PL3494085T3 - Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu - Google Patents

Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu

Info

Publication number
PL3494085T3
PL3494085T3 PL17822387T PL17822387T PL3494085T3 PL 3494085 T3 PL3494085 T3 PL 3494085T3 PL 17822387 T PL17822387 T PL 17822387T PL 17822387 T PL17822387 T PL 17822387T PL 3494085 T3 PL3494085 T3 PL 3494085T3
Authority
PL
Poland
Prior art keywords
fluorosulfonyl
drying
lithium bis
imide salt
purifying lithium
Prior art date
Application number
PL17822387T
Other languages
English (en)
Inventor
Grégory Schmidt
Rémy Teissier
Original Assignee
Arkema France
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France filed Critical Arkema France
Publication of PL3494085T3 publication Critical patent/PL3494085T3/pl

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/056Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566Liquid materials
    • H01M10/0568Liquid materials characterised by the solutes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/087Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
    • C01B21/093Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • B01D11/0492Applications, solvents used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36Azeotropic distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0009Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • H01M10/0525Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00Electrolytes
    • H01M2300/0017Non-aqueous electrolytes
    • H01M2300/0025Organic electrolyte
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/133Renewable energy sources, e.g. sunlight

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • Thermal Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Secondary Cells (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
PL17822387T 2016-12-08 2017-12-07 Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu PL3494085T3 (pl)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1662129A FR3059993A1 (fr) 2016-12-08 2016-12-08 Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide
EP17822387.1A EP3494085B1 (fr) 2016-12-08 2017-12-07 Procédé de séchage et de purification du sel de lithium de bis(fluorosulfonyl)imide
PCT/FR2017/053446 WO2018104674A1 (fr) 2016-12-08 2017-12-07 Procédé de séchage et de purification du sel de lithium de bis(fluorosulfonyl)imide

Publications (1)

Publication Number Publication Date
PL3494085T3 true PL3494085T3 (pl) 2022-05-02

Family

ID=58347546

Family Applications (1)

Application Number Title Priority Date Filing Date
PL17822387T PL3494085T3 (pl) 2016-12-08 2017-12-07 Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu

Country Status (8)

Country Link
US (2) US11316200B2 (pl)
EP (1) EP3494085B1 (pl)
JP (1) JP6989596B2 (pl)
KR (1) KR102397162B1 (pl)
CN (1) CN109923063B (pl)
FR (1) FR3059993A1 (pl)
PL (1) PL3494085T3 (pl)
WO (1) WO2018104674A1 (pl)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
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FR3059994B1 (fr) * 2016-12-08 2021-03-19 Arkema France Procede de sechage et de purification de lifsi
FR3059993A1 (fr) 2016-12-08 2018-06-15 Arkema France Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide
WO2020100115A1 (en) * 2018-11-16 2020-05-22 Ses Holdings Pte. Ltd. Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (lifsi) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries
US10967295B2 (en) 2018-11-16 2021-04-06 Ses Holdings Pte. Ltd. Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries
FR3088931B1 (fr) * 2018-11-28 2021-01-22 Arkema France Procédé de préparation du sel de lithium de bis(fluorosulfonyl)imide
CA3134664A1 (en) 2019-03-29 2020-10-08 Lithium Americas Corporation Method of lithium extraction from sedimentary clay
KR20220012911A (ko) * 2019-05-31 2022-02-04 가부시키가이샤 닛폰 쇼쿠바이 전해질 조성물, 용매 조성물, 비수전해액 및 그 용도
US12489138B2 (en) 2019-10-15 2025-12-02 Industry-University Cooperation Foundation Hanyang University Erica Campus Intermediate product of solid electrolyte, solid electrolyte using same, secondary battery including same, and method for manufacturing same
EP4047683A4 (en) 2019-10-15 2024-03-13 Industry-University Cooperation Foundation Hanyang University ERICA Campus Intermediate product of electrode, electrode powder, electrode using same, electrode pellet using same and method for producing each thereof
WO2021171948A1 (ja) * 2020-02-27 2021-09-02 株式会社日本触媒 組成物、電解液材料及び電解液
CN111675678B (zh) * 2020-06-29 2022-06-17 国联汽车动力电池研究院有限责任公司 一种用于离子液体的深度干燥除水方法
CN116390894A (zh) 2020-09-10 2023-07-04 索尔维公司 双(氟磺酰基)酰亚胺盐的纯化
CN117480114A (zh) * 2021-06-30 2024-01-30 株式会社日本触媒 磺酰亚胺水溶液的精制方法、非水电解液的制造方法及电解质组合物的制造方法
US20240391774A1 (en) * 2021-09-23 2024-11-28 Specialty Operations France Method for producing ultra-pure bis(chlorosulfonyl)imide
US20230178804A1 (en) * 2021-12-02 2023-06-08 Honeywell International Inc. Processes for producing lithium bis(fluorosulfonyl) imide
EP4273097A4 (en) * 2022-01-29 2024-10-02 Contemporary Amperex Technology Co., Limited LITHIUM BIS(FLUOROSULFONYL)IMIDE, ITS PREPARATION METHOD, ELECTROLYTE AND SECONDARY BATTERY
CN114380305A (zh) * 2022-01-29 2022-04-22 宁德时代新能源科技股份有限公司 一种在双氟磺酰亚胺锂的生产中回收原辅材料的方法
FR3134576B1 (fr) 2022-04-19 2025-07-18 Arkema France Procédé de préparation d’un sel de lithium fonctionnalisé
CN115677543B (zh) * 2022-10-14 2023-10-20 衢州市九洲化工有限公司 一种(二氟甲磺酰基)(三氟甲磺酰基)亚胺锂的合成方法
KR20250117675A (ko) * 2022-12-15 2025-08-05 스페셜티 오퍼레이션스 프랑스 비스(플루오로 설포닐)이미드 염 용액의 제조 방법
CN120530079A (zh) 2022-12-15 2025-08-22 法国特种经营公司 用于纯化双(氟磺酰基)亚胺盐的方法
CN116283671A (zh) * 2023-03-17 2023-06-23 浙江大学 一种低含水量双(三氟甲烷磺酰)亚胺锂的制备方法
FR3149134A1 (fr) 2023-05-25 2024-11-29 Arkema France Electrolyte à haute concentration en LiFSI
KR102720708B1 (ko) * 2023-09-08 2024-10-22 주식회사 천보비엘에스 리튬 비스(플루오로설포닐)이미드 용액 및 이를 포함하는 전지

