NO982567L - Forbedret hydrogenolyse av 2,4,6,8,10,12-heksaazatetracyklo (5.5.0.05.903.11) dodekan - Google Patents

Forbedret hydrogenolyse av 2,4,6,8,10,12-heksaazatetracyklo (5.5.0.05.903.11) dodekan

Info

Publication number
NO982567L
NO982567L NO982567A NO982567A NO982567L NO 982567 L NO982567 L NO 982567L NO 982567 A NO982567 A NO 982567A NO 982567 A NO982567 A NO 982567A NO 982567 L NO982567 L NO 982567L
Authority
NO
Norway
Prior art keywords
hbiw
hydrogen
dodecane
tadb
hydrogenation
Prior art date
Application number
NO982567A
Other languages
English (en)
Norwegian (no)
Other versions
NO982567D0 (no
Inventor
Robert B Wardle
Wayne W Edwards
Original Assignee
Thiokol Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Thiokol Corp filed Critical Thiokol Corp
Publication of NO982567D0 publication Critical patent/NO982567D0/no
Publication of NO982567L publication Critical patent/NO982567L/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains four or more hetero rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
NO982567A 1995-12-07 1998-06-04 Forbedret hydrogenolyse av 2,4,6,8,10,12-heksaazatetracyklo (5.5.0.05.903.11) dodekan NO982567L (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/568,451 US5739325A (en) 1995-12-07 1995-12-07 Hydrogenolysis of 2,4,6,8,10,12-Hexabenzyl-2,4,6,8,10,12-Hexaazatetracyclo 5.5.0.05,9.03,11 !dodecane
PCT/US1996/019130 WO1997020785A1 (fr) 1995-12-07 1996-12-04 Procede ameliore d'hydrogenolyse du 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0?5,9.03,11¿]dodecane

Publications (2)

Publication Number Publication Date
NO982567D0 NO982567D0 (no) 1998-06-04
NO982567L true NO982567L (no) 1998-08-05

Family

ID=24271352

Family Applications (1)

Application Number Title Priority Date Filing Date
NO982567A NO982567L (no) 1995-12-07 1998-06-04 Forbedret hydrogenolyse av 2,4,6,8,10,12-heksaazatetracyklo (5.5.0.05.903.11) dodekan

Country Status (5)

Country Link
US (1) US5739325A (fr)
EP (1) EP0865417B1 (fr)
JP (1) JP4083219B2 (fr)
NO (1) NO982567L (fr)
WO (1) WO1997020785A1 (fr)

