PL427718A1 - Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen - Google Patents

Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen

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Publication number
PL427718A1
PL427718A1 PL427718A PL42771818A PL427718A1 PL 427718 A1 PL427718 A1 PL 427718A1 PL 427718 A PL427718 A PL 427718A PL 42771818 A PL42771818 A PL 42771818A PL 427718 A1 PL427718 A1 PL 427718A1
Authority
PL
Poland
Prior art keywords
amino acid
ibuprofen
acid derivative
alkyl ester
derivative
Prior art date
Application number
PL427718A
Other languages
Polish (pl)
Other versions
PL237699B1 (en
Inventor
Paula Ossowicz
Joanna Klebeko
Ewa Janus
Original Assignee
Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Zachodniopomorski Uniwersytet Technologiczny W Szczecinie filed Critical Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority to PL427718A priority Critical patent/PL237699B1/en
Publication of PL427718A1 publication Critical patent/PL427718A1/en
Publication of PL237699B1 publication Critical patent/PL237699B1/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

Przedmiotem zgłoszenia jest aminokwasowa pochodna ibuprofenu, która charakteryzuje się tym, że ma postać o wzorze, gdzie łańcuch alkilowy R stanowi łańcuch etylowy, izopropylowy, propylowy lub butylowy, a w części kationowej ma ester alkilowy L-waliny, zaś część anionową stanowi anion ibuprofenianowy. Zgłoszenie obejmuje też sposób wytwarzania aminokwasowej pochodnej ibuprofenu, polegający na reakcji równomolowej ilości estru alkilowego aminokwasu z kwasem, charakteryzuje się tym, że ester alkilowy L-waliny poddaje się reakcji z kwasem (RS)-2-[4-(2-metylopropylo)fenylo]propanowym, w środowisku rozpuszczalnika organicznego w temperaturze od 25°C do 35°C w czasie od 5 do 15 minut wytwarzając pochodną o wzorze.The subject of the application is an amino acid derivative of ibuprofen, which is characterized in the form of formula wherein the R alkyl chain is ethyl, isopropyl, propyl or butyl, and the cationic part has an L-valine alkyl ester, and the anionic part is the ibuprofenate anion. The application also includes a process for the preparation of the amino acid derivative of ibuprofen by reacting an equimolar amount of the amino acid alkyl ester with an acid, characterized in that the L-valine alkyl ester is reacted with the acid (RS) -2- [4- (2-methylpropyl) phenyl ] propane, in an organic solvent at a temperature of 25 ° C to 35 ° C for 5 to 15 minutes to generate the derivative of formula.

PL427718A 2018-11-13 2018-11-13 Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen PL237699B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL427718A PL237699B1 (en) 2018-11-13 2018-11-13 Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL427718A PL237699B1 (en) 2018-11-13 2018-11-13 Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen

Publications (2)

Publication Number Publication Date
PL427718A1 true PL427718A1 (en) 2020-05-18
PL237699B1 PL237699B1 (en) 2021-05-17

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ID=70725767

Family Applications (1)

Application Number Title Priority Date Filing Date
PL427718A PL237699B1 (en) 2018-11-13 2018-11-13 Amino acid derivative of ibuprofen and method of preparing amino acid derivative of ibuprofen

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PL (1) PL237699B1 (en)

Also Published As

Publication number Publication date
PL237699B1 (en) 2021-05-17

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