NL8202305A - Werkwijze ter vervaardiging van koolstofvezels uit petroleumpek. - Google Patents

Werkwijze ter vervaardiging van koolstofvezels uit petroleumpek. Download PDF

Info

Publication number: NL8202305A
Authority: NL; Netherlands
Prior art keywords: fibers; temperature; pitch; treatment; infusible
Prior art date: 1981-06-09

Application number

NL8202305A

Other languages

English (en)

Dutch (nl)

Original Assignee

British Petroleum Co Plc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1981-06-09

Filing date

1982-06-08

Publication date

1983-01-03

1982-06-08 Application filed by British Petroleum Co Plc filed Critical British Petroleum Co Plc

1983-01-03 Publication of NL8202305A publication Critical patent/NL8202305A/nl

Links

238000000034 method Methods 0.000 title claims description 28
229920000049 Carbon (fiber) Polymers 0.000 title claims description 20
239000004917 carbon fiber Substances 0.000 title claims description 20
238000004519 manufacturing process Methods 0.000 title claims description 12
239000003208 petroleum Substances 0.000 title claims description 11
239000000835 fiber Substances 0.000 claims description 123
229920005989 resin Polymers 0.000 claims description 64
239000011347 resin Substances 0.000 claims description 64
238000011282 treatment Methods 0.000 claims description 46
238000009987 spinning Methods 0.000 claims description 16
238000003763 carbonization Methods 0.000 claims description 14
239000000203 mixture Substances 0.000 claims description 12
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 11
238000010438 heat treatment Methods 0.000 claims description 9
229910052760 oxygen Inorganic materials 0.000 claims description 9
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
239000001301 oxygen Substances 0.000 claims description 8
229910052799 carbon Inorganic materials 0.000 claims description 6
238000004230 steam cracking Methods 0.000 claims description 6
229910002804 graphite Inorganic materials 0.000 claims description 5
239000010439 graphite Substances 0.000 claims description 5
229910052736 halogen Inorganic materials 0.000 claims description 3
150000002367 halogens Chemical class 0.000 claims description 3
230000001105 regulatory effect Effects 0.000 claims description 2
239000011295 pitch Substances 0.000 description 67
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 26
229910052757 nitrogen Inorganic materials 0.000 description 13
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
239000007789 gas Substances 0.000 description 11
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 10
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
230000015572 biosynthetic process Effects 0.000 description 8
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 7
239000002994 raw material Substances 0.000 description 7
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
238000007669 thermal treatment Methods 0.000 description 5
MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 4
238000001944 continuous distillation Methods 0.000 description 4
239000007791 liquid phase Substances 0.000 description 4
239000000463 material Substances 0.000 description 4
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
240000007124 Brassica oleracea Species 0.000 description 3
235000003899 Brassica oleracea var acephala Nutrition 0.000 description 3
235000011301 Brassica oleracea var capitata Nutrition 0.000 description 3
235000001169 Brassica oleracea var oleracea Nutrition 0.000 description 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
229910052786 argon Inorganic materials 0.000 description 3
239000003245 coal Substances 0.000 description 3
239000000284 extract Substances 0.000 description 3
238000005087 graphitization Methods 0.000 description 3
239000001257 hydrogen Substances 0.000 description 3
229910052739 hydrogen Inorganic materials 0.000 description 3
239000002904 solvent Substances 0.000 description 3
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
230000032683 aging Effects 0.000 description 2
239000010426 asphalt Substances 0.000 description 2
239000012159 carrier gas Substances 0.000 description 2
229920002678 cellulose Polymers 0.000 description 2
239000001913 cellulose Substances 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
239000000460 chlorine Substances 0.000 description 2
229910052801 chlorine Inorganic materials 0.000 description 2
238000004821 distillation Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000001307 helium Substances 0.000 description 2
229910052734 helium Inorganic materials 0.000 description 2
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
229920002521 macromolecule Polymers 0.000 description 2
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
230000003647 oxidation Effects 0.000 description 2
238000007254 oxidation reaction Methods 0.000 description 2
239000011301 petroleum pitch Substances 0.000 description 2
229920000642 polymer Polymers 0.000 description 2
239000002689 soil Substances 0.000 description 2
239000007858 starting material Substances 0.000 description 2
239000000126 substance Substances 0.000 description 2
239000011593 sulfur Substances 0.000 description 2
229910052717 sulfur Inorganic materials 0.000 description 2
238000012360 testing method Methods 0.000 description 2
KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
239000004698 Polyethylene Substances 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
230000002411 adverse Effects 0.000 description 1
230000003466 anti-cipated effect Effects 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
238000007664 blowing Methods 0.000 description 1
238000010000 carbonizing Methods 0.000 description 1
239000004359 castor oil Substances 0.000 description 1
235000019438 castor oil Nutrition 0.000 description 1
239000011300 coal pitch Substances 0.000 description 1
239000011280 coal tar Substances 0.000 description 1
239000011294 coal tar pitch Substances 0.000 description 1
239000000571 coke Substances 0.000 description 1
239000012141 concentrate Substances 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000010924 continuous production Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000005336 cracking Methods 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
238000007872 degassing Methods 0.000 description 1
230000001627 detrimental effect Effects 0.000 description 1
238000009826 distribution Methods 0.000 description 1
230000008030 elimination Effects 0.000 description 1
238000003379 elimination reaction Methods 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
238000000605 extraction Methods 0.000 description 1
238000001125 extrusion Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
230000004907 flux Effects 0.000 description 1
ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
238000010348 incorporation Methods 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
230000001788 irregular Effects 0.000 description 1
230000009916 joint effect Effects 0.000 description 1
239000007788 liquid Substances 0.000 description 1
239000004973 liquid crystal related substance Substances 0.000 description 1
238000002074 melt spinning Methods 0.000 description 1
238000010309 melting process Methods 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
239000003921 oil Substances 0.000 description 1
239000011368 organic material Substances 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
239000003209 petroleum derivative Substances 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
239000004014 plasticizer Substances 0.000 description 1
229920002239 polyacrylonitrile Polymers 0.000 description 1
238000006068 polycondensation reaction Methods 0.000 description 1
-1 polyethylene Polymers 0.000 description 1
229920000573 polyethylene Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
229920000915 polyvinyl chloride Polymers 0.000 description 1
239000004800 polyvinyl chloride Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
238000012545 processing Methods 0.000 description 1
239000004576 sand Substances 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
230000000153 supplemental effect Effects 0.000 description 1
238000004416 surface enhanced Raman spectroscopy Methods 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000010998 test method Methods 0.000 description 1
238000003878 thermal aging Methods 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
238000005406 washing Methods 0.000 description 1
238000004804 winding Methods 0.000 description 1

