NL8302076A - Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen. - Google Patents

Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen. Download PDF

Info

Publication number: NL8302076A
Authority: NL; Netherlands
Prior art keywords: process according; concentration; added; sample; electrolysis
Prior art date: 1983-06-10

Application number

NL8302076A

Other languages

English (en)

Dutch (nl)

Original Assignee

Tno

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-06-10

Filing date

1983-06-10

Publication date

1985-01-02

1983-06-10 Application filed by Tno filed Critical Tno

1983-06-10 Priority to NL8302076A priority Critical patent/NL8302076A/nl

1984-06-08 Priority to PCT/NL1984/000017 priority patent/WO1984004968A1/en

1984-06-08 Priority to AT84200832T priority patent/ATE30357T1/de

1984-06-08 Priority to DE8484200832T priority patent/DE3466907D1/de

1984-06-08 Priority to US06/706,852 priority patent/US4778570A/en

1984-06-08 Priority to EP84200832A priority patent/EP0128627B1/de

1984-06-08 Priority to JP59502322A priority patent/JPS60501673A/ja

1985-01-02 Publication of NL8302076A publication Critical patent/NL8302076A/nl

Links

238000000034 method Methods 0.000 title claims abstract description 34
229910052736 halogen Inorganic materials 0.000 title claims abstract description 14
150000002367 halogens Chemical class 0.000 title claims abstract description 14
238000005868 electrolysis reaction Methods 0.000 claims abstract description 14
239000000010 aprotic solvent Substances 0.000 claims abstract description 4
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 21
-1 halide ions Chemical class 0.000 claims description 18
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical group CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 15
OAKJQQAXSVQMHS-UHFFFAOYSA-N hydrazine group Chemical group NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 12
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims description 10
229910052753 mercury Inorganic materials 0.000 claims description 9
239000003792 electrolyte Substances 0.000 claims description 8
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 8
239000002904 solvent Substances 0.000 claims description 7
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
150000004820 halides Chemical class 0.000 claims description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 4
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims description 2
FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims description 2
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 2
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
229910021397 glassy carbon Inorganic materials 0.000 claims description 2
229910002804 graphite Inorganic materials 0.000 claims description 2
239000010439 graphite Substances 0.000 claims description 2
239000000463 material Substances 0.000 claims description 2
229910052751 metal Inorganic materials 0.000 claims description 2
239000002184 metal Substances 0.000 claims description 2
229910052725 zinc Inorganic materials 0.000 claims description 2
239000011701 zinc Substances 0.000 claims description 2
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
229910052739 hydrogen Inorganic materials 0.000 claims 1
239000001257 hydrogen Substances 0.000 claims 1
229910052709 silver Inorganic materials 0.000 claims 1
239000004332 silver Substances 0.000 claims 1
239000000126 substance Substances 0.000 abstract description 12
238000004458 analytical method Methods 0.000 abstract description 8
150000002896 organic halogen compounds Chemical class 0.000 description 8
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 5
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
229910052799 carbon Inorganic materials 0.000 description 4
150000004045 organic chlorine compounds Chemical class 0.000 description 4
IZUPBVBPLAPZRR-UHFFFAOYSA-N pentachlorophenol Chemical compound OC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl IZUPBVBPLAPZRR-UHFFFAOYSA-N 0.000 description 4
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
229910052794 bromium Inorganic materials 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 3
239000007772 electrode material Substances 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
239000012528 membrane Substances 0.000 description 3
VADKRMSMGWJZCF-UHFFFAOYSA-N 2-bromophenol Chemical compound OC1=CC=CC=C1Br VADKRMSMGWJZCF-UHFFFAOYSA-N 0.000 description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
238000013019 agitation Methods 0.000 description 2
239000002894 chemical waste Substances 0.000 description 2
229910052801 chlorine Inorganic materials 0.000 description 2
239000000460 chlorine Substances 0.000 description 2
238000000605 extraction Methods 0.000 description 2
238000005192 partition Methods 0.000 description 2
229910052697 platinum Inorganic materials 0.000 description 2
238000003918 potentiometric titration Methods 0.000 description 2
239000001294 propane Substances 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
238000001179 sorption measurement Methods 0.000 description 2
FHCLGDLYRUPKAM-UHFFFAOYSA-N 1,2,3-tribromopropane Chemical compound BrCC(Br)CBr FHCLGDLYRUPKAM-UHFFFAOYSA-N 0.000 description 1
WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
VFWCMGCRMGJXDK-UHFFFAOYSA-N 1-chlorobutane Chemical compound CCCCCl VFWCMGCRMGJXDK-UHFFFAOYSA-N 0.000 description 1
PTTPXKJBFFKCEK-UHFFFAOYSA-N 2-Methyl-4-heptanone Chemical compound CC(C)CC(=O)CC(C)C PTTPXKJBFFKCEK-UHFFFAOYSA-N 0.000 description 1
SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 1
AVPYQKSLYISFPO-UHFFFAOYSA-N 4-chlorobenzaldehyde Chemical compound ClC1=CC=C(C=O)C=C1 AVPYQKSLYISFPO-UHFFFAOYSA-N 0.000 description 1
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 1
UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
229910021607 Silver chloride Inorganic materials 0.000 description 1
230000002411 adverse Effects 0.000 description 1
235000019270 ammonium chloride Nutrition 0.000 description 1
238000003556 assay Methods 0.000 description 1
JMWSLIGNGRZDIH-UHFFFAOYSA-N benzene-1,4-diol;2-bromophenol Chemical compound OC1=CC=C(O)C=C1.OC1=CC=CC=C1Br JMWSLIGNGRZDIH-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 description 1
229940106681 chloroacetic acid Drugs 0.000 description 1
MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 1
238000003776 cleavage reaction Methods 0.000 description 1
238000002485 combustion reaction Methods 0.000 description 1
230000006378 damage Effects 0.000 description 1
238000009792 diffusion process Methods 0.000 description 1
239000000428 dust Substances 0.000 description 1
150000003977 halocarboxylic acids Chemical class 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
229910052740 iodine Inorganic materials 0.000 description 1
239000011630 iodine Substances 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
239000007788 liquid Substances 0.000 description 1
238000003760 magnetic stirring Methods 0.000 description 1
150000002730 mercury Chemical class 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
UNFUYWDGSFDHCW-UHFFFAOYSA-N monochlorocyclohexane Chemical compound ClC1CCCCC1 UNFUYWDGSFDHCW-UHFFFAOYSA-N 0.000 description 1
229910017604 nitric acid Inorganic materials 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
210000000056 organ Anatomy 0.000 description 1
239000005416 organic matter Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
239000002798 polar solvent Substances 0.000 description 1
125000001453 quaternary ammonium group Chemical group 0.000 description 1
230000007017 scission Effects 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
238000003756 stirring Methods 0.000 description 1
DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 description 1