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KR101291903B1 (ko) * 2008-07-23 2013-07-31 다이이치 고교 세이야쿠 가부시키가이샤 비스(플루오로설포닐)이미드 음이온 화합물의 제조 방법과 이온대화합물
JP5443118B2 (ja) * 2009-03-31 2014-03-19 三菱マテリアル株式会社 ビス(フルオロスルホニル)イミド塩の製造方法、ビス(フルオロスルホニル)イミド塩及びフルオロ硫酸塩の製造方法、並びにビス(フルオロスルホニル)イミド・オニウム塩の製造方法
KR101345271B1 (ko) * 2009-11-27 2013-12-27 가부시기가이샤 닛뽕쇼꾸바이 플루오로설포닐이미드염 및 플루오로설포닐이미드염의 제조방법
WO2011149095A1 (ja) 2010-05-28 2011-12-01 株式会社日本触媒 フルオロスルホニルイミドのアルカリ金属塩およびその製造方法
SG192235A1 (en) * 2011-03-03 2013-09-30 Nippon Soda Co Process for producing fluorine-containing sulfonylimide salt
KR101233325B1 (ko) * 2011-04-11 2013-02-14 로베르트 보쉬 게엠베하 리튬 이차 전지용 전해액 및 이를 포함하는 리튬 이차 전지
GB201110520D0 (en) * 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
FR2975694B1 (fr) 2011-05-24 2013-08-02 Arkema France Procede de preparation de bis(fluorosulfonyl)imidure de lithium
JP6208929B2 (ja) 2011-08-12 2017-10-04 株式会社日本触媒 フッ素原子を含むイオン性化合物またはフッ素原子を含むイオン性化合物含有組成物を包装してなる包装体
CA2904489C (en) * 2013-03-18 2017-02-14 Nippon Soda Co., Ltd. Method for producing disulfonylamine alkali metal salt
JP6139944B2 (ja) 2013-04-01 2017-05-31 株式会社日本触媒 フルオロスルホニルイミドのアルカリ金属塩の製造方法
JP6368466B2 (ja) * 2013-09-09 2018-08-01 株式会社日本触媒 フルオロスルホニルイミドの包装体の製造方法
FR3020060B1 (fr) * 2014-04-18 2016-04-01 Arkema France Preparation d'imides contenant un groupement fluorosulfonyle
JP2016088809A (ja) 2014-11-05 2016-05-23 株式会社日本触媒 フルオロスルホニルイミド塩の製造方法
CN104495767B (zh) * 2014-11-21 2017-01-04 湖南博氟新材料科技有限公司 一种双氟磺酰亚胺锂盐的制备方法
CN104925765B (zh) * 2015-05-21 2017-08-08 上海康鹏科技有限公司 一种双氟磺酰亚胺锂盐的制备方法
CN105836719B (zh) * 2016-04-29 2018-06-01 南京远淑医药科技有限公司 一种利用芳香甲基胺合成双氟磺酰亚胺锂盐的方法
CN105923614B (zh) * 2016-04-29 2018-01-09 南京远淑医药科技有限公司 一种利用邻苯二甲酰亚胺制备双氟磺酰亚胺锂盐的方法
JP6806514B2 (ja) 2016-09-27 2021-01-06 株式会社日本触媒 ビス(フルオロスルホニル)イミドのアルカリ金属塩と有機溶媒とを含む電解液材料の製造方法
FR3059994B1 (fr) * 2016-12-08 2021-03-19 Arkema France Procede de sechage et de purification de lifsi
FR3059993A1 (fr) 2016-12-08 2018-06-15 Arkema France Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide
FR3081723B1 (fr) * 2018-06-01 2022-04-15 Arkema France Procede de purification d'un sel de lithium de bis(fluorosulfonyl)imide

Also Published As

Publication number Publication date
CN109923063A (zh) 2019-06-21
US20190379088A1 (en) 2019-12-12
KR102397162B1 (ko) 2022-05-11
EP3494085B1 (fr) 2022-03-02
KR20190042089A (ko) 2019-04-23
US20220216520A1 (en) 2022-07-07
WO2018104674A1 (fr) 2018-06-14
FR3059993A1 (fr) 2018-06-15
CN109923063B (zh) 2023-08-15
US11316200B2 (en) 2022-04-26
JP2020500133A (ja) 2020-01-09
EP3494085A1 (fr) 2019-06-12
JP6989596B2 (ja) 2022-01-05

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