PL1937630T3 - Sposób wytwarzania nadtlenków organicznych za pomocą mikrotechniki reakcyjnej - Google Patents
Sposób wytwarzania nadtlenków organicznych za pomocą mikrotechniki reakcyjnejInfo
- Publication number
- PL1937630T3 PL1937630T3 PL06806251T PL06806251T PL1937630T3 PL 1937630 T3 PL1937630 T3 PL 1937630T3 PL 06806251 T PL06806251 T PL 06806251T PL 06806251 T PL06806251 T PL 06806251T PL 1937630 T3 PL1937630 T3 PL 1937630T3
- Authority
- PL
- Poland
- Prior art keywords
- production
- organic peroxides
- peroxides
- microreaction
- technique
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 150000001451 organic peroxides Chemical class 0.000 title abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 239000012933 diacyl peroxide Substances 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- -1 ketone peroxides Chemical class 0.000 abstract 1
- 150000002978 peroxides Chemical class 0.000 abstract 1
- 150000004978 peroxycarbonates Chemical class 0.000 abstract 1
- 125000005634 peroxydicarbonate group Chemical group 0.000 abstract 1
- 230000003068 static effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/16—Peroxy compounds the —O—O— group being bound between two carbon atoms not further substituted by oxygen atoms, i.e. peroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/82—Combinations of dissimilar mixers
- B01F33/821—Combinations of dissimilar mixers with consecutive receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
- B01F35/715—Feeding the components in several steps, e.g. successive steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/20—Peroxy compounds the —O—O— group being bound to a carbon atom further substituted by singly—bound oxygen atoms
- C07C409/22—Peroxy compounds the —O—O— group being bound to a carbon atom further substituted by singly—bound oxygen atoms having two —O—O— groups bound to the carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/38—Peroxy compounds the —O—O— group being bound between a >C=O group and a carbon atom, not further substituted by oxygen atoms, i.e. esters of peroxy acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/30—Micromixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/82—Combinations of dissimilar mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00851—Additional features
- B01J2219/00858—Aspects relating to the size of the reactor
- B01J2219/00862—Dimensions of the reaction cavity itself
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00873—Heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00889—Mixing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00925—Irradiation
- B01J2219/00932—Sonic or ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005049294A DE102005049294C5 (de) | 2005-10-14 | 2005-10-14 | Verfahren zur Herstellung organischer Peroxide mittels Mikroreaktionstechnik |
| EP06806251A EP1937630B1 (de) | 2005-10-14 | 2006-10-13 | Verfahren zur herstellung organischer peroxide mittels mikroreaktionstechnik |
| PCT/EP2006/009898 WO2007042313A2 (de) | 2005-10-14 | 2006-10-13 | Verfahren zur herstellung organischer peroxide mittels mikroreaktionstechnik |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL1937630T3 true PL1937630T3 (pl) | 2012-03-30 |
Family
ID=37905095
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL06806251T PL1937630T3 (pl) | 2005-10-14 | 2006-10-13 | Sposób wytwarzania nadtlenków organicznych za pomocą mikrotechniki reakcyjnej |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7968753B2 (pl) |
| EP (1) | EP1937630B1 (pl) |
| CN (1) | CN101287704A (pl) |
| AT (1) | ATE518830T1 (pl) |
| DE (1) | DE102005049294C5 (pl) |