Classifications

- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/42—Measuring deposition or liberation of materials from an electrolyte; Coulometry, i.e. measuring coulomb-equivalent of material in an electrolyte
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/19—Halogen containing
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/19—Halogen containing
- Y10T436/196666—Carbon containing compound [e.g., vinylchloride, etc.]
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/25—Chemistry: analytical and immunological testing including sample preparation
- Y10T436/25375—Liberation or purification of sample or separation of material from a sample [e.g., filtering, centrifuging, etc.]

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Health & Medical Sciences (AREA)
Physics & Mathematics (AREA)
Chemical Kinetics & Catalysis (AREA)
Electrochemistry (AREA)
Molecular Biology (AREA)
Analytical Chemistry (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
General Physics & Mathematics (AREA)
Immunology (AREA)
Pathology (AREA)
Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

NL8302076A 1983-06-10 1983-06-10 Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen. NL8302076A (nl)

Priority Applications (7)

Application Number	Priority Date	Filing Date	Title
NL8302076A NL8302076A (nl)	1983-06-10	1983-06-10	Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen.
PCT/NL1984/000017 WO1984004968A1 (en)	1983-06-10	1984-06-08	Process of determination of the concentration of halogen in organic samples
AT84200832T ATE30357T1 (de)	1983-06-10	1984-06-08	Verfahren zur halogenbestimmung in organischen proben.
DE8484200832T DE3466907D1 (en)	1983-06-10	1984-06-08	Process of determining the concentration of halogen in organic samples
US06/706,852 US4778570A (en)	1983-06-10	1984-06-08	Process for determining the organic halogen content of organic samples
EP84200832A EP0128627B1 (de)	1983-06-10	1984-06-08	Verfahren zur Halogenbestimmung in organischen Proben
JP59502322A JPS60501673A (ja)	1983-06-10	1984-06-08	有機物試料中のハロゲン濃度の決定法

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL8302076		1983-06-10
NL8302076A NL8302076A (nl)	1983-06-10	1983-06-10	Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen.

