PL3494085T3 - Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu - Google Patents
Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imiduInfo
- Publication number
- PL3494085T3 PL3494085T3 PL17822387T PL17822387T PL3494085T3 PL 3494085 T3 PL3494085 T3 PL 3494085T3 PL 17822387 T PL17822387 T PL 17822387T PL 17822387 T PL17822387 T PL 17822387T PL 3494085 T3 PL3494085 T3 PL 3494085T3
- Authority
- PL
- Poland
- Prior art keywords
- fluorosulfonyl
- drying
- lithium bis
- imide salt
- purifying lithium
- Prior art date
Links
- 238000001035 drying Methods 0.000 title 1
- VDVLPSWVDYJFRW-UHFFFAOYSA-N lithium;bis(fluorosulfonyl)azanide Chemical class [Li+].FS(=O)(=O)[N-]S(F)(=O)=O VDVLPSWVDYJFRW-UHFFFAOYSA-N 0.000 title 1
- 238000000034 method Methods 0.000 title 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
- H01M10/0566—Liquid materials
- H01M10/0568—Liquid materials characterised by the solutes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
- C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0009—Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M2300/00—Electrolytes
- H01M2300/0017—Non-aqueous electrolytes
- H01M2300/0025—Organic electrolyte
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/133—Renewable energy sources, e.g. sunlight
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Electrochemistry (AREA)
- Manufacturing & Machinery (AREA)
- General Chemical & Material Sciences (AREA)
- Thermal Sciences (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Secondary Cells (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1662129A FR3059993A1 (fr) | 2016-12-08 | 2016-12-08 | Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide |
| PCT/FR2017/053446 WO2018104674A1 (fr) | 2016-12-08 | 2017-12-07 | Procédé de séchage et de purification du sel de lithium de bis(fluorosulfonyl)imide |
| EP17822387.1A EP3494085B1 (fr) | 2016-12-08 | 2017-12-07 | Procédé de séchage et de purification du sel de lithium de bis(fluorosulfonyl)imide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL3494085T3 true PL3494085T3 (pl) | 2022-05-02 |
Family
ID=58347546
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL17822387T PL3494085T3 (pl) | 2016-12-08 | 2017-12-07 | Sposób suszenia i oczyszczania soli litowej bis(fluorosulfonylo)imidu |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US11316200B2 (pl) |
| EP (1) | EP3494085B1 (pl) |
| JP (1) | JP6989596B2 (pl) |
| KR (1) | KR102397162B1 (pl) |
| CN (1) | CN109923063B (pl) |
| FR (1) | FR3059993A1 (pl) |
| PL (1) | PL3494085T3 (pl) |
| WO (1) | WO2018104674A1 (pl) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3059993A1 (fr) | 2016-12-08 | 2018-06-15 | Arkema France | Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide |
| FR3059994B1 (fr) * | 2016-12-08 | 2021-03-19 | Arkema France | Procede de sechage et de purification de lifsi |
| WO2021075871A1 (ko) | 2019-10-15 | 2021-04-22 | 한양대학교에리카산학협력단 | 고체 전해질의 중간 생성물, 이를 이용한 고체 전해질, 이를 포함하는 이차 전지, 및 그들의 제조 방법 |