Classifications

- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Textile Engineering (AREA)
Inorganic Fibers (AREA)
Working-Up Tar And Pitch (AREA)

NL8202305A 1981-06-09 1982-06-08 Werkwijze ter vervaardiging van koolstofvezels uit petroleumpek. NL8202305A (nl)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
GB8117658		1981-06-09
GB8117658		1981-06-09

Publications (1)

Publication Number	Publication Date
NL8202305A true NL8202305A (nl)	1983-01-03

Family

ID=10522384

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8202305A NL8202305A (nl)	1981-06-09	1982-06-08	Werkwijze ter vervaardiging van koolstofvezels uit petroleumpek.

Country Status (6)

Country	Link
US (1)	US4431623A (fr)
JP (1)	JPS584824A (fr)
BE (1)	BE893464A (fr)
DE (1)	DE3221367A1 (fr)
FR (1)	FR2509331B1 (fr)
NL (1)	NL8202305A (fr)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2532322B1 (fr) *	1982-08-24	1985-08-23	Agency Ind Science Techn	Compositions de brai, procedes de preparation desdites compositions, filament de brai, procede de preparation dudit filament, fibre de carbone a base de brai et procede de preparation de ladite fibre de carbone
JPS59145286A (ja) *	1983-02-08	1984-08-20	Fuji Standard Res Kk	高強度炭素繊維用原料として好適なメソフエ−スピツチ
US4581123A (en) *	1983-03-28	1986-04-08	E. I. Du Pont De Nemours And Company	Custom blended precursor for carbon artifact manufacture
US4574077A (en) *	1983-10-14	1986-03-04	Nippon Oil Company Limited	Process for producing pitch based graphite fibers
JPS6088125A (ja) *	1983-10-14	1985-05-17	Nippon Oil Co Ltd	ピツチ系黒鉛化繊維の製造方法
JPH0627172B2 (ja) *	1985-10-02	1994-04-13	三菱石油株式会社	光学的異方性ピッチの製造方法
JPS62295926A (ja) *	1986-06-16	1987-12-23	Nitto Boseki Co Ltd	炭素繊維チヨツプドストランドの製造方法
JPS63134119A (ja) *	1986-11-25	1988-06-06	Mitsubishi Electric Corp	ワイヤカツト放電加工用電極材料
US4915926A (en) *	1988-02-22	1990-04-10	E. I. Dupont De Nemours And Company	Balanced ultra-high modulus and high tensile strength carbon fibers
US5238672A (en) *	1989-06-20	1993-08-24	Ashland Oil, Inc.	Mesophase pitches, carbon fiber precursors, and carbonized fibers
FR2801297B1 (fr) *	1999-11-19	2002-02-01	Centre Nat Rech Scient	Charbons actifs et leur procede d'obtention a partir d'un brai partiellement mesophase et partiellement mesogene
RU2537306C2 (ru) *	2013-01-14	2014-12-27	Евгений Савельевич Дашут	Способ организации переработки тяжелых углеводородных соединений с получением объемного углеродного каркаса (варианты)

