 0.000 claims description 30
240000003538 Chamaemelum nobile Species 0.000 claims 1
239000000284 extract Substances 0.000 abstract description 44
244000042664 Matricaria chamomilla Species 0.000 description 59
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 47
CUFNKYGDVFVPHO-UHFFFAOYSA-N azulene Chemical compound C1=CC=CC2=CC=CC2=C1 CUFNKYGDVFVPHO-UHFFFAOYSA-N 0.000 description 30
239000000341 volatile oil Substances 0.000 description 21
RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 description 19
XADJWCRESPGUTB-UHFFFAOYSA-N apigenin Natural products C1=CC(O)=CC=C1C1=CC(=O)C2=CC(O)=C(O)C=C2O1 XADJWCRESPGUTB-UHFFFAOYSA-N 0.000 description 18
235000008714 apigenin Nutrition 0.000 description 18
229940117893 apigenin Drugs 0.000 description 18
RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 description 17
238000001035 drying Methods 0.000 description 16
229940036350 bisabolol Drugs 0.000 description 15
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 description 12
KZNIFHPLKGYRTM-UHFFFAOYSA-N apigenin Chemical compound C1=CC(O)=CC=C1C1=CC(=O)C2=C(O)C=C(O)C=C2O1 KZNIFHPLKGYRTM-UHFFFAOYSA-N 0.000 description 12
HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 description 12
239000000126 substance Substances 0.000 description 12
GXGJIOMUZAGVEH-UHFFFAOYSA-N Chamazulene Chemical compound CCC1=CC=C(C)C2=CC=C(C)C2=C1 GXGJIOMUZAGVEH-UHFFFAOYSA-N 0.000 description 10
PMRJYBALQVLLSJ-UHFFFAOYSA-N chamazulene Natural products CCC1=CC2=C(C)CCC2=CC=C1 PMRJYBALQVLLSJ-UHFFFAOYSA-N 0.000 description 10
-1 saturated aliphatic alcohols Chemical class 0.000 description 8
241000196324 Embryophyta Species 0.000 description 7
229930182478 glucoside Natural products 0.000 description 6
239000000463 material Substances 0.000 description 6
WJHRAVIQWFQMKF-IPYPFGDCSA-N Bisabolol oxide A Chemical compound C1CC(C)=CC[C@H]1[C@@]1(C)OC(C)(C)[C@@H](O)CC1 WJHRAVIQWFQMKF-IPYPFGDCSA-N 0.000 description 5
230000000052 comparative effect Effects 0.000 description 5
239000007788 liquid Substances 0.000 description 5
238000003860 storage Methods 0.000 description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
SYTRJRUSWMMZLV-UHFFFAOYSA-N 4-epimatricin Natural products C1=CC(O)(C)C2C1=C(C)CC(OC(C)=O)C1C2OC(=O)C1C SYTRJRUSWMMZLV-UHFFFAOYSA-N 0.000 description 3
WJHRAVIQWFQMKF-UHFFFAOYSA-N Bisabolol oxide A Natural products C1CC(C)=CCC1C1(C)OC(C)(C)C(O)CC1 WJHRAVIQWFQMKF-UHFFFAOYSA-N 0.000 description 3
SYTRJRUSWMMZLV-VQGWEXQJSA-N Matricin Chemical compound [C@@H]1([C@H](CC(C)=C2[C@@H]3[C@](C=C2)(C)O)OC(C)=O)[C@@H]3OC(=O)[C@H]1C SYTRJRUSWMMZLV-VQGWEXQJSA-N 0.000 description 3
SYTRJRUSWMMZLV-AHWDLOTJSA-N Matricin Natural products O=C(O[C@@H]1[C@H]2[C@H](C)C(=O)O[C@@H]2[C@H]2[C@](O)(C)C=CC2=C(C)C1)C SYTRJRUSWMMZLV-AHWDLOTJSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
150000001298 alcohols Chemical class 0.000 description 3
230000007423 decrease Effects 0.000 description 3
230000002255 enzymatic effect Effects 0.000 description 3
238000007710 freezing Methods 0.000 description 3
230000008014 freezing Effects 0.000 description 3
238000002803 maceration Methods 0.000 description 3
239000001500 (2R)-6-methyl-2-[(1R)-4-methyl-1-cyclohex-3-enyl]hept-5-en-2-ol Substances 0.000 description 2
229930189957 Bisabolol oxide Natural products 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
102000004190 Enzymes Human genes 0.000 description 2
108090000790 Enzymes Proteins 0.000 description 2
XLYOFNOQVPJJNP-ZSJDYOACSA-N Heavy water Chemical compound [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 2
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
239000004480 active ingredient Substances 0.000 description 2
229930003944 flavone Natural products 0.000 description 2
150000002213 flavones Chemical class 0.000 description 2
235000011949 flavones Nutrition 0.000 description 2
239000007789 gas Substances 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
229910052757 nitrogen Inorganic materials 0.000 description 2
238000005325 percolation Methods 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
YTAQZPGBTPDBPW-UHFFFAOYSA-N 2-phenylchromene-3,4-dione Chemical compound O1C2=CC=CC=C2C(=O)C(=O)C1C1=CC=CC=C1 YTAQZPGBTPDBPW-UHFFFAOYSA-N 0.000 description 1
238000009835 boiling Methods 0.000 description 1
125000004432 carbon atom Chemical group C* 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
229940119217 chamomile extract Drugs 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
239000002274 desiccant Substances 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000000796 flavoring agent Substances 0.000 description 1
235000019634 flavors Nutrition 0.000 description 1
229930182470 glycoside Natural products 0.000 description 1
150000002338 glycosides Chemical class 0.000 description 1
230000002779 inactivation Effects 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000000203 mixture Substances 0.000 description 1
239000002243 precursor Substances 0.000 description 1