| US10967295B2 (en) | 2018-11-16 | 2021-04-06 | Ses Holdings Pte. Ltd. | Processes for removing reactive solvent from lithium bis(fluorosulfonyl)imide (LiFSI) using organic solvents that are stable toward anodes in lithium-ion and lithium-metal batteries |
| KR102725403B1 (ko) * | 2018-11-16 | 2024-11-04 | 에스이에스 홀딩스 피티이. 엘티디. | 리튬 이온 및 리튬 금속 배터리 내의 애노드에 대해 안정한 유기 용매를 사용하여 리튬 비스(플루오로설포닐)이미드 (LiFSI)로부터 반응성 용매를 제거하는 방법 |
| FR3088931B1 (fr) * | 2018-11-28 | 2021-01-22 | Arkema France | Procédé de préparation du sel de lithium de bis(fluorosulfonyl)imide |
| CN113825848A (zh) | 2019-03-29 | 2021-12-21 | 锂业美洲公司 | 从沉积粘土中提取锂的方法 |
| WO2020241161A1 (ja) * | 2019-05-31 | 2020-12-03 | 株式会社日本触媒 | 電解質組成物、溶媒組成物、非水電解液及びその用途 |
| US20230089471A1 (en) * | 2020-02-27 | 2023-03-23 | Nippon Shokubai Co., Ltd. | Composition, electrolytic solution material, and electrolytic solution |
| CN111675678B (zh) * | 2020-06-29 | 2022-06-17 | 国联汽车动力电池研究院有限责任公司 | 一种用于离子液体的深度干燥除水方法 |
| JP2023541873A (ja) * | 2020-09-10 | 2023-10-04 | ソルヴェイ（ソシエテ アノニム） | ビス（フルオロスルホニル）イミド塩の精製 |
| US20250070254A1 (en) * | 2021-06-30 | 2025-02-27 | Nippon Shokubai Co., Ltd. | Method for purifying aqueous sulfonylimide solution, method for producing non-aqueous electrolyte, and method for producing electrolyte composition |
| WO2023046720A1 (en) * | 2021-09-23 | 2023-03-30 | Rhodia Operations | Method for producing ultra-pure bis(chlorosulfonyl)imide |
| US20230178804A1 (en) * | 2021-12-02 | 2023-06-08 | Honeywell International Inc. | Processes for producing lithium bis(fluorosulfonyl) imide |
| EP4273097A4 (en) * | 2022-01-29 | 2024-10-02 | Contemporary Amperex Technology Co., Limited | LITHIUM BIS(FLUOROSULFONYL)IMIDE, ITS PREPARATION METHOD, ELECTROLYTE AND SECONDARY BATTERY |
| WO2023142028A1 (zh) | 2022-01-29 | 2023-08-03 | 宁德时代新能源科技股份有限公司 | 一种在双氟磺酰亚胺锂的生产中回收原辅材料的方法 |
| CN114380305A (zh) * | 2022-01-29 | 2022-04-22 | 宁德时代新能源科技股份有限公司 | 一种在双氟磺酰亚胺锂的生产中回收原辅材料的方法 |
| FR3134576B1 (fr) | 2022-04-19 | 2025-07-18 | Arkema France | Procédé de préparation d’un sel de lithium fonctionnalisé |
| CN115677543B (zh) * | 2022-10-14 | 2023-10-20 | 衢州市九洲化工有限公司 | 一种(二氟甲磺酰基)(三氟甲磺酰基)亚胺锂的合成方法 |
| KR20250123834A (ko) * | 2022-12-15 | 2025-08-18 | 스페셜티 오퍼레이션스 프랑스 | 비스(플루오로 설포닐)이미드 염의 정제 공정 |
| JP2025539540A (ja) * | 2022-12-15 | 2025-12-05 | スペシャルティ オペレーションズ フランス | ビス（フルオロスルホニル）イミド塩の溶液を製造するための方法 |
| CN116283671A (zh) * | 2023-03-17 | 2023-06-23 | 浙江大学 | 一种低含水量双（三氟甲烷磺酰）亚胺锂的制备方法 |
| FR3149134A1 (fr) | 2023-05-25 | 2024-11-29 | Arkema France | Electrolyte à haute concentration en LiFSI |
| KR102720708B1 (ko) * | 2023-09-08 | 2024-10-22 | 주식회사 천보비엘에스 | 리튬 비스(플루오로설포닐)이미드 용액 및 이를 포함하는 전지 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101291903B1 (ko) * | 2008-07-23 | 2013-07-31 | 다이이치 고교 세이야쿠 가부시키가이샤 | 비스(플루오로설포닐)이미드 음이온 화합물의 제조 방법과 이온대화합물 |
| JP5443118B2 (ja) | 2009-03-31 | 2014-03-19 | 三菱マテリアル株式会社 | ビス（フルオロスルホニル）イミド塩の製造方法、ビス（フルオロスルホニル）イミド塩及びフルオロ硫酸塩の製造方法、並びにビス（フルオロスルホニル）イミド・オニウム塩の製造方法 |
| EP2505551B2 (en) * | 2009-11-27 | 2022-03-09 | Nippon Shokubai Co., Ltd. | Fluorosulfonyl imide salt and method for producing fluorosulfonyl imide salt |