| PL (1) | PL1937630T3 (pl) |
| WO (1) | WO2007042313A2 (pl) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005049294C5 (de) | 2005-10-14 | 2012-05-03 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren zur Herstellung organischer Peroxide mittels Mikroreaktionstechnik |
| EP1849804A1 (en) * | 2006-04-27 | 2007-10-31 | Arkema France | Process of free-radical polymerization or crosslinking in the presence of an organic peroxide by an ex situ process |
| EP1852418A1 (en) | 2006-04-27 | 2007-11-07 | Arkema France | Process for synthesizing selected organic peroxides |
| DE102006032165A1 (de) * | 2006-07-12 | 2008-01-24 | Evonik Degussa Gmbh | Kontinuierliches Verfahren zur Herstellung von Acylperoxiden |
| FR2955508B1 (fr) | 2010-01-25 | 2012-03-30 | Corning Inc | Microreacteurs avec dispositif microfluidique plan et systeme d'application d'ultrasons ; mise en oeuvre de reactions chimiques en leur sein |
| WO2012025548A1 (en) | 2010-08-27 | 2012-03-01 | Solvay Sa | Process for the preparation of alkenones |
| CN102442933B (zh) * | 2010-10-08 | 2013-11-06 | 淄博正华助剂股份有限公司 | 溶剂型过氧化新癸酸特丁酯(bnp)的制备方法 |
| FR2968660B1 (fr) | 2010-12-14 | 2014-03-07 | Solvay | Procede de preparation d'une solution organique d'un peroxydicarbonate de dialkyle |
| CN102584663A (zh) * | 2011-12-26 | 2012-07-18 | 淄博正华助剂股份有限公司 | 溶剂型质量分数75%过氧化二碳酸二(2-乙基己基)酯的制法 |
| CN102659960B (zh) * | 2011-12-26 | 2014-08-20 | 淄博正华助剂股份有限公司 | 溶剂型质量分数60%过氧化二碳酸二(2-乙基己基)酯的制法 |
| EP2664607A1 (en) | 2012-05-16 | 2013-11-20 | Solvay Sa | Fluorination process |
| DE102012216945A1 (de) * | 2012-09-21 | 2014-05-28 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren und Vorrichtung zur Herstellung organischer Peroxide mittels Millireaktionstechnik |
| US9550731B2 (en) | 2014-05-22 | 2017-01-24 | Honeywell Federal Manufacturing & Technologies, Llc | Method for phase transfer synthesis of organic peroxides |
| CN104370789A (zh) * | 2014-11-26 | 2015-02-25 | 淄博正华助剂股份有限公司 | 连续流制备过氧化二碳酸双(2-乙基己基)酯(ehp)的方法 |
| CN104496874A (zh) * | 2014-11-26 | 2015-04-08 | 淄博正华助剂股份有限公司 | 连续流制备过氧化新癸酸异丙苯酯(cnp)的方法 |
| CN104447471A (zh) * | 2014-11-26 | 2015-03-25 | 淄博正华助剂股份有限公司 | 连续流制备过氧化二-(3,5,5-三甲基己酰)的方法 |
| CN104592080A (zh) * | 2014-11-26 | 2015-05-06 | 淄博正华助剂股份有限公司 | 连续流制备过氧化新癸酸特丁酯(bnp)的方法 |
| FR3042793B1 (fr) * | 2015-10-26 | 2019-12-27 | Arkema France | Synthese de peroxydes organiques a l'aide d'un reacteur agite a ecoulement oscillatoire |
| CN107698480B (zh) * | 2016-08-13 | 2020-09-11 | 上海惠和化德生物科技有限公司 | 一种无放大效应的过氧化新癸酸叔丁酯的连续流合成工艺 |
| CN107698479A (zh) * | 2016-08-18 | 2018-02-16 | 上海惠和化德生物科技有限公司 | 一种无放大效应的过氧化‑2‑乙基己基碳酸叔丁酯的连续流合成工艺 |
| CN107056670B (zh) * | 2017-06-13 | 2019-02-26 | 西安万德能源化学股份有限公司 | 一种二叔基过氧化物的制备方法 |
| CN109384699B (zh) * | 2017-08-12 | 2024-10-22 | 上海惠和化德生物科技有限公司 | 一种以双氧水为原料直接制备有机过氧化物的在线全连续流生产工艺 |
| WO2019034004A1 (zh) | 2017-08-12 | 2019-02-21 | 上海惠和化德生物科技有限公司 | 一种以双氧水为原料直接制备有机过氧化物的在线全连续流生产工艺 |
| CN109553560A (zh) * | 2017-08-12 | 2019-04-02 | 上海惠和化德生物科技有限公司 | 一种由醇或烷烃直接制备有机过氧化物的在线全连续流生产工艺 |
| CN111770913B (zh) * | 2017-12-19 | 2023-05-16 | 诺力昂化学品国际有限公司 | 制备粉状有机过氧化物配制剂的方法 |
| MX2020007875A (es) * | 2018-01-25 | 2020-09-07 | Nouryon Chemicals Int Bv | Proceso para la produccion de un fertilizante. |
| CN109265384B (zh) * | 2018-11-02 | 2021-02-12 | 南京工业大学 | 一种制备过氧化二碳酸二(2-乙基己基)酯的方法 |
| CN109369489B (zh) * | 2018-11-20 | 2020-09-08 | 淄博正华助剂股份有限公司 | 过氧化酮的合成方法 |
| CN109485592A (zh) * | 2018-11-20 | 2019-03-19 | 淄博正华助剂股份有限公司 | 过氧化二碳酸酯的合成方法 |
| CN109369490B (zh) * | 2018-11-20 | 2020-09-08 | 淄博正华助剂股份有限公司 | 叔丁基过氧化碳酸酯的合成方法 |
| FR3090630B1 (fr) * | 2018-12-19 | 2021-10-29 | Arkema France | Préparation d’une composition comprenant un peroxyde organique par transfert de solvant |
