PL436027A1 - Method of obtaining poly (naringenin) - Google Patents
Method of obtaining poly (naringenin)Info
- Publication number
- PL436027A1 PL436027A1 PL436027A PL43602720A PL436027A1 PL 436027 A1 PL436027 A1 PL 436027A1 PL 436027 A PL436027 A PL 436027A PL 43602720 A PL43602720 A PL 43602720A PL 436027 A1 PL436027 A1 PL 436027A1
- Authority
- PL
- Poland
- Prior art keywords
- naringenin
- rpm
- solution
- hours
- room temperature
- Prior art date
Links
- WGEYAGZBLYNDFV-UHFFFAOYSA-N naringenin Natural products C1(=O)C2=C(O)C=C(O)C=C2OC(C1)C1=CC=C(CC1)O WGEYAGZBLYNDFV-UHFFFAOYSA-N 0.000 title abstract 4
- 229940117954 naringenin Drugs 0.000 title abstract 3
- 235000007625 naringenin Nutrition 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- FTVWIRXFELQLPI-ZDUSSCGKSA-N (S)-naringenin Chemical compound C1=CC(O)=CC=C1[C@H]1OC2=CC(O)=CC(O)=C2C(=O)C1 FTVWIRXFELQLPI-ZDUSSCGKSA-N 0.000 title 1
- FTVWIRXFELQLPI-CYBMUJFWSA-N (R)-naringenin Chemical compound C1=CC(O)=CC=C1[C@@H]1OC2=CC(O)=CC(O)=C2C(=O)C1 FTVWIRXFELQLPI-CYBMUJFWSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 239000000243 solution Substances 0.000 abstract 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 2
- IVIDDMGBRCPGLJ-UHFFFAOYSA-N 2,3-bis(oxiran-2-ylmethoxy)propan-1-ol Chemical compound C1OC1COC(CO)COCC1CO1 IVIDDMGBRCPGLJ-UHFFFAOYSA-N 0.000 abstract 1
- JLPULHDHAOZNQI-JLOPVYAASA-N [(2r)-3-hexadecanoyloxy-2-[(9e,12e)-octadeca-9,12-dienoyl]oxypropyl] 2-(trimethylazaniumyl)ethyl phosphate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C\C\C=C\CCCCC JLPULHDHAOZNQI-JLOPVYAASA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000005119 centrifugation Methods 0.000 abstract 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób otrzymywania poli(naringeniny), który polega na tym, że najpierw sporządza się roztwór (+)-naringeniny w roztworze wodnym wodorotlenku sodu, następnie sporządzony roztwór dodaje się do roztworu L-α lecytyny w cykloheksanie i całość miesza się przez 2 godziny z szybkością 1000 obrotów/minutę w temperaturze pokojowej, po czym dodaje się eter diglicydylowy glicerolu i miesza całość przez 2 godziny z szybkością 1000 obrotów/minutę. W końcu otrzymaną poli(naringeninę) przemywa się dwukrotnie cykloheksanem z odwirowaniem z szybkością 6000 obrotów/minutę w temperaturze pokojowej i suszy w temperaturze 35°C przez 72 godziny.The subject of the application is the method of obtaining poly (naringenin), which consists in preparing a solution of (+) - naringenin in an aqueous solution of sodium hydroxide, then the prepared solution is added to the solution of L-α lecithin in cyclohexane and the whole is mixed for 2 hours at 1000 rpm at room temperature, then added glycerol diglycidyl ether and stirred for 2 hours at 1000 rpm. Finally, the obtained poly (naringenin) is washed twice with cyclohexane under centrifugation at 6000 rpm at room temperature and dried at 35 ° C for 72 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL436027A PL244848B1 (en) | 2020-11-20 | 2020-11-20 | Method of obtaining poly(naringenin) |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL436027A PL244848B1 (en) | 2020-11-20 | 2020-11-20 | Method of obtaining poly(naringenin) |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL436027A1 true PL436027A1 (en) | 2022-05-23 |
| PL244848B1 PL244848B1 (en) | 2024-03-11 |
Family
ID=81710116
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL436027A PL244848B1 (en) | 2020-11-20 | 2020-11-20 | Method of obtaining poly(naringenin) |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL244848B1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL443024A1 (en) * | 2022-12-01 | 2024-06-03 | Politechnika Łódzka | Elastomer composition with increased resistance to oxidation and changing color during aging |
| CN120082184A (en) * | 2025-05-07 | 2025-06-03 | 成都大金立合成材料有限责任公司 | A kind of weather-resistant unsaturated polyester resin and its preparation method and application in photovoltaics |
-
2020
- 2020-11-20 PL PL436027A patent/PL244848B1/en unknown
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL443024A1 (en) * | 2022-12-01 | 2024-06-03 | Politechnika Łódzka | Elastomer composition with increased resistance to oxidation and changing color during aging |
| PL249428B1 (en) * | 2022-12-01 | 2026-04-13 | Politechnika Lodzka | An elastomer composition with increased resistance to oxidation and changing color during aging |
| CN120082184A (en) * | 2025-05-07 | 2025-06-03 | 成都大金立合成材料有限责任公司 | A kind of weather-resistant unsaturated polyester resin and its preparation method and application in photovoltaics |
Also Published As
| Publication number | Publication date |
|---|---|
| PL244848B1 (en) | 2024-03-11 |
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