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3595946A (en) *	1968-06-04	1971-07-27	Great Lakes Carbon Corp	Process for the production of carbon filaments from coal tar pitch
JPS4842696B1 (fr) *	1969-02-13	1973-12-14
US3656904A (en) *	1970-06-10	1972-04-18	Celanese Corp	Graphitization process
DE2350769A1 (de) *	1972-10-31	1974-05-09	Union Carbide Corp	Verfahren zur herstellung graphitisierbarer kohlenstoff-fasern
JPS5137967B2 (fr) *	1973-06-02	1976-10-19
FR2250571B1 (fr) *	1973-11-12	1980-01-04	British Petroleum Co
JPS5834568B2 (ja) *	1975-03-10	1983-07-27	旭化成株式会社	炭素繊維の製造方法
FR2392144A1 (fr) *	1977-05-25	1978-12-22	British Petroleum Co	Procede de fabrication de fibres de carbone et de graphite a partir de brais de petrole
US4219404A (en) *	1979-06-14	1980-08-26	Exxon Research & Engineering Co.	Vacuum or steam stripping aromatic oils from petroleum pitch
FR2467177A1 (fr) *	1979-10-09	1981-04-17	British Petroleum Co	Procede de fabrication de charbons actifs a surface specifique elevee a partir de brai de petrole
US4351816A (en) *	1980-12-17	1982-09-28	Union Carbide Corporation	Method for producing a mesophase pitch derived carbon yarn and fiber

1982
- 1982-06-04 US US06/385,080 patent/US4431623A/en not_active Expired - Fee Related
- 1982-06-05 DE DE3221367A patent/DE3221367A1/de not_active Ceased
- 1982-06-08 JP JP57097046A patent/JPS584824A/ja active Pending
- 1982-06-08 NL NL8202305A patent/NL8202305A/nl not_active Application Discontinuation
- 1982-06-08 FR FR8209948A patent/FR2509331B1/fr not_active Expired
- 1982-06-09 BE BE0/208309A patent/BE893464A/fr not_active IP Right Cessation

Also Published As

Publication number	Publication date
DE3221367A1 (de)	1983-01-13
US4431623A (en)	1984-02-14
BE893464A (fr)	1982-12-09
FR2509331A1 (fr)	1983-01-14
FR2509331B1 (fr)	1986-04-18
JPS584824A (ja)	1983-01-12

Legal Events

Date	Code	Title
1985-01-01	A85	Still pending on 85-01-01
1989-08-01	BA	A request for search or an international-type search has been filed
1989-12-01	BB	A search report has been drawn up
1990-05-01	BC	A request for examination has been filed
1994-02-01	BV	The patent application has lapsed

Publication	Publication Date	Title
US4197283A (en)	1980-04-08	Carbon fibres
US4277324A (en)	1981-07-07	Treatment of pitches in carbon artifact manufacture
US4026788A (en)	1977-05-31	Process for producing mesophase pitch
DE3330575C2 (fr)	1987-08-27
NL8202305A (nl)	1983-01-03	Werkwijze ter vervaardiging van koolstofvezels uit petroleumpek.
EP0198471B1 (fr)	1989-11-23	Procédé de purification d'un matériau de départ à utiliser dans la production de produits de charbon
US4277325A (en)	1981-07-07	Treatment of pitches in carbon artifact manufacture
EP0034410A2 (fr)	1981-08-26	Procédé de préparation d'une base pour la fabrication d'objets façonnés en carbone
US4115527A (en)	1978-09-19	Production of carbon fibers having high anisotropy
KR960007714B1 (ko)	1996-06-08	초고 모듈러스와 높은 인장강도가 균형을 이룬 탄소섬유 및 이의 제조방법
US4597853A (en)	1986-07-01	Pitch as a raw material for making carbon fibers and process for producing the same
US4503026A (en)	1985-03-05	Spinnable precursors from petroleum pitch, fibers spun therefrom and method of preparation thereof
US5968435A (en)	1999-10-19	Process for manufacturing pitch-type carbon fiber
JPS58214531A (ja)	1983-12-13	ピツチ系炭素繊維製造用ピツチの調製方法
JPH045710B2 (fr)	1992-02-03
JPS602352B2 (ja)	1985-01-21	プリメソフエ−ス炭素質の製造方法
EP4229117A1 (fr)	2023-08-23	Procédé de contrôle de points de ramollissement de matériaux hydrocarbonés pétroliers
JP3786967B2 (ja)	2006-06-21	炭素繊維製造のための自己安定化性ピッチ
CN1085748C (zh)	2002-05-29	制备溶剂化各向同性沥青、碳制品的方法及溶剂化各向同性沥青和碳纤维
WO2025081265A1 (fr)	2025-04-24	Production de fibres de carbone à partir d'un matériau précurseur à base d'asphaltène
GB2100240A (en)	1982-12-22	Process for the production of carbon fibres from petroleum pitch
JPS59136383A (ja)	1984-08-04	炭素繊維製造用ピツチの調製方法
JPS6183317A (ja)	1986-04-26	炭素繊維の製造方法
JPS62162022A (ja)	1987-07-17	炭素繊維の製造方法
JPH01249887A (ja)	1989-10-05	メソフェースピッチの製造方法