Classifications

- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea

Landscapes

Health & Medical Sciences (AREA)
Natural Medicines & Medicinal Plants (AREA)
Life Sciences & Earth Sciences (AREA)
Animal Behavior & Ethology (AREA)
Public Health (AREA)
Alternative & Traditional Medicine (AREA)
Biotechnology (AREA)
Botany (AREA)
Medical Informatics (AREA)
Medicinal Chemistry (AREA)
Microbiology (AREA)
Mycology (AREA)
Pharmacology & Pharmacy (AREA)
Epidemiology (AREA)
Chemical & Material Sciences (AREA)
General Health & Medical Sciences (AREA)
Engineering & Computer Science (AREA)
Veterinary Medicine (AREA)
Medicines Containing Plant Substances (AREA)
Cosmetics (AREA)
Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Agricultural Chemicals And Associated Chemicals (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Fats And Perfumes (AREA)
Compounds Of Unknown Constitution (AREA)
Preparation Of Fruits And Vegetables (AREA)
Gears, Cams (AREA)
Breeding Of Plants And Reproduction By Means Of Culturing (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Coloring Foods And Improving Nutritive Qualities (AREA)
External Artificial Organs (AREA)
Saccharide Compounds (AREA)
Valve-Gear Or Valve Arrangements (AREA)
Catalysts (AREA)
Preliminary Treatment Of Fibers (AREA)
Mechanical Operated Clutches (AREA)
Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Materials For Medical Uses (AREA)
Anti-Oxidant Or Stabilizer Compositions (AREA)
Other Investigation Or Analysis Of Materials By Electrical Means (AREA)

NL8502554A 1984-09-19 1985-09-18 Werkwijze voor het winnen van houdbare kamille-extracten, die rijk zijn aan actieve stof. NL194264C (nl)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE3434342		1984-09-19
DE3434342		1984-09-19

Publications (3)

Publication Number	Publication Date
NL8502554A NL8502554A (nl)	1986-04-16
NL194264B NL194264B (nl)	2001-07-02
NL194264C true NL194264C (nl)	2001-11-05

Family

ID=6245768

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8502554A NL194264C (nl)	1984-09-19	1985-09-18	Werkwijze voor het winnen van houdbare kamille-extracten, die rijk zijn aan actieve stof.

Country Status (31)