| EP3736250B1 (en) | 2010-05-28 | 2023-07-26 | Nippon Shokubai Co., Ltd. | Alkali metal salt of fluorosulfonyl imide |
| KR101632857B1 (ko) * | 2011-03-03 | 2016-06-22 | 닛뽕소다 가부시키가이샤 | 불소 함유 술포닐이미드염의 제조 방법 |
| KR101233325B1 (ko) * | 2011-04-11 | 2013-02-14 | 로베르트 보쉬 게엠베하 | 리튬 이차 전지용 전해액 및 이를 포함하는 리튬 이차 전지 |
| GB201110520D0 (en) * | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
| FR2975694B1 (fr) * | 2011-05-24 | 2013-08-02 | Arkema France | Procede de preparation de bis(fluorosulfonyl)imidure de lithium |
| JP6208929B2 (ja) | 2011-08-12 | 2017-10-04 | 株式会社日本触媒 | フッ素原子を含むイオン性化合物またはフッ素原子を含むイオン性化合物含有組成物を包装してなる包装体 |
| KR101741939B1 (ko) * | 2013-03-18 | 2017-05-30 | 닛뽕소다 가부시키가이샤 | 디술포닐아민알칼리 금속염의 제조 방법 |
| JP6139944B2 (ja) | 2013-04-01 | 2017-05-31 | 株式会社日本触媒 | フルオロスルホニルイミドのアルカリ金属塩の製造方法 |
| JP6368466B2 (ja) * | 2013-09-09 | 2018-08-01 | 株式会社日本触媒 | フルオロスルホニルイミドの包装体の製造方法 |
| FR3020060B1 (fr) * | 2014-04-18 | 2016-04-01 | Arkema France | Preparation d'imides contenant un groupement fluorosulfonyle |
| JP2016088809A (ja) | 2014-11-05 | 2016-05-23 | 株式会社日本触媒 | フルオロスルホニルイミド塩の製造方法 |
| CN104495767B (zh) * | 2014-11-21 | 2017-01-04 | 湖南博氟新材料科技有限公司 | 一种双氟磺酰亚胺锂盐的制备方法 |
| CN104925765B (zh) * | 2015-05-21 | 2017-08-08 | 上海康鹏科技有限公司 | 一种双氟磺酰亚胺锂盐的制备方法 |
| CN105836719B (zh) * | 2016-04-29 | 2018-06-01 | 南京远淑医药科技有限公司 | 一种利用芳香甲基胺合成双氟磺酰亚胺锂盐的方法 |
| CN105923614B (zh) * | 2016-04-29 | 2018-01-09 | 南京远淑医药科技有限公司 | 一种利用邻苯二甲酰亚胺制备双氟磺酰亚胺锂盐的方法 |
| JP6806514B2 (ja) | 2016-09-27 | 2021-01-06 | 株式会社日本触媒 | ビス（フルオロスルホニル）イミドのアルカリ金属塩と有機溶媒とを含む電解液材料の製造方法 |
| FR3059993A1 (fr) | 2016-12-08 | 2018-06-15 | Arkema France | Procede de sechage et de purification du sel de lithium de bis(fluorosulfonyl)imide |
| FR3059994B1 (fr) * | 2016-12-08 | 2021-03-19 | Arkema France | Procede de sechage et de purification de lifsi |
| FR3081723B1 (fr) * | 2018-06-01 | 2022-04-15 | Arkema France | Procede de purification d'un sel de lithium de bis(fluorosulfonyl)imide |
-
2016
- 2016-12-08 FR FR1662129A patent/FR3059993A1/fr active Pending
-
2017
- 2017-12-07 WO PCT/FR2017/053446 patent/WO2018104674A1/fr not_active Ceased
- 2017-12-07 KR KR1020197009901A patent/KR102397162B1/ko active Active
- 2017-12-07 EP EP17822387.1A patent/EP3494085B1/fr active Active
- 2017-12-07 US US16/331,850 patent/US11316200B2/en active Active
- 2017-12-07 JP JP2019515221A patent/JP6989596B2/ja active Active
- 2017-12-07 PL PL17822387T patent/PL3494085T3/pl unknown
- 2017-12-07 CN CN201780068681.7A patent/CN109923063B/zh active Active
-
2022
- 2022-03-23 US US17/702,056 patent/US20220216520A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| CN109923063B (zh) | 2023-08-15 |
| JP2020500133A (ja) | 2020-01-09 |
| CN109923063A (zh) | 2019-06-21 |
| KR20190042089A (ko) | 2019-04-23 |
| US20220216520A1 (en) | 2022-07-07 |
| EP3494085A1 (fr) | 2019-06-12 |
| WO2018104674A1 (fr) | 2018-06-14 |
| EP3494085B1 (fr) | 2022-03-02 |
| FR3059993A1 (fr) | 2018-06-15 |
| US20190379088A1 (en) | 2019-12-12 |
| KR102397162B1 (ko) | 2022-05-11 |
| US11316200B2 (en) | 2022-04-26 |
| JP6989596B2 (ja) | 2022-01-05 |
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