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US7129348B1 (en) 1988-12-21 2006-10-31 Alliant Techsystems Inc. Polycyclic, polyamides as precursors for energetic polycyclic polynitramine oxidizers
JP2844125B2 (ja) 1995-02-01 1999-01-06 旭化成工業株式会社 ヘキサアザイソウルチタン誘導体およびその製造方法
DE69608359T2 (de) * 1995-02-01 2001-02-08 Asahi Kasei Kogyo K.K., Osaka Hexaazaisowurtzitan-derivate und verfahren zu deren herstellung
FR2830532B1 (fr) * 1996-02-15 2005-09-16 Poudres & Explosifs Ste Nale Procede de synthese de derives de l'hexaazaisowurtzitane et forme polymorphe alpha d'un derive de l'hexaazaisowurtzitane
JP2000510087A (ja) * 1996-05-03 2000-08-08 イーストマン ケミカル カンパニー 爆薬処方物
WO1998005666A1 (fr) * 1996-08-07 1998-02-12 Asahi Kasei Kogyo Kabushiki Kaisya Procede pour la preparation d'hexanitrohexaazaisowurtzitanes
DE69722949T2 (de) 1996-10-14 2004-05-13 Asahi Kasei Kogyo K.K. Verfahren zur herstellung acylierter hexaazaisowurtzitan-derivate
AU5374398A (en) * 1996-12-17 1998-07-15 Cordant Technologies, Inc. Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo (5.5.0.05,903,11)-dodecane
DE69822652T2 (de) * 1997-10-14 2004-12-23 Asahi Kasei Chemicals Corp. Verfahren zur herstellung von hexakis(arylmethyl)hexaazaisowurtzitan
FR2770216B1 (fr) * 1997-10-29 1999-12-03 Poudres & Explosifs Ste Nale Procede d'obtention de la forme polymorphe epsilon de l'hexanitrohexaazaisowurtzitane
JP2770018B1 (ja) * 1997-11-26 1998-06-25 旭化成工業株式会社 ヘキサニトロヘキサアザイソウルチタン組成物及び該組成物を配合して成る高性能火薬組成物
US6297373B1 (en) * 1997-12-26 2001-10-02 Asahi Kasei Kabushiki Kaisha Method for acylating hexakis (arylmethyl) hexaazaisowurtzitane
FI104800B2 (fi) * 1998-02-24 2003-11-14 Ponsse Oy Syöttötela
US6015898A (en) * 1998-05-01 2000-01-18 The United States Of America, As Represented By The Secretary Of The Army Processes and compositions for nitration of N-substituted isowurtzitane compounds with concentrated nitric acid at elevated temperatures to form HNIW and recovery of gamma HNIW with high yields and purities
US6107483A (en) * 1998-07-31 2000-08-22 Cordant Technologies Inc. Process for the large-scale synthesis of 4,10-dinitro-2,6,8-12-tetraoxa-4,10-diazatetracyclo-[5.5.0.05,903,11]-do decane
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
US6391130B1 (en) 1999-02-16 2002-05-21 Alliant Techsystems Inc. Process for making 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6156137A (en) * 1999-11-05 2000-12-05 Atlantic Research Corporation Gas generative compositions
US6350871B1 (en) 2000-03-31 2002-02-26 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US7288648B2 (en) * 2000-10-06 2007-10-30 Alliant Techsystems Inc. High temperature crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US6992185B2 (en) 2002-01-09 2006-01-31 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
RU2359753C1 (ru) * 2008-02-14 2009-06-27 Институт катализа им. Г.К. Борескова Сибирского отделения Российской академии наук (статус государственного учреждения) Катализатор, способ его приготовления и способ получения тетраацетилдиформилгексаазаизовюрцитана
RU2431636C1 (ru) * 2010-05-11 2011-10-20 Учреждение Российской академии наук Институт проблем химико-энергетических технологий Сибирского отделения РАН (ИПХЭТ СО РАН) Способ получения 2,4,6,8,10,12-гексабензил-2,4,6,8,10,12-гексаазатетрацикло[5,5,0,03,11,05,9]додекана
CN107353293B (zh) * 2016-07-28 2019-08-16 湖北航天化学技术研究所 一种三步反应制备cl-20的方法
RU2641694C1 (ru) * 2016-12-14 2018-01-22 Акционерное общество "Федеральный научно-производственный центр "Алтай" Способ получения катализатора и способ его применения для многократного использования в промышленном процессе двухстадийного гидрогенолиза при производстве 2,4,6,8,10,12-гексанитро-2,4,6,8,10,12-гексаазатетрацикло[5,5,0,03,11,05,9]додекана
CN111644194B (zh) * 2020-06-19 2021-05-28 北京理工大学 Pd/mpg-C3N4催化剂在HBIW氢解反应中的循环应用方法
CN113210000A (zh) * 2021-05-07 2021-08-06 北京理工大学 Pd/g-C3N4NS催化剂在HBIW氢解反应中的应用
CN114452975B (zh) * 2021-12-27 2024-05-10 西安近代化学研究所 一种蜂窝陶瓷负载钯基催化剂及其在hbiw氢解脱苄中的应用
CN115611905B (zh) * 2022-09-09 2024-08-16 南京铁鸣能源科技有限公司 一种基于单原子催化剂高效合成cl-20高含能笼状化合物的方法
CN115672317A (zh) * 2022-10-19 2023-02-03 北京工业大学 一种提高Pd(OH)2/C催化剂氢解脱苄活性的方法
CN120479419B (zh) * 2025-07-16 2025-09-30 北京理工大学 Pd(OH)2/超薄载球型二维SiO2催化剂的制备方法及其产品与应用

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US2459002A (en) * 1944-09-26 1949-01-11 American Cyanamid Co Preparation of acyl-nitroarylides
US2485855A (en) * 1944-12-30 1949-10-25 Us Seeretary Of The Navy Nitramines
US3228929A (en) * 1964-06-08 1966-01-11 Aerojet General Co Certain 1-trinitroalkylene-substituted dinitrotriazacycloalkanes and their preparation
US3535390A (en) * 1968-03-26 1970-10-20 Sun Oil Co Nitroadamantanes
FR2238703B1 (fr) * 1973-07-24 1977-02-18 Poudres & Explosifs Ste Nale
US4432902A (en) * 1982-07-20 1984-02-21 The United States Of America As Represented By The Department Of Energy Method for synthesizing HMX
US4485237A (en) * 1983-03-08 1984-11-27 The United States Of America As Represented By The Secretary Of The Navy Insensitive polynitramine compound
US5124493A (en) * 1991-10-15 1992-06-23 The United States Of America As Represented By The Secretary Of The Army Process of producing XMX in 100% yield and purity
US5409617A (en) * 1993-07-13 1995-04-25 Sri International Environmentally acceptable waste disposal by conversion of hydrothermally labile compounds

Also Published As

Publication number Publication date
NO982567D0 (no) 1998-06-04
EP0865417B1 (fr) 2004-03-31
US5739325A (en) 1998-04-14
JP2000501706A (ja) 2000-02-15
EP0865417A1 (fr) 1998-09-23
WO1997020785A1 (fr) 1997-06-12
JP4083219B2 (ja) 2008-04-30
EP0865417A4 (fr) 2001-05-02

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