Country	Link
US (1)	US4786497A (cs)
EP (1)	EP0175185B1 (cs)
JP (1)	JPH0641414B2 (cs)
KR (1)	KR900000544B1 (cs)
AT (1)	ATE58836T1 (cs)
BR (1)	BR8504573A (cs)
CA (1)	CA1251142A (cs)
CS (1)	CS254346B2 (cs)
DD (1)	DD240496A5 (cs)
DE (2)	DE3530790A1 (cs)
DK (1)	DK161799C (cs)
ES (1)	ES8608881A1 (cs)
FI (1)	FI79469C (cs)
GB (1)	GB2164559B (cs)
GR (1)	GR852243B (cs)
HU (1)	HU193449B (cs)
IE (1)	IE58215B1 (cs)
IL (1)	IL76388A (cs)
IN (1)	IN164169B (cs)
MA (1)	MA20530A1 (cs)
MT (1)	MTP970B (cs)
MX (1)	MX161477A (cs)
MY (1)	MY100507A (cs)
NL (1)	NL194264C (cs)
NO (1)	NO164276C (cs)
PL (1)	PL255422A1 (cs)
PT (1)	PT81148B (cs)
RO (1)	RO93515B (cs)
SU (1)	SU1642947A3 (cs)
YU (1)	YU45989B (cs)
ZA (1)	ZA857166B (cs)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
IN163594B (cs) *	1984-03-16	1988-10-15	Degussa
MX161477A (es) *	1984-09-19	1990-09-28	Degussa	Procedimiento para extraer los constituyentes de la manzanilla
EP0285752B1 (de) *	1987-02-13	1993-10-27	ASTA Medica Aktiengesellschaft	Kamillenöle mit hohem Gehalt an natürlichen Polyinen und Verfahren zu deren Herstellung
US6300370B1 (en)	1987-02-13	2001-10-09	Asta Medica Aktiengesellschaft	Camomile oils having a high content of natural poly-ynes and process for their preparation
DE3913280C2 (de) *	1989-04-22	1995-02-16	Paul Haslauer	Bedampfungsgerät
EP0496230A1 (de) *	1991-01-23	1992-07-29	ASTA Medica Aktiengesellschaft	Herstellung eines Kamillenextraktes mit antimikrobiellen Eigenschaften
JP2513550B2 (ja) *	1991-09-24	1996-07-03	相互印刷工芸株式会社	カミツレ成分の抽出方法
JP2010163363A (ja) *	2009-01-13	2010-07-29	Kao Corp	アピゲニン高濃度含有エキスの製造方法
CN102911791A (zh) *	2012-09-25	2013-02-06	常州亚环环保科技有限公司	一种栀子花精油液的提取方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE609884C (de) *	1932-12-22	1935-02-25	Ig Farbenindustrie Ag	Verfahren zur Darstellung von haltbaren Kamillenauszuegen
GB505983A (en) *	1937-11-17	1939-05-17	Ig Farbenindustrie Ag	Improvements in the manufacture and production of pharmaceutically active substances
FR1015120A (fr) *	1947-08-13	1952-08-27		Procédé de préparation d'extraits actifs renfermant de l'azulène à partir de camomille ou de plantes analogues
DE1093951B (de) *	1959-02-12	1960-12-01	Chemiewerk Homburg Zweignieder	Verfahren zur Extraktion proazulenhaltiger Drogen
DE1296305B (de) *	1965-08-26	1969-05-29	Thomae Gmbh Dr K	Verfahren zur Extraktion von Kamille
DE2227292C3 (de) *	1972-06-05	1981-01-08	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung von Kamillenextrakten
CH572368A5 (cs) *	1973-03-28	1976-02-13	Sulzer Ag
DE2316363A1 (de) *	1973-04-02	1974-10-17	Degussa	Verfahren zur herstellung von kamillenextrakten
DE2402802C3 (de) *	1974-01-22	1979-06-13	Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt	Gewinnung einer Kamillendroge mit hohem Chamazulen- und Bisabololgehalt
IT1157945B (it) *	1982-06-02	1987-02-18	Bonomelli Spa	Composizione terapeutica ad attivita' antibatterica a base di una frazione estratta da fiori di camomilla e processo per la preparazione di detta frazione
DE3423207C3 (de) *	1983-06-29	1996-09-26	Asta Medica Ag	Verfahren zur Herstellung einer neuen Kamillensorte (Bezeichnung Manzana)
IN163594B (cs) *	1984-03-16	1988-10-15	Degussa
MX161477A (es) *	1984-09-19	1990-09-28	Degussa	Procedimiento para extraer los constituyentes de la manzanilla