| CN111072542A (zh) * | 2019-12-26 | 2020-04-28 | 云南正邦科技有限公司 | 一种多点进料与强化混合连续生产过氧化二异丁酰的方法 |
| CN116655508B (zh) * | 2022-10-18 | 2026-03-10 | 常熟市滨江化工有限公司 | 一种用微通道反应器制备过氧化苯甲酸叔丁酯的方法 |
| CN116730889B (zh) * | 2023-06-13 | 2026-02-03 | 清华大学 | 过氧化二-(3,5,5-三甲基己酰)的合成方法及实施该合成方法的设备 |
| CN119350209B (zh) * | 2024-09-18 | 2026-04-07 | 江西理文化工有限公司 | 一种过氧化二碳酸二异丙酯的制备方法及过氧化二碳酸二异丙酯的应用 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4075236A (en) * | 1976-09-30 | 1978-02-21 | Pennwalt Corporation | Continuous manufacture of peroxyesters |
| US4222671A (en) * | 1978-09-05 | 1980-09-16 | Gilmore Oscar Patrick | Static mixer |
| KR900000170B1 (ko) * | 1984-06-05 | 1990-01-23 | 가부시끼가이샤 도오시바 | 다이내믹형 메모리셀과 그 제조방법 |
| US5021516A (en) * | 1989-06-26 | 1991-06-04 | E. I. Du Pont De Nemours And Company | Poly(perfluoroether)acyl peroxides |
| US5137369A (en) * | 1991-01-18 | 1992-08-11 | Hodan John A | Static mixing device |
| DE4416343C2 (de) * | 1994-05-09 | 1996-10-17 | Karlsruhe Forschzent | Statischer Mikro-Vermischer |
| DE19511603A1 (de) * | 1995-03-30 | 1996-10-02 | Norbert Dr Ing Schwesinger | Vorrichtung zum Mischen kleiner Flüssigkeitsmengen |
| US5831131A (en) * | 1995-08-30 | 1998-11-03 | E. I. Du Pont De Nemours And Company | Process for preparing peroxides |
| DE19540292C1 (de) * | 1995-10-28 | 1997-01-30 | Karlsruhe Forschzent | Statischer Mikrovermischer |
| DE69808489T2 (de) * | 1997-07-25 | 2003-07-10 | Akzo Nobel N.V., Arnheim/Arnhem | Verfahren zur herstellung eines tertiären esters |
| DE19741645A1 (de) * | 1997-09-22 | 1999-03-25 | Bayer Ag | Verfahren und Vorrichtung zur Oxidation organischer Verbindungen in flüssiger Phase unter Verwendung peroxidischer Oxidationsmittel |
| DE10020632A1 (de) * | 2000-04-27 | 2001-10-31 | Merck Patent Gmbh | Verfahren zur Expodierung von Olefinen |
| DE10103425A1 (de) * | 2001-01-26 | 2002-08-01 | Basf Ag | Statischer Mischer mit geschichtetem Aufbau |
| DE20218972U1 (de) * | 2002-12-07 | 2003-02-13 | Ehrfeld Mikrotechnik AG, 55234 Wendelsheim | Statischer Laminationsmikrovermischer |
| DE20304101U1 (de) * | 2003-03-14 | 2003-05-22 | Ehrfeld Mikrotechnik AG, 55234 Wendelsheim | Mikrovermischer mit integriertem Wärmetauscher |
| DE10350484B4 (de) * | 2003-12-20 | 2006-02-02 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren und Vorrichtung zur Markierung von Proteinen |
| DE502005005027D1 (de) | 2004-02-17 | 2008-09-25 | Ehrfeld Mikrotechnik Bts Gmbh | Mikromischer |
| DE102005049294C5 (de) | 2005-10-14 | 2012-05-03 | Ehrfeld Mikrotechnik Bts Gmbh | Verfahren zur Herstellung organischer Peroxide mittels Mikroreaktionstechnik |
-
2005
- 2005-10-14 DE DE102005049294A patent/DE102005049294C5/de not_active Expired - Fee Related
-
2006
- 2006-10-13 AT AT06806251T patent/ATE518830T1/de active
- 2006-10-13 EP EP06806251A patent/EP1937630B1/de not_active Revoked
- 2006-10-13 WO PCT/EP2006/009898 patent/WO2007042313A2/de not_active Ceased
- 2006-10-13 CN CNA2006800383002A patent/CN101287704A/zh active Pending
- 2006-10-13 PL PL06806251T patent/PL1937630T3/pl unknown
- 2006-10-13 US US12/089,908 patent/US7968753B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE102005049294A1 (de) | 2007-04-26 |
| DE102005049294C5 (de) | 2012-05-03 |
| US7968753B2 (en) | 2011-06-28 |
| US20090043122A1 (en) | 2009-02-12 |
| EP1937630B1 (de) | 2011-08-03 |
| WO2007042313A2 (de) | 2007-04-19 |
| WO2007042313A3 (de) | 2007-06-14 |
| ATE518830T1 (de) | 2011-08-15 |
| DE102005049294B4 (de) | 2009-03-26 |
| EP1937630A2 (de) | 2008-07-02 |
| CN101287704A (zh) | 2008-10-15 |
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