Publications (1)

Publication Number	Publication Date
NL8302076A true NL8302076A (nl)	1985-01-02

Family

ID=19841992

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8302076A NL8302076A (nl)	1983-06-10	1983-06-10	Werkwijze voor het bepalen van het gehalte aan organisch gebonden halogeen.

Country Status (7)

Country	Link
US (1)	US4778570A (de)
EP (1)	EP0128627B1 (de)
JP (1)	JPS60501673A (de)
AT (1)	ATE30357T1 (de)
DE (1)	DE3466907D1 (de)
NL (1)	NL8302076A (de)
WO (1)	WO1984004968A1 (de)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2634077B2 (ja) *	1989-01-18	1997-07-23	ダイセル化学工業株式会社	微量ヨウ化物の測定装置
US5427955A (en) *	1993-06-01	1995-06-27	Utah State University Foundation	Photochemical determination of organic compounds
US5569809A (en) *	1995-07-03	1996-10-29	General Electric Company	Method for destruction of chlorinated hydrocarbons
US6190922B1 (en)	1998-04-16	2001-02-20	Strategic Diagnostics Inc.	Substrate supported liquid extraction
CN102539511B (zh) *	2012-01-31	2013-09-04	金发科技股份有限公司	自动电位滴定法测定阻燃剂溴含量的方法
CN104502434A (zh) *	2014-12-25	2015-04-08	北京彤程创展科技有限公司	一种测定橡胶和橡胶制品中卤素含量的方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB711812A (en) *	1951-11-06	1954-07-14	Leeds & Northrup Co	Improvements in electrolytic determination of the concentration of a constituent in a solution
DE1086918B (de) *	1958-05-09	1960-08-11	Friedrich Oehme Dipl Chem	Verfahren zur coulometrischen Wasserbestimmung
US3523872A (en) *	1965-02-18	1970-08-11	Beckman Instruments Inc	Gas analysis
US3413199A (en) *	1965-09-29	1968-11-26	Fischer & Porter Co	Method for measurement of residual chlorine or the like
FR2079881A5 (de) *	1970-02-16	1971-11-12	Rhone Poulenc Sa
US3876514A (en) *	1971-12-06	1975-04-08	Monsanto Co	Electrolysis of allyl halides
US4028201A (en) *	1972-11-13	1977-06-07	Monsanto Company	Electrolytic monocarboxylation of activated olefins
FR2239920A5 (en) *	1973-07-31	1975-02-28	Dow Chemical Co	Determination of chlorine or bromine in gas mixture - by coulometric cell balanced in absence of chlorine or bromine
SU576536A1 (ru) *	1975-07-01	1977-10-15	Предприятие П/Я А-7411	Способ определени трехбромистого фосфора
US4072584A (en) *	1976-12-21	1978-02-07	Allied Chemical Corporation	Electrochemical production of organic thiols
US4160802A (en) *	1978-02-23	1979-07-10	University Of Illinois Foundation	Instrument for the automated determination of organic halogens
JPS6026687A (ja) *	1983-07-26	1985-02-09	Kanegafuchi Chem Ind Co Ltd	低水素過電圧陰極の劣化防止方法

1983
- 1983-06-10 NL NL8302076A patent/NL8302076A/nl not_active Application Discontinuation
1984
- 1984-06-08 WO PCT/NL1984/000017 patent/WO1984004968A1/en not_active Ceased
- 1984-06-08 AT AT84200832T patent/ATE30357T1/de not_active IP Right Cessation
- 1984-06-08 JP JP59502322A patent/JPS60501673A/ja active Granted
- 1984-06-08 US US06/706,852 patent/US4778570A/en not_active Expired - Fee Related
- 1984-06-08 EP EP84200832A patent/EP0128627B1/de not_active Expired
- 1984-06-08 DE DE8484200832T patent/DE3466907D1/de not_active Expired

Also Published As

Publication number	Publication date
JPS60501673A (ja)	1985-10-03
DE3466907D1 (en)	1987-11-26
ATE30357T1 (de)	1987-11-15
EP0128627A1 (de)	1984-12-19
WO1984004968A1 (en)	1984-12-20
US4778570A (en)	1988-10-18
JPH0450978B2 (de)	1992-08-17
EP0128627B1 (de)	1987-10-21

Legal Events

Date	Code	Title	Description
1985-01-02	A1B	A search report has been drawn up
1987-02-02	BV	The patent application has lapsed

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