1985
- 1985-08-16 MX MX206315A patent/MX161477A/es unknown
- 1985-08-29 EP EP85110864A patent/EP0175185B1/de not_active Expired - Lifetime
- 1985-08-29 DE DE19853530790 patent/DE3530790A1/de not_active Ceased
- 1985-08-29 AT AT85110864T patent/ATE58836T1/de not_active IP Right Cessation
- 1985-08-29 DE DE8585110864T patent/DE3580814D1/de not_active Expired - Lifetime
- 1985-09-13 IL IL76388A patent/IL76388A/xx not_active IP Right Cessation
- 1985-09-16 GR GR852243A patent/GR852243B/el unknown
- 1985-09-16 RO RO120125A patent/RO93515B/ro unknown
- 1985-09-17 KR KR1019850006776A patent/KR900000544B1/ko not_active Expired
- 1985-09-17 DD DD85280700A patent/DD240496A5/de not_active IP Right Cessation
- 1985-09-17 FI FI853562A patent/FI79469C/fi not_active IP Right Cessation
- 1985-09-18 NL NL8502554A patent/NL194264C/nl not_active IP Right Cessation
- 1985-09-18 ES ES547081A patent/ES8608881A1/es not_active Expired
- 1985-09-18 MA MA20756A patent/MA20530A1/fr unknown
- 1985-09-18 YU YU147485A patent/YU45989B/sh unknown
- 1985-09-18 CS CS856645A patent/CS254346B2/cs not_active IP Right Cessation
- 1985-09-18 CA CA000491049A patent/CA1251142A/en not_active Expired
- 1985-09-18 PL PL25542285A patent/PL255422A1/xx unknown
- 1985-09-18 ZA ZA857166A patent/ZA857166B/xx unknown
- 1985-09-18 GB GB8523097A patent/GB2164559B/en not_active Expired
- 1985-09-18 SU SU853953190A patent/SU1642947A3/ru active
- 1985-09-18 JP JP60204584A patent/JPH0641414B2/ja not_active Expired - Fee Related
- 1985-09-18 DK DK424185A patent/DK161799C/da not_active IP Right Cessation
- 1985-09-18 PT PT81148A patent/PT81148B/pt unknown
- 1985-09-18 NO NO853660A patent/NO164276C/no not_active IP Right Cessation
- 1985-09-18 MT MT970A patent/MTP970B/xx unknown
- 1985-09-18 IE IE230985A patent/IE58215B1/en not_active IP Right Cessation
- 1985-09-19 HU HU853513A patent/HU193449B/hu unknown
- 1985-09-19 BR BR8504573A patent/BR8504573A/pt unknown
- 1985-12-19 IN IN916/CAL/85A patent/IN164169B/en unknown
1987
- 1987-06-18 MY MYPI87000840A patent/MY100507A/en unknown
- 1987-09-08 US US07/096,211 patent/US4786497A/en not_active Expired - Lifetime

Also Published As

Publication number	Publication date
IE58215B1 (en)	1993-08-11
HUT38258A (en)	1986-05-28
IL76388A (en)	1990-07-12
ES547081A0 (es)	1986-09-01
IE852309L (en)	1986-03-19
DD240496A5 (de)	1986-11-05
MA20530A1 (fr)	1986-04-01
GR852243B (cs)	1986-01-17
JPS6178728A (ja)	1986-04-22
GB8523097D0 (en)	1985-10-23
DE3530790A1 (de)	1986-03-27
MTP970B (en)	1986-07-28
BR8504573A (pt)	1986-07-15
ES8608881A1 (es)	1986-09-01
DK161799C (da)	1992-02-24
KR900000544B1 (ko)	1990-01-31
PT81148A (de)	1985-10-01
NL8502554A (nl)	1986-04-16
CA1251142A (en)	1989-03-14
EP0175185A3 (en)	1987-12-23
GB2164559B (en)	1989-06-21
YU45989B (sh)	1992-12-21
EP0175185A2 (de)	1986-03-26
US4786497A (en)	1988-11-22
GB2164559A (en)	1986-03-26
PT81148B (pt)	1988-01-22
EP0175185B1 (de)	1990-12-05
DK424185D0 (da)	1985-09-18
DK424185A (da)	1986-03-20
ATE58836T1 (de)	1990-12-15
YU147485A (en)	1988-04-30
FI79469C (fi)	1990-01-10
NO853660L (no)	1986-03-20
NO164276C (no)	1990-09-19
DE3580814D1 (de)	1991-01-17
FI853562L (fi)	1986-03-20
ZA857166B (en)	1986-08-27
IN164169B (cs)	1989-01-28
JPH0641414B2 (ja)	1994-06-01
RO93515B (ro)	1988-04-01
NO164276B (no)	1990-06-11
NL194264B (nl)	2001-07-02
KR860002274A (ko)	1986-04-24
HU193449B (en)	1987-10-28
FI79469B (fi)	1989-09-29
RO93515A (ro)	1988-03-30
MX161477A (es)	1990-09-28
DK161799B (da)	1991-08-19
SU1642947A3 (ru)	1991-04-15
MY100507A (en)	1990-10-30
PL255422A1 (en)	1986-08-12
CS254346B2 (en)	1988-01-15
IL76388A0 (en)	1986-01-31
FI853562A0 (fi)	1985-09-17

Legal Events

Date	Code	Title	Description
1992-09-01	BA	A request for search or an international-type search has been filed
1992-11-02	BB	A search report has been drawn up
1992-12-01	BC	A request for examination has been filed
2001-07-02	CNR	Transfer of rights (patent application after its laying open for public inspection)	Free format text: ASTA MEDICA AKTIENGESELLSCHAFT;DEGUSSA-HUELS AKTIENGESELLSCHAFT
2002-12-02	SNR	Assignments of patents or rights arising from examined patent applications	Owner name: VIATRIS GMBH & CO. KG
2005-11-01	V4	Discontinued because of reaching the maximum lifetime of a patent	Effective date: 20050918

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