PL3197859T3 - Sposób wytwarzania diestrów kwasu tereftalowego z dehydratacją alkoholu zawracanego - Google Patents
Sposób wytwarzania diestrów kwasu tereftalowego z dehydratacją alkoholu zawracanegoInfo
- Publication number
- PL3197859T3 PL3197859T3 PL15766173T PL15766173T PL3197859T3 PL 3197859 T3 PL3197859 T3 PL 3197859T3 PL 15766173 T PL15766173 T PL 15766173T PL 15766173 T PL15766173 T PL 15766173T PL 3197859 T3 PL3197859 T3 PL 3197859T3
- Authority
- PL
- Poland
- Prior art keywords
- dehydration
- terephthalic acid
- producing diesters
- recirculated alcohol
- recirculated
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/80—Phthalic acid esters
- C07C69/82—Terephthalic acid esters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14186143 | 2014-09-24 | ||
| EP15766173.7A EP3197859B1 (de) | 2014-09-24 | 2015-09-21 | Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-entwässerung |
| PCT/EP2015/071576 WO2016046118A1 (de) | 2014-09-24 | 2015-09-21 | Verfahren zur herstellung von terephthalsäurediestern mit rückalkohol-entwässerung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL3197859T3 true PL3197859T3 (pl) | 2019-08-30 |
Family
ID=51660314
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL15766173T PL3197859T3 (pl) | 2014-09-24 | 2015-09-21 | Sposób wytwarzania diestrów kwasu tereftalowego z dehydratacją alkoholu zawracanego |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US10207978B2 (pl) |
| EP (1) | EP3197859B1 (pl) |
| CN (1) | CN106715382A (pl) |
| BR (1) | BR112017005839A2 (pl) |
| CA (1) | CA2962305C (pl) |
| ES (1) | ES2724982T3 (pl) |
| MX (1) | MX2017003920A (pl) |
| PL (1) | PL3197859T3 (pl) |
| RU (1) | RU2668223C1 (pl) |
| TR (1) | TR201904928T4 (pl) |
| TW (1) | TW201612150A (pl) |
| WO (1) | WO2016046118A1 (pl) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2917178T3 (es) | 2015-07-09 | 2022-07-07 | Basf Se | Composiciones curables |
| US12104013B2 (en) * | 2017-07-17 | 2024-10-01 | Technip Zimmer Gmbh | Method for preparing polyesters |
| CN112439377A (zh) * | 2019-08-29 | 2021-03-05 | 江苏察克润滑科技有限公司 | 一种用于制备防锈液的反应釜 |
| KR102501597B1 (ko) * | 2019-09-25 | 2023-02-20 | 주식회사 엘지화학 | 디에스테르계 조성물의 제조 시스템 및 제조방법 |
| KR102683132B1 (ko) * | 2019-09-27 | 2024-07-10 | 주식회사 엘지화학 | 디에스터계 물질의 정제 유닛 및 이를 포함하는 디에스터계 물질의 정제 시스템 |
| KR102797136B1 (ko) * | 2020-11-17 | 2025-04-18 | 주식회사 엘지화학 | 디에스터계 화합물의 제조방법 |
| CN115282894A (zh) * | 2022-06-30 | 2022-11-04 | 福建久策气体股份有限公司 | 一种二氟乙酰乙酸乙酯生产装置及其工作方法 |
Family Cites Families (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB798439A (en) | 1954-10-26 | 1958-07-23 | Bayer Ag | Process for the manufacture of terephthalic acid dimethyl ester |
| DE1286003B (de) * | 1966-06-21 | 1969-01-02 | Metallgesellschaft Ag | Verfahren zur kontinuierlichen Veresterung von Terephthal- und Isophthalsaeure mit AEthylenglykol |
| US3617226A (en) * | 1968-04-26 | 1971-11-02 | Huels Chemische Werke Ag | Apparatus for the continuous preparation of esters |
| BE789047A (fr) * | 1971-09-20 | 1973-03-20 | Montedison Spa | Procede pour l'esterification en continu d'acides dicarboxyliques et d'alcools |
| BR8103970A (pt) | 1980-10-20 | 1982-08-24 | Ad Ind Inc | Processo para remocao de vapor de agua de etanol gasoso |
| GB2088739B (en) | 1980-11-28 | 1983-11-30 | Coal Industry Patents Ltd | Drying organic solvents |
| US4372857A (en) | 1981-03-05 | 1983-02-08 | Union Carbide Corporation | Liquid adsorption process and apparatus |
| US4465875A (en) | 1982-09-27 | 1984-08-14 | Calgon Carbon Corporation | Process for dehydrating ethanol |
| US4487614A (en) | 1983-11-16 | 1984-12-11 | Union Carbide Corporation | Adsorption separation cycle |
| GB2151501A (en) | 1983-12-22 | 1985-07-24 | Coal Ind | Continuous sorption process |
| US4726818A (en) | 1984-12-20 | 1988-02-23 | Union Carbide Corporation | Bulk removal of water from organic liquids |
| GB8601082D0 (en) | 1986-01-17 | 1986-02-19 | Distillers Co Carbon Dioxide | Potable spirit production |
| US4670580A (en) * | 1986-03-31 | 1987-06-02 | Celanese Corporation | Process for preparing oligomeric glycol esters of dicarboxylic acids |
| DE69012682T2 (de) | 1989-06-12 | 1995-04-06 | Merck & Co Inc | Verfahren zur Entfernung von bakteriellen Endotoxinen aus gram-negativen Polysacchariden. |
| JPH04308543A (ja) | 1991-04-06 | 1992-10-30 | Kobe Steel Ltd | 含水エタノールの精製方法 |
| JP3379758B2 (ja) | 1994-02-07 | 2003-02-24 | クイアジェン・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング | イソプロパノール含有水溶液を用いる核酸のトランスフェクション効率の増強 |
| FR2719039B1 (fr) | 1994-04-22 | 1996-06-21 | Interis | Nouveau procédé de déshydratation d'alcool par adsorption/regénération sur tamis moléculaire, et installation pour sa mise en Óoeuvre. |
| AU4314099A (en) | 1998-06-01 | 1999-12-20 | Immune Response Corporation, The | Novel method of large scale plasmid purification |
| DE10043545A1 (de) * | 2000-09-05 | 2002-03-14 | Oxeno Olefinchemie Gmbh | Verfahren zur Herstellung von Carbonsäureestern |
| DE10056179A1 (de) | 2000-11-13 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von Estern mehrbasiger Säuren |
| JP4996791B2 (ja) | 2001-03-14 | 2012-08-08 | Jnc株式会社 | エンドトキシン吸着体、及びそれを用いたエンドトキシンの除去方法 |
| DE602004020473D1 (de) | 2003-06-24 | 2009-05-20 | Organon Nv | Abtrennung von lipopolysacchariden aus lipopolysaccharidkomplexen mit hilfe von nicht-entzündbaren lösungsmitteln |
| US7531308B2 (en) | 2004-04-23 | 2009-05-12 | Sigma-Aldrich Co. | Process for the reduction of endotoxins in a plasmid preparation using a carbohydrate non-ionic detergent with silica chromatography |
| US7799942B2 (en) * | 2005-08-12 | 2010-09-21 | Eastman Chemical Company | Production of terephthalic acid di-esters |
| US7276621B2 (en) | 2005-08-12 | 2007-10-02 | Eastman Chemical Company | Production of di-(2-ethylhexyl) terephthalate |
| JP4956945B2 (ja) | 2005-09-12 | 2012-06-20 | 三菱化学株式会社 | テレフタル酸ジエステルの製造方法 |
| WO2007115046A1 (en) | 2006-03-31 | 2007-10-11 | Invitrogen Corporation | Low-endotoxin nucleic acid preparations |
| CN101511387A (zh) | 2006-09-08 | 2009-08-19 | 惠氏公司 | 使用亲和色谱法纯化蛋白质的精氨酸洗涤液 |
| US7943094B2 (en) | 2006-12-07 | 2011-05-17 | Grupo Petrotemex, S.A. De C.V. | Polyester production system employing horizontally elongated esterification vessel |
| US8034970B2 (en) | 2007-06-27 | 2011-10-11 | H R D Corporation | Method of making phthalic acid diesters |
| CN102256923B (zh) | 2008-12-16 | 2013-12-04 | 巴斯夫欧洲公司 | 制备羧酸酯的方法 |
| ES2422262T3 (es) | 2008-12-16 | 2013-09-10 | Basf Se | Procedimiento para la elaboración de un éster crudo |
| CN102958898B (zh) | 2010-08-25 | 2015-05-20 | 埃克森美孚化学专利公司 | 酯的制备方法 |
| TWI654177B (zh) | 2013-10-31 | 2019-03-21 | 德商巴斯夫歐洲公司 | 製備羧酸酯的方法及其作爲塑化劑的用途 |
| CN106232571B (zh) | 2014-04-22 | 2019-05-28 | 巴斯夫欧洲公司 | 在离子液体和酸性酯化催化剂的存在下制备羧酸酯的方法及其作为塑化剂的用途 |
-
2015
- 2015-09-21 CN CN201580051362.6A patent/CN106715382A/zh active Pending
- 2015-09-21 TR TR2019/04928T patent/TR201904928T4/tr unknown
- 2015-09-21 PL PL15766173T patent/PL3197859T3/pl unknown
- 2015-09-21 EP EP15766173.7A patent/EP3197859B1/de active Active
- 2015-09-21 ES ES15766173T patent/ES2724982T3/es active Active
- 2015-09-21 US US15/513,757 patent/US10207978B2/en active Active
- 2015-09-21 CA CA2962305A patent/CA2962305C/en not_active Expired - Fee Related
- 2015-09-21 MX MX2017003920A patent/MX2017003920A/es unknown
- 2015-09-21 WO PCT/EP2015/071576 patent/WO2016046118A1/de not_active Ceased
- 2015-09-21 RU RU2017113965A patent/RU2668223C1/ru not_active IP Right Cessation
- 2015-09-21 BR BR112017005839A patent/BR112017005839A2/pt not_active Application Discontinuation
- 2015-09-23 TW TW104131415A patent/TW201612150A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| TW201612150A (en) | 2016-04-01 |
| WO2016046118A1 (de) | 2016-03-31 |
| CA2962305C (en) | 2019-06-11 |
| US10207978B2 (en) | 2019-02-19 |
| EP3197859A1 (de) | 2017-08-02 |
| EP3197859B1 (de) | 2019-02-06 |
| CN106715382A (zh) | 2017-05-24 |
| TR201904928T4 (tr) | 2019-05-21 |
| MX2017003920A (es) | 2017-06-28 |
| ES2724982T3 (es) | 2019-09-18 |
| BR112017005839A2 (pt) | 2018-01-30 |
| US20170297997A1 (en) | 2017-10-19 |
| RU2668223C1 (ru) | 2018-09-27 |
| CA2962305A1 (en) | 2016-03